# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 060418a in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 173.53 _exptl_crystal_F_000 708.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.5601 _cell_length_b 12.1936 _cell_length_c 13.1022 _cell_angle_alpha 64.603 _cell_angle_beta 75.781 _cell_angle_gamma 75.120 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9582.92 11800.32 831.96 o 2 0 0 5021.25 6582.09 466.33 o 3 0 0 3393.78 4285.21 306.89 o 4 0 0 3817.27 4824.69 346.24 o 5 0 0 1415.33 1517.75 116.58 o 6 0 0 2533.00 2652.29 197.83 o 7 0 0 422.61 407.82 47.07 o 8 0 0 27.27 30.47 26.49 o 9 0 0 237.25 287.59 49.98 o 10 0 0 1017.96 950.20 90.90 o 11 0 0 660.27 651.47 72.11 o 12 0 0 208.20 148.45 49.20 o 13 0 0 3.57 -53.15 35.43 o -12 1 0 42.17 -9.28 31.55 o -11 1 0 94.18 46.77 37.66 o -10 1 0 540.06 568.50 64.08 o -9 1 0 286.20 317.08 47.48 o -8 1 0 16.60 7.46 24.30 o -7 1 0 168.17 171.91 33.68 o -6 1 0 173.46 189.39 32.13 o -5 1 0 1191.00 1151.14 91.68 o -4 1 0 1760.80 2079.98 154.07 o -3 1 0 11828.18 14152.54 999.13 o -2 1 0 921.24 1177.39 60.90 o -1 1 0 1787.01 1532.10 109.73 o 0 1 0 11929.19 11835.35 844.72 o 1 1 0 7398.42 7470.01 307.00 o 2 1 0 1986.40 2503.53 116.42 o 3 1 0 1503.92 1920.24 82.33 o 4 1 0 1567.16 1899.51 100.61 o 5 1 0 8437.14 10545.39 749.36 o 6 1 0 802.58 850.22 73.83 o 7 1 0 560.81 508.07 54.39 o 8 1 0 73.16 58.21 31.11 o 9 1 0 31.84 -6.31 29.90 o 10 1 0 764.75 780.57 81.19 o 12 1 0 84.63 134.21 44.54 o 13 1 0 14.28 23.45 42.28 o -12 2 0 4.19 9.14 34.08 o -11 2 0 98.72 70.09 39.01 o -10 2 0 149.19 109.64 38.57 o -9 2 0 25.61 8.94 27.74 o -8 2 0 1.67 2.02 23.12 o -7 2 0 55.82 59.16 25.61 o -6 2 0 667.27 604.94 56.62 o -5 2 0 1641.28 1466.87 113.07 o -4 2 0 216.57 241.19 28.55 o -3 2 0 2.65 -3.77 7.63 o -1 2 0 377.38 251.31 21.23 o 0 2 0 106.83 90.82 7.90 o 1 2 0 12032.39 10439.01 429.18 o 2 2 0 546.51 510.55 23.29 o 3 2 0 318.34 330.06 17.37 o 4 2 0 19.28 18.65 7.15 o 5 2 0 1874.25 2076.13 91.02 o 6 2 0 1871.47 2331.33 176.10 o 7 2 0 1930.95 2246.50 172.73 o 8 2 0 205.16 285.36 46.34 o 9 2 0 63.56 73.23 35.10 o 10 2 0 164.32 185.34 48.29 o 11 2 0 761.03 843.37 88.91 o 12 2 0 163.93 122.26 48.80 o 13 2 0 23.66 41.07 43.57 o -12 3 0 12.98 -14.00 33.11 o -11 3 0 4.41 -11.54 29.80 o -10 3 0 9.82 -6.24 25.78 o -9 3 0 0.01 -27.77 23.89 o -8 3 0 3.87 25.07 22.71 o -7 3 0 22.86 16.37 22.41 o -6 3 0 25.82 33.68 17.95 o -5 3 0 206.20 212.37 31.25 o -4 3 0 30.44 25.91 12.40 o -3 3 0 1725.60 1631.98 84.81 o -2 3 0 171.95 170.59 18.93 o -1 3 0 965.82 893.78 67.01 o 0 3 0 1997.42 1960.61 122.57 o 1 3 0 316.48 252.09 13.37 o 2 3 0 284.74 262.05 13.94 o 3 3 0 2353.91 2164.01 91.82 o 4 3 0 181.01 215.96 14.65 o 5 3 0 1239.14 1313.81 93.15 o 6 3 0 1182.92 1165.84 55.27 o 7 3 0 16.68 5.11 13.55 o 8 3 0 392.96 510.73 56.01 o 9 3 0 652.36 747.84 74.91 o 10 3 0 150.71 154.09 43.84 o 11 3 0 256.10 281.01 57.00 o 12 3 0 339.69 272.84 55.72 o 13 3 0 26.92 5.74 43.87 o -11 4 0 58.94 3.81 31.05 o -10 4 0 29.58 19.91 31.89 o -9 4 0 9.93 -0.94 26.59 o -8 4 0 394.11 347.05 47.78 o -7 4 0 0.35 33.41 20.75 o -6 4 0 35.88 20.59 19.81 o -5 4 0 148.77 99.36 18.44 o -4 4 0 10.49 2.04 8.50 o -3 4 0 984.43 852.85 66.41 o -2 4 0 50.00 65.06 13.36 o -1 4 0 214.60 202.65 15.11 o 0 4 0 67.09 97.94 24.53 o 1 4 0 547.53 460.12 34.37 o 2 4 0 217.65 194.60 12.31 o 3 4 0 2.57 0.88 5.02 o 4 4 0 270.83 231.30 15.70 o 5 4 0 1.14 -12.68 8.46 o 6 4 0 554.40 553.49 30.60 o 7 4 0 135.01 174.01 18.91 o 8 4 0 763.17 765.60 42.18 o 9 4 0 80.87 69.08 30.27 o 10 4 0 21.47 -5.60 32.94 o 11 4 0 40.46 17.01 37.96 o 12 4 0 99.13 138.60 50.22 o 13 4 0 74.30 52.71 48.80 o -11 5 0 98.81 102.89 37.22 o -10 5 0 476.01 501.35 64.35 o -9 5 0 234.39 249.96 43.84 o -8 5 0 12.80 -32.70 21.80 o -7 5 0 87.97 52.81 25.75 o -6 5 0 4.23 -5.23 18.39 o -5 5 0 479.34 336.36 26.68 o -4 5 0 294.45 239.76 21.41 o -3 5 0 811.57 654.51 54.22 o -2 5 0 418.72 330.44 23.28 o -1 5 0 80.36 72.90 17.89 o 0 5 0 71.63 56.05 9.87 o 1 5 0 207.69 259.96 16.04 o 2 5 0 117.14 82.26 9.39 o 3 5 0 8.34 7.23 5.66 o 4 5 0 381.01 333.57 19.72 o 5 5 0 251.31 264.72 19.74 o 6 5 0 34.21 27.91 20.59 o 7 5 0 288.76 354.68 26.29 o 8 5 0 0.20 -16.99 11.33 o 9 5 0 89.25 53.44 23.45 o 10 5 0 1.06 4.59 30.71 o 11 5 0 12.87 -17.99 34.08 o 12 5 0 28.60 4.62 41.14 o 13 5 0 37.27 58.18 46.13 o -10 6 0 245.02 235.72 46.54 o -9 6 0 919.17 789.55 75.28 o -8 6 0 87.03 82.14 32.77 o -7 6 0 90.84 53.79 27.87 o -6 6 0 85.81 81.74 25.41 o -5 6 0 856.70 742.84 82.87 o -4 6 0 765.75 764.64 46.05 o -3 6 0 905.59 772.46 46.84 o -2 6 0 882.67 782.42 46.23 o -1 6 0 124.15 153.26 26.39 o 0 6 0 356.41 334.17 