# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 081204e in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 243.38 _exptl_crystal_F_000 776.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.6059 _cell_length_b 12.2128 _cell_length_c 14.5219 _cell_angle_alpha 104.921 _cell_angle_beta 104.271 _cell_angle_gamma 91.991 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 20063.83 19660.59 255.07 o 2 0 0 857.23 798.36 33.63 o 3 0 0 4756.75 4938.74 77.33 o 4 0 0 332.46 336.14 18.56 o 5 0 0 2539.23 2588.17 57.26 o 6 0 0 7473.22 7625.98 137.09 o 7 0 0 4240.93 4640.51 95.29 o 8 0 0 477.40 428.64 32.06 o 9 0 0 55.00 38.96 19.22 o 10 0 0 348.93 432.03 54.49 o 11 0 0 19.13 -23.55 28.88 o -11 1 0 342.02 390.93 57.54 o -10 1 0 3.18 -15.19 18.69 o -9 1 0 32.97 -10.82 15.92 o -8 1 0 5.63 -18.12 12.08 o -7 1 0 2255.60 2348.07 62.53 o -6 1 0 8081.48 8052.40 144.50 o -5 1 0 9850.17 10285.06 153.85 o -4 1 0 4072.77 3932.88 69.62 o -3 1 0 1657.85 1657.54 35.48 o -2 1 0 703.66 627.45 20.91 o -1 1 0 7891.55 7713.06 103.92 o 0 1 0 5600.13 6199.06 124.64 o 1 1 0 45124.74 42210.80 1261.12 o 2 1 0 20483.50 21635.46 221.16 o 3 1 0 443.06 486.32 18.80 o 4 1 0 1491.76 1572.45 64.38 o 5 1 0 934.47 942.27 33.39 o 6 1 0 414.94 347.41 24.50 o 7 1 0 1450.73 1501.60 50.49 o 8 1 0 589.88 556.16 40.71 o 9 1 0 66.27 39.00 19.32 o 10 1 0 442.57 453.30 55.38 o 11 1 0 254.62 329.33 55.66 o 12 1 0 96.21 101.70 43.44 o -11 2 0 925.50 1015.14 81.26 o -10 2 0 1011.53 1036.56 54.02 o -9 2 0 96.37 58.87 38.55 o -8 2 0 46.38 -12.20 18.36 o -7 2 0 1.33 -15.88 10.58 o -6 2 0 4220.29 4138.40 82.46 o -5 2 0 12762.83 13684.51 195.37 o -4 2 0 4095.43 4005.81 71.50 o -3 2 0 437.99 331.84 26.16 o -2 2 0 6.29 6.67 6.25 o -1 2 0 3939.37 3711.33 51.23 o 0 2 0 4940.24 5291.39 109.09 o 1 2 0 3023.72 2962.87 37.82 o 2 2 0 41.65 70.54 6.35 o 3 2 0 1768.21 1973.88 47.81 o 4 2 0 1365.43 1278.42 36.33 o 5 2 0 3687.89 3809.85 75.83 o 6 2 0 2266.86 2252.41 58.63 o 7 2 0 37.64 31.63 15.11 o 8 2 0 101.98 51.70 23.02 o 9 2 0 14.84 -22.27 25.88 o 10 2 0 212.33 272.56 52.21 o 11 2 0 784.47 908.94 81.15 o -12 3 0 123.91 81.04 46.05 o -11 3 0 838.54 740.81 71.04 o -10 3 0 1711.21 1791.72 95.43 o -9 3 0 791.03 799.37 42.72 o -8 3 0 16.21 -5.99 17.52 o -7 3 0 600.32 545.04 53.66 o -6 3 0 383.17 347.39 23.59 o -5 3 0 471.28 426.33 22.98 o -4 3 0 10379.54 10509.14 152.61 o -3 3 0 4282.55 4183.15 79.54 o -2 3 0 1401.64 1243.16 29.00 o 0 3 0 59236.05 55544.83 996.87 o 1 3 0 1409.67 