Received 25 August 2009
Accepted 12 September 2009
Online 19 September 2009
|Single-crystal X-ray study|
|T = 298 K|
|Mean (C-C) = 0.005 Å|
|R = 0.086|
|wR = 0.246|
|Data-to-parameter ratio = 21.0|
aOrdered Matter Science Research Center, College of Chemistry and Chemical Engineering, Southeast University, Nanjing 210096, People's Republic of China
Correspondence e-mail: email@example.com
In the crystal of the title compound, C15H25NO, the molecules are linked into chains propagating in  by intermolecular N-HO hydrogen bonds.
For a related structure, see: SiMa (2009). For further synthetic details, see: Tadashi & Sasaki (1969).
Mr = 235.36
Monoclinic, C 2/c
a = 32.257 (7) Å
b = 9.4353 (19) Å
c = 9.5328 (19) Å
= 101.69 (3)°
V = 2841.1 (10) Å3
Z = 8
Mo K radiation
= 0.07 mm-1
T = 298 K
0.20 × 0.20 × 0.20 mm
Rigaku SCXmini diffractometer
Absorption correction: none
14458 measured reflections
3260 independent reflections
1544 reflections with I > 2(I)
Rint = 0.077
|D-HA ||D-H ||HA ||DA ||D-HA |
|N1-H1CO1i ||0.99 ||1.96 ||2.896 (3) ||158 |
|Symmetry code: (i) . |
Data collection: CrystalClear (Rigaku, 2005); cell refinement: CrystalClear; data reduction: CrystalClear; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: SHELXTL (Sheldrick, 2008); software used to prepare material for publication: SHELXL97.
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: HB5069 ).
The author is grateful to the starter fund of Southeast University for financial support to buy the X-ray diffractometer.
Rigaku (2005). CrystalClear. Rigaku Corporation, Tokyo, Japan.
Sheldrick, G. M. (2008). Acta Cryst. A64, 112-122.
SiMa, W. (2009). Acta Cryst. E65, o2452.
Tadashi, X. & Sasaki, Y. (1969). Bull. Chem. Soc. Jpn, 42, 1617-1621.
Acta Cryst (2009). E65, o2492 [ doi:10.1107/S1600536809036897 ]