24.09 o 1 6 0 1008.37 807.19 38.67 o 2 6 0 116.22 89.06 11.10 o 3 6 0 6.76 4.53 6.46 o 4 6 0 48.90 47.87 10.72 o 5 6 0 14.55 0.28 8.08 o 6 6 0 244.23 248.49 21.06 o 7 6 0 369.53 370.11 27.79 o 8 6 0 151.76 170.44 20.33 o 9 6 0 280.19 352.26 38.27 o 10 6 0 34.67 10.38 27.01 o 11 6 0 0.44 1.79 30.07 o 12 6 0 4.67 10.53 33.41 o -8 7 0 120.56 143.76 38.94 o -7 7 0 16.09 3.10 26.19 o -6 7 0 129.71 129.62 31.99 o -5 7 0 419.91 344.23 100.37 o -4 7 0 1328.89 1427.98 79.43 o -3 7 0 755.13 671.64 42.74 o -2 7 0 930.24 857.62 74.32 o -1 7 0 38.78 29.97 12.79 o 0 7 0 57.23 18.56 21.97 o 1 7 0 1342.44 1419.94 64.39 o 2 7 0 4434.73 4167.65 176.35 o 3 7 0 680.14 636.50 32.39 o 4 7 0 30.13 22.40 8.53 o 5 7 0 0.86 -12.38 8.25 o 6 7 0 475.58 488.86 29.47 o 7 7 0 808.44 931.68 80.48 o 8 7 0 449.41 472.85 41.15 o 9 7 0 100.86 130.02 62.04 o 10 7 0 119.69 100.14 27.14 o 11 7 0 38.90 32.71 25.08 o 12 7 0 24.96 23.86 41.98 o -6 8 0 17.17 58.65 38.50 o -5 8 0 31.86 31.86 28.85 o -4 8 0 847.52 802.95 78.76 o -3 8 0 1146.60 1184.04 102.58 o -2 8 0 584.44 543.60 54.70 o -1 8 0 18.26 -11.44 13.19 o 0 8 0 44.57 27.95 18.51 o 1 8 0 942.58 904.11 56.09 o 2 8 0 2601.46 2492.18 135.21 o 3 8 0 251.75 271.37 38.37 o 4 8 0 3.36 4.12 12.57 o 5 8 0 361.32 278.49 29.97 o 6 8 0 690.07 708.25 49.90 o 7 8 0 730.57 810.12 56.20 o 8 8 0 373.35 496.72 45.24 o 9 8 0 97.69 71.18 35.55 o 10 8 0 30.60 -8.07 22.19 o 11 8 0 1.07 -14.16 23.42 o -7 9 0 19.36 14.24 52.54 o -6 9 0 13.25 8.64 34.62 o -5 9 0 2.74 2.77 28.41 o -4 9 0 121.08 157.93 38.10 o -3 9 0 715.95 723.75 71.70 o -2 9 0 277.93 361.39 48.62 o -1 9 0 5.91 -15.05 15.15 o 0 9 0 281.38 339.43 33.22 o 1 9 0 835.32 847.42 79.36 o 2 9 0 393.99 372.72 50.31 o 3 9 0 902.53 754.86 70.76 o 4 9 0 133.61 81.20 28.62 o 5 9 0 17.32 -16.37 23.35 o 6 9 0 16.09 6.85 27.00 o 7 9 0 266.89 287.99 49.27 o 8 9 0 321.79 321.94 56.15 o 9 9 0 220.48 225.32 51.73 o 10 9 0 1.68 -13.77 32.19 o 11 9 0 12.11 39.08 37.53 o -6 10 0 13.75 -9.08 36.04 o -5 10 0 30.08 23.83 34.18 o -4 10 0 58.74 79.85 32.50 o -3 10 0 26.25 -20.59 23.12 o -2 10 0 24.99 -10.90 19.44 o -1 10 0 86.60 87.78 38.88 o 0 10 0 25.77 5.67 29.26 o 1 10 0 37.26 41.95 28.92 o 2 10 0 259.36 225.22 39.65 o 3 10 0 611.45 578.79 62.59 o 4 10 0 8.21 -6.75 25.85 o 5 10 0 24.96 26.05 27.94 o 6 10 0 86.68 39.89 29.97 o 7 10 