1672.88 34.51 o 2 3 0 718.84 771.79 18.23 o 3 3 0 132.73 107.96 8.51 o 4 3 0 682.07 774.61 22.24 o 5 3 0 4264.07 4375.85 84.06 o 6 3 0 4662.88 4859.06 96.11 o 7 3 0 2215.71 2329.40 65.33 o 8 3 0 120.87 45.27 30.44 o 9 3 0 17.14 -18.05 26.77 o 10 3 0 73.51 58.60 38.88 o 11 3 0 162.06 197.91 53.71 o -12 4 0 8.93 -45.07 30.05 o -11 4 0 64.16 43.27 35.44 o -10 4 0 819.07 736.08 65.38 o -9 4 0 1205.80 1301.59 79.54 o -8 4 0 410.44 462.59 45.96 o -7 4 0 502.92 477.63 37.19 o -6 4 0 3778.40 3611.22 77.65 o -5 4 0 917.67 879.26 32.66 o -4 4 0 1971.23 2004.89 47.41 o -3 4 0 46.37 68.29 27.02 o -2 4 0 653.53 747.07 23.54 o -1 4 0 2279.31 2565.24 67.82 o 0 4 0 15040.35 15049.83 293.78 o 1 4 0 10484.40 10784.03 224.57 o 2 4 0 2884.64 3079.90 59.19 o 3 4 0 21.90 -6.50 8.03 o 4 4 0 41.15 17.77 7.62 o 5 4 0 1620.29 1615.45 36.06 o 6 4 0 3569.03 3796.55 146.53 o 7 4 0 2838.51 2872.18 117.70 o 8 4 0 803.67 827.01 68.54 o 9 4 0 16.18 -22.66 28.88 o 10 4 0 3.40 -29.05 30.49 o 11 4 0 89.26 45.32 37.83 o -11 5 0 184.29 169.08 47.94 o -10 5 0 0.11 -17.33 28.38 o -9 5 0 136.04 87.65 33.05 o -8 5 0 447.05 434.97 46.99 o -7 5 0 251.17 262.76 24.86 o -6 5 0 4340.08 4265.62 88.13 o -5 5 0 12403.27 12711.41 189.31 o -4 5 0 2283.17 2047.79 49.82 o -3 5 0 935.73 854.80 28.41 o -2 5 0 2.19 -2.78 4.08 o -1 5 0 71.74 81.54 14.89 o 0 5 0 9031.39 9944.57 211.46 o 1 5 0 16921.95 16662.70 334.16 o 2 5 0 9925.62 10700.90 157.62 o 3 5 0 1428.15 1392.86 42.48 o 4 5 0 261.88 223.55 17.36 o 5 5 0 185.19 175.53 20.31 o 6 5 0 242.67 181.02 35.66 o 7 5 0 1172.00 1145.51 75.15 o 8 5 0 1022.07 990.76 75.32 o 9 5 0 246.05 233.62 49.21 o 10 5 0 0.02 -24.33 27.61 o -11 6 0 467.69 416.03 62.49 o -10 6 0 657.89 666.32 67.88 o -9 6 0 7.33 -14.44 23.00 o -8 6 0 0.66 -11.94 21.16 o -7 6 0 1.89 -11.22 17.89 o -6 6 0 3212.28 3026.27 72.82 o -5 6 0 6998.15 6926.25 143.58 o -4 6 0 13057.87 13343.12 196.16 o -3 6 0 3310.86 3467.42 70.32 o -2 6 0 10.92 -6.03 5.87 o -1 6 0 18.68 -0.11 9.55 o 0 6 0 114.15 132.64 21.16 o 1 6 0 9424.91 9864.70 222.24 o 2 6 0 5526.44 5765.07 101.53 o 3 6 0 4242.95 4274.20 86.29 o 4 6 0 69.38 85.83 20.05 o 5 6 0 301.93 276.64 25.89 o 6 6 0 554.67 496.07 52.32 o 7 6 0 55.42 40.16 26.99 o 8 6 0 135.82 141.42 39.60 o 9 6 0 53.95 -18.16 31.16 o 10 6 0 3.48 -13.05 34.05 o -11 7 0 420.31 536.18 73.54 o -10 7 0 904.55 1026.86 82.65 o -9 7 0 1235.60 1286.87 85.93 o -8 7 0 216.00 151.08 40.10 o -7 7 0 12.51 -22.91 15.27 o -6 7 0 23.97 -2.39 16.39 o -5 