0 18.25 41.24 34.15 o 8 10 0 33.86 -8.71 32.70 o 9 10 0 26.27 -7.46 33.68 o 10 10 0 12.21 8.37 38.00 o -2 11 0 139.96 189.42 52.78 o -1 11 0 29.92 37.36 36.85 o 0 11 0 23.58 -0.13 34.56 o 1 11 0 93.47 52.11 34.32 o 2 11 0 254.16 299.87 48.73 o 3 11 0 24.48 12.99 28.68 o 4 11 0 9.37 -13.19 26.46 o 5 11 0 11.26 -3.54 30.84 o 6 11 0 156.84 157.76 42.62 o 7 11 0 125.39 114.91 40.90 o 8 11 0 9.28 -11.78 36.45 o 9 11 0 6.27 -11.00 42.28 o -3 12 0 13.02 38.44 52.88 o -2 12 0 11.32 46.34 43.16 o -1 12 0 1.51 -12.15 38.91 o 0 12 0 21.58 16.06 36.24 o 1 12 0 12.49 27.34 36.85 o 2 12 0 30.78 19.47 27.91 o 3 12 0 0.12 -2.33 33.31 o 4 12 0 2.61 -24.37 28.89 o 5 12 0 0.73 -16.94 33.11 o 6 12 0 40.90 26.19 36.41 o 7 12 0 14.63 13.19 33.14 o 1 13 0 0.16 25.34 37.93 o 2 13 0 0.08 -13.87 35.57 o 3 13 0 9.97 -33.04 37.29 o -6 -12 1 23.31 26.12 35.03 o -5 -12 1 31.79 4.62 34.05 o -4 -12 1 29.18 43.57 33.58 o -3 -12 1 98.51 97.83 42.25 o -2 -12 1 35.78 73.70 39.79 o -1 -12 1 46.06 37.29 41.07 o 0 -12 1 32.93 56.63 43.26 o 1 -12 1 22.46 52.61 46.30 o 2 -12 1 75.23 94.05 53.29 o -8 -11 1 42.81 -6.88 38.44 o -7 -11 1 219.38 285.19 54.16 o -6 -11 1 22.41 29.73 34.52 o -5 -11 1 2.95 -42.16 28.11 o -4 -11 1 8.88 -19.68 28.11 o -3 -11 1 178.60 230.73 47.89 o -2 -11 1 128.94 111.23 39.52 o -1 -11 1 2.96 3.58 32.70 o 0 -11 1 50.40 18.02 40.16 o 1 -11 1 53.77 72.15 41.24 o 2 -11 1 191.14 347.72 63.71 o -9 -10 1 30.51 0.98 38.37 o -8 -10 1 67.25 81.84 43.63 o -7 -10 1 112.94 128.20 38.54 o -6 -10 1 202.77 190.94 43.67 o -5 -10 1 5.82 -38.87 25.91 o -4 -10 1 31.31 -10.39 25.01 o -3 -10 1 268.87 276.18 46.67 o -2 -10 1 664.05 732.93 75.04 o -1 -10 1 36.67 3.54 31.45 o 0 -10 1 18.48 2.73 31.08 o 1 -10 1 82.50 48.60 38.23 o 2 -10 1 59.40 88.89 31.52 o 3 -10 1 449.63 482.02 62.69 o 4 -10 1 281.23 344.18 55.64 o 5 -10 1 0.80 1.55 29.39 o 6 -10 1 12.40 -8.74 35.77 o -10 -9 1 8.95 4.66 38.67 o -9 -9 1 23.85 4.66 34.02 o -8 -9 1 187.03 123.34 41.03 o -7 -9 1 179.61 118.01 39.65 o -6 -9 1 5.96 -35.26 24.97 o -5 -9 1 22.31 -7.86 26.46 o -4 -9 1 47.29 54.40 27.23 o -3 -9 1 233.34 191.65 35.16 o -2 -9 1 945.72 918.48 85.27 o -1 -9 1 454.51 468.70 39.02 o 0 -9 1 10.03 -0.62 15.53 o 1 -9 1 19.10 32.23 20.72 o 2 -9 1 284.57 270.65 43.30 o 3 -9 1 728.27 721.86 72.18 o 4 -9 1 289.85 425.67 59.86 o 5 -9 1 60.92 55.45 30.34 o 6 -9 1 3.41 -15.29 29.90 o 7 -9 1 35.27 38.81 48.63 o -11 -8 1 17.14 -20.15 35.20 o -10 -8 1 45.87 21.16 32.90 o -9 -8 1 6.12 3.64 29.53 o -8 -8 1 79.16 50.72 35.10 o -7 -8 1 152.93 118.72 35.87 o -6 -8 1 1.37 -30.62 20.41 o -5 -8 1 29.27 -20.11 24.57 o -4 -8 1 55.73 37.35 13.73 o -3 -8 1 15.77 4.82 12.02 o -2 -8 1 1123.95 1084.95 65.66 o -1 -8 1 1453.85 1423.34 82.91 o 0 -8 1 106.34 108.67 25.65 o 1 -8 1 76.25 14.34 20.01 o 2 -8 1 561.40 486.27 52.77 o 3 -8 1 1158.37 1027.98 91.65 o 4 -8 1 262.06 276.18 46.03 o 5 -8 1 24.12 14.75 24.64 o 6 -8 1 3.64 -24.77 24.87 o 7 -8 1 3.62 -43.29 30.30 o 8 -8 1 192.51 353.05 80.14 o -11 -7 1 18.18 55.62 35.84 o -10 -7 1 175.92 162.57 30.41 o -9 -7 1 179.07 174.42 44.98 o -8 -7 1 170.55 153.54 27.68 o -7 -7 1 0.37 -1.12 11.91 o -6 -7 1 123.61 99.84 16.36 o -5 -7 1 26.24 5.29 11.84 o -4 -7 1 863.54 740.64 48.13 o -3 -7 1 153.85 140.66 21.68 o -2 -7 1 730.16 636.79 50.11 o -1 -7 1 188.56 195.56 27.45 o 0 -7 1 68.62 62.13 20.62 o 1 -7 1 13.50 6.99 15.12 o 2 -7 1 24.78 -0.37 14.27 o 3 -7 1 302.03 278.58 41.81 o 4 -7 1 432.76 441.66 51.63 o 5 -7 1 39.29 26.93 25.92 o 6 -7 1 1.23 -20.25 27.13 o 7 -7 1 3.67 -31.96 34.76 o -12 -6 1 5.23 -6.78 34.66 o -11 -6 1 1.60 -27.30 32.97 o -10 -6 1 297.14 306.78 34.95 o -9 -6 1 539.38 589.64 36.21 o -8 -6 1 189.00 220.07 23.20 o -7 -6 1 68.59 57.95 30.00 o -6 -6 1 14.43 7.83 11.01 o -5 -6 1 432.32 405.27 24.68 o -4 -6 1 417.34 378.86 24.66 o -3 -6 1 260.22 267.87 33.35 o -2 -6 1 258.26 287.01 25.19 o -1 -6 1 271.84 293.98 19.12 o 0 -6 1 635.21 616.79 82.33 o 1 -6 1 948.16 852.33 48.81 o 2 -6 1 146.03 137.18 15.57 o 3 -6 1 58.09 58.32 9.80 o 4 -6 1 35.48 24.38 9.82 o 5 -6 1 119.26 81.22 18.74 o 6 -6 1 125.44 54.10 21.19 o 7 -6 1 277.78 247.83 38.37 o 8 -6 1 0.13 0.61 23.72 o 9 -6 1 265.07 217.09 42.76 o -12 -5 1 0.83 8.67 36.38 o -11 -5 1 75.05 90.68 39.15 o -10 -5 1 188.86 210.37 32.22 o -9 -5 1 586.04 635.73 46.26 o -8 -5 1 264.98 343.52 27.53 o -7 -5 1 299.66 331.79 39.50 o -6 -5 1 116.72 113.76 15.90 o -5 -5 1 443.44 476.42 31.22 o -4 -5 1 10.34 -1.95 6.98 o -2 -5 1 448.14 350.72 19.66 o -1 -5 1 24.75 22.30 6.65 o 0 -5 1 1.20 0.66 6.10 o 1 -5 1 7.76 0.57 6.21 o 2 -5 1 301.39 279.75 21.57 o 3 -5 1 897.20 794.64 37.57 o 4 -5 1 153.37 128.21 15.72 o 5 -5 1 333.35 281.11 34.83 o 6 -5 1 