7 0 2762.70 2750.90 67.86 o -4 7 0 4816.82 4798.60 93.52 o -3 7 0 5197.86 5454.21 100.31 o -2 7 0 2769.29 2669.35 56.01 o -1 7 0 39.47 17.89 13.78 o 0 7 0 343.19 242.07 28.61 o 1 7 0 2.57 -13.39 11.05 o 2 7 0 1088.76 1116.69 39.57 o 3 7 0 1588.09 1545.45 119.42 o 4 7 0 425.79 413.87 52.93 o 5 7 0 314.03 276.78 46.27 o 6 7 0 1215.95 1253.54 82.10 o 7 7 0 579.93 603.39 62.38 o 8 7 0 123.48 100.93 39.88 o 9 7 0 0.29 -39.91 26.61 o -10 8 0 588.37 641.71 69.38 o -9 8 0 813.69 970.37 79.43 o -8 8 0 883.72 940.49 72.49 o -7 8 0 65.29 15.11 27.61 o -6 8 0 406.84 346.27 43.55 o -5 8 0 255.38 233.79 35.66 o -4 8 0 322.42 324.25 25.01 o -3 8 0 2226.96 2275.86 60.24 o -2 8 0 2300.31 2239.57 53.90 o -1 8 0 71.15 24.77 19.44 o 0 8 0 2084.41 2220.64 86.37 o 1 8 0 1689.91 1625.31 75.43 o 2 8 0 369.60 363.40 26.32 o 3 8 0 24.90 2.49 19.19 o 4 8 0 75.56 6.44 24.94 o 5 8 0 105.91 59.10 28.99 o 6 8 0 447.91 414.81 55.55 o 7 8 0 1132.30 1248.77 90.43 o 8 8 0 469.55 502.41 71.38 o 9 8 0 58.96 -12.61 33.72 o -10 9 0 0.03 -41.91 27.94 o -9 9 0 353.31 279.11 51.21 o -8 9 0 597.02 613.00 61.82 o -7 9 0 150.63 109.15 37.16 o -6 9 0 248.31 121.48 37.55 o -5 9 0 1309.72 1425.62 79.82 o -4 9 0 1864.58 1887.70 87.43 o -3 9 0 167.10 188.35 21.87 o -2 9 0 136.29 120.43 22.36 o -1 9 0 99.33 24.33 19.94 o 0 9 0 181.90 118.42 29.66 o 1 9 0 2451.31 2645.66 70.10 o 2 9 0 2665.73 2635.29 71.43 o 3 9 0 836.31 795.39 46.13 o 4 9 0 86.67 39.88 30.27 o 5 9 0 24.92 -31.99 21.33 o 6 9 0 195.20 145.53 42.33 o 7 9 0 237.19 282.34 57.66 o 8 9 0 314.94 405.87 64.93 o -9 10 0 148.58 86.71 41.49 o -8 10 0 6.47 2.22 27.99 o -7 10 0 151.99 132.64 38.55 o -6 10 0 27.20 30.11 29.49 o -5 10 0 990.57 997.31 72.93 o -4 10 0 1884.41 2004.29 96.70 o -3 10 0 2602.13 2663.05 108.20 o -2 10 0 986.64 949.78 33.93 o -1 10 0 96.38 27.11 22.88 o 0 10 0 52.76 15.39 22.44 o 1 10 0 519.07 481.53 33.59 o 2 10 0 900.53 934.69 44.70 o 3 10 0 1546.77 1687.68 93.04 o 4 10 0 513.76 556.84 60.21 o 5 10 0 47.62 41.77 34.10 o 6 10 0 4.30 -33.49 28.83 o 7 10 0 27.65 -18.83 32.33 o -8 11 0 253.36 210.40 54.82 o -7 11 0 30.68 -7.94 27.44 o -6 11 0 9.82 -16.77 23.50 o -5 11 0 388.34 385.87 54.27 o -4 11 0 1824.37 2002.96 103.37 o -3 11 0 1895.91 1978.91 98.65 o -2 11 0 1223.83 1395.29 79.93 o 0 11 0 1.69 -23.05 19.44 o 1 11 0 28.83 -3.64 16.77 o 2 11 0 378.81 444.97 53.32 o 3 11 0 468.31 481.96 57.21 o 4 11 0 286.24 348.77 55.77 o 5 11 0 28.98 18.33 37.77 o 6 11 0 4.57 -29.83 32.83 o -7 12 0 182.24 212.96 51.49 o -6 12 0 15.95 -6.55 32.27 o -5 12 0 30.93 -6.78 25.50 o -4 12 0 125.05 100.15 39.33 o -3 12 0 1110.00 1198.66 81.37 o -2 12 0 1127.70 1106.57 78.71 o -1 12 0 321.66 323.22 50.66 o 0 12 0 1.74 -36.24 24.16 o 1 12 0 147.71 95.87 39.94 o 2 12 0 120.16 94.48 39.33 o 3 12 0 23.91 -3.28 31.27 o 4 12 0 85.18 49.44 37.83 o 5 12 0 17.44 21.00 37.66 o -5 13 0 10.10 19.83 31.88 o -4 13 0 7.74 -18.77 26.55 o -3 13 0 1.76 8.78 25.05 o -2 13 0 146.34 186.02 42.94 o 1 13 0 166.17 163.58 50.21 o 2 13 0 217.74 147.47 45.27 o 3 13 0 172.01 121.42 45.21 o 2 -14 1 5.86 2.61 31.77 o 3 -14 1 79.08 86.43 38.10 o -3 -13 1 135.20 104.92 47.10 o -2 -13 1 8.27 -36.55 31.83 o -1 -13 1 107.56 112.76 46.05 o 2 -13 1 59.21 65.10 32.11 o 3 -13 1 46.97 20.44 27.22 o 4 -13 1 1.50 -0.33 28.72 o 5 -13 1 181.55 182.91 51.82 o -5 -12 1 135.39 187.19 51.93 o -4 -12 1 91.80 58.21 34.55 o -3 -12 1 2.66 -1.11 29.88 o -2 -12 1 20.29 -39.74 26.50 o -1 -12 1 49.26 -11.11 26.83 o 0 -12 1 646.34 599.61 59.21 o 1 -12 1 1386.77 1436.29 88.76 o 2 -12 1 1506.65 1840.38 99.15 o 3 -12 1 125.78 61.27 37.83 o 4 -12 1 92.37 57.66 32.66 o 5 -12 1 55.72 36.88 31.33 o 6 -12 1 278.82 287.72 52.77 o 7 -12 1 517.08 584.06 69.21 o -6 -11 1 95.81 146.81 48.05 o -5 -11 1 413.56 434.14 59.16 o -4 -11 1 531.34 503.02 59.66 o -3 -11 1 241.70 274.84 49.32 o -2 -11 1 82.79 37.10 28.94 o -1 -11 1 71.30 -8.28 23.44 o 0 -11 1 300.03 354.32 47.88 o 1 -11 1 941.20 861.58 43.76 o 2 -11 1 1622.58 1661.86 56.92 o 3 -11 1 1733.95 2036.23 101.65 o 4 -11 1 90.83 61.49 33.83 o 5 -11 1 6.11 -32.33 21.55 o 6 -11 1 2.53 -21.72 23.16 o 7 -11 1 144.41 150.69 42.05 o 8 -11 1 382.69 366.43 61.10 o -7 -10 1 15.23 -12.55 33.99 o -6 -10 1 99.35 39.27 35.16 o -5 -10 1 378.54 343.60 55.82 o -4 -10 1 1256.88 1367.80 86.76 o -3 -10 1 982.53 1070.35 74.32 o -2 -10 1 63.89 59.71 27.38 o -1 -10 1 10.64 -19.39 20.55 o 0 -10 1 0.06 -19.94 17.33 o 1 -10 1 374.19 306.11 27.54 o 2 -10 1 1930.77 2142.83 60.85 o 3 -10 1 1118.24 1238.21 51.56 o 4 -10 1 286.17 200.68 40.33 o 5 -10 1 33.71 -8.94 27.77 o 6 -10 1 556.37 518.90 57.71 o 7 -10 1 153.68 116.42 37.33 o 8 -10 1 0.01 -8.78 25.66 o 9 -10 1 106.28 57.93 39.16 o -8 -9 1 245.81 239.57 56.82 o -7 -9 1 56.16 -2.94 31.49 o -6 -9 1 2.62 -21.83 25.00 o -5 -9 1 2.43 -12.00 24.61 o -4 -9 1 392.15 372.60 48.38 o -3 -9 1 1344.32 1327.86 77.93 o -2 -9 1 1504.55 1535.65 51.47 o -1 -9 1 5.90 -14.05 18.33 o 0 -9 1 568.93 527.62 48.21 o 2 -9 1 40.80 41.62 13.55 o 