14.76 8.44 17.55 o 7 -5 1 2.86 3.54 21.73 o 8 -5 1 147.69 121.93 28.35 o 9 -5 1 10.87 -8.71 25.21 o 10 -5 1 1.80 -31.28 25.78 o 11 -5 1 1.98 3.95 35.13 o -12 -4 1 111.20 167.38 49.47 o -11 -4 1 248.99 303.89 55.14 o -10 -4 1 61.51 39.89 34.29 o -9 -4 1 580.31 633.89 63.67 o -8 -4 1 395.07 441.28 29.58 o -7 -4 1 241.35 245.78 33.64 o -6 -4 1 1759.43 1624.94 73.72 o -5 -4 1 3071.18 3368.63 143.59 o -4 -4 1 409.92 388.54 26.62 o -3 -4 1 8.72 -5.12 6.90 o -2 -4 1 430.66 378.19 19.94 o -1 -4 1 201.76 162.98 19.80 o 0 -4 1 1639.11 1611.99 136.22 o 1 -4 1 1285.57 1133.99 61.13 o 2 -4 1 294.91 298.01 16.44 o 3 -4 1 122.50 108.94 12.20 o 4 -4 1 397.19 394.02 37.76 o 5 -4 1 1095.08 1170.41 92.19 o 6 -4 1 141.47 123.95 25.82 o 7 -4 1 219.50 179.16 30.78 o 8 -4 1 644.06 601.67 58.68 o 9 -4 1 446.61 292.75 44.81 o 10 -4 1 59.65 73.70 31.28 o 11 -4 1 9.26 -20.65 28.65 o -13 -3 1 73.64 99.48 48.80 o -12 -3 1 154.20 126.52 46.57 o -11 -3 1 427.14 394.35 60.97 o -10 -3 1 224.05 190.50 44.92 o -9 -3 1 115.19 153.61 42.15 o -8 -3 1 555.67 555.04 41.85 o -7 -3 1 1272.30 1276.78 68.70 o -6 -3 1 1285.10 1236.89 58.08 o -5 -3 1 1297.92 1385.82 62.71 o -4 -3 1 2782.94 2971.08 126.06 o -3 -3 1 134.49 115.99 9.96 o -2 -3 1 2331.50 2053.68 87.18 o -1 -3 1 6141.90 5368.53 223.01 o 0 -3 1 4326.86 4463.78 395.43 o 1 -3 1 1358.29 1367.36 72.11 o 2 -3 1 512.98 487.42 23.36 o 3 -3 1 98.91 111.27 11.87 o 4 -3 1 2098.17 1477.40 111.45 o 5 -3 1 4031.72 3632.49 263.87 o 6 -3 1 1672.71 1649.52 127.38 o 7 -3 1 28.59 4.22 18.97 o 8 -3 1 9.14 -22.10 21.46 o 9 -3 1 644.06 507.05 55.51 o 10 -3 1 406.48 312.43 50.55 o 11 -3 1 210.58 198.60 44.81 o 12 -3 1 6.97 20.96 33.78 o -13 -2 1 2.47 -21.50 35.23 o -12 -2 1 143.42 212.74 56.09 o -11 -2 1 537.42 518.76 72.75 o -10 -2 1 219.41 268.76 52.71 o -9 -2 1 30.84 68.34 36.82 o -8 -2 1 104.05 101.54 34.66 o -7 -2 1 856.15 927.69 58.49 o -6 -2 1 3823.70 4206.28 264.02 o -5 -2 1 1493.32 1542.66 69.26 o -4 -2 1 123.13 123.00 11.45 o -3 -2 1 22.01 15.99 6.30 o -2 -2 1 1082.07 930.21 40.51 o -1 -2 1 982.61 930.68 40.82 o 0 -2 1 8088.32 7710.65 552.91 o 1 -2 1 379.95 437.45 20.09 o 2 -2 1 291.03 241.49 22.88 o 3 -2 1 838.39 1036.95 78.99 o 4 -2 1 4198.35 4671.80 335.24 o 5 -2 1 1407.15 1349.18 104.77 o 6 -2 1 237.30 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