3 -9 1 513.32 595.76 40.91 o 4 -9 1 465.69 460.34 32.23 o 5 -9 1 17.03 0.61 20.66 o 6 -9 1 654.02 564.12 58.16 o 7 -9 1 1236.31 1194.94 79.82 o 8 -9 1 556.09 547.67 60.21 o 9 -9 1 138.35 128.42 44.55 o 10 -9 1 0.44 -42.10 32.44 o -9 -8 1 188.99 139.86 49.10 o -8 -8 1 429.39 432.25 62.71 o -7 -8 1 148.48 121.75 41.33 o -6 -8 1 7.87 -18.83 25.55 o -5 -8 1 223.30 174.63 39.99 o -4 -8 1 446.95 344.21 44.49 o -3 -8 1 43.33 24.42 14.03 o -2 -8 1 144.03 98.25 18.25 o -1 -8 1 896.36 851.51 55.38 o 0 -8 1 283.59 298.61 34.77 o 2 -8 1 5682.14 5570.04 98.21 o 3 -8 1 1208.75 1282.78 45.88 o 4 -8 1 75.24 35.25 19.75 o 5 -8 1 6.39 2.25 10.99 o 6 -8 1 149.17 129.31 31.72 o 7 -8 1 1259.20 1263.65 79.43 o 8 -8 1 1344.62 1341.36 85.71 o 9 -8 1 672.42 721.75 68.99 o 10 -8 1 132.42 92.26 41.44 o -10 -7 1 1.07 -43.33 28.88 o -9 -7 1 17.32 10.66 34.16 o -8 -7 1 168.59 146.47 43.55 o -7 -7 1 98.08 62.15 35.05 o -6 -7 1 0.67 -7.83 21.11 o -5 -7 1 1266.63 1288.20 76.71 o -4 -7 1 2888.74 2959.51 71.53 o -3 -7 1 1726.56 1676.98 48.94 o -2 -7 1 36.46 5.09 10.61 o -1 -7 1 482.39 431.81 37.33 o 0 -7 1 278.39 227.29 29.38 o 2 -7 1 8763.12 8773.70 131.81 o 3 -7 1 9729.96 10104.21 226.57 o 4 -7 1 2977.18 3055.34 154.03 o 5 -7 1 256.22 226.69 38.77 o 6 -7 1 5.43 -0.36 11.57 o 7 -7 1 190.48 110.48 33.66 o 8 -7 1 721.25 665.76 60.88 o 9 -7 1 1007.44 1108.85 81.04 o 10 -7 1 331.86 514.29 68.49 o 11 -7 1 9.86 -3.72 32.77 o -10 -6 1 262.55 262.73 54.77 o -9 -6 1 222.71 227.57 48.49 o -8 -6 1 46.68 57.16 28.99 o -7 -6 1 59.39 17.66 26.44 o -6 -6 1 7.09 -21.83 18.27 o -5 -6 1 167.42 211.45 21.66 o -4 -6 1 5193.32 5306.65 78.67 o -3 -6 1 6879.52 6994.97 116.84 o -2 -6 1 6693.49 6923.05 112.67 o -1 -6 1 1845.57 1968.19 73.82 o 0 -6 1 689.50 710.42 41.55 o 1 -6 1 1424.98 1209.97 33.52 o 2 -6 1 3314.73 3321.49 94.32 o 3 -6 1 8464.14 8345.55 133.97 o 4 -6 1 7882.90 8015.86 133.66 o 5 -6 1 2174.63 2178.92 59.29 o 6 -6 1 49.48 35.36 37.27 o 7 -6 1 68.78 73.00 17.83 o 8 -6 1 0.23 -13.78 18.11 o 9 -6 1 94.60 70.99 34.16 o 10 -6 1 390.22 361.49 56.38 o 11 -6 1 24.27 4.72 29.88 o -11 -5 1 12.65 -27.94 31.94 o -10 -5 1 139.71 177.02 49.10 o -9 -5 1 747.14 938.82 78.10 o -8 -5 1 996.38 1088.24 76.93 o -7 -5 1 444.15 408.76 48.27 o -6 -5 1 5.83 -15.12 10.08 o -5 -5 1 1.88 -10.95 7.30 o -4 -5 1 847.41 844.35 33.44 o -3 -5 1 9721.35 9811.67 118.04 o -2 -5 1 11696.44 12148.83 171.15 o -1 -5 1 6425.77 6375.86 152.42 o 0 -5 1 101.31 62.71 15.16 o 1 -5 1 146.40 111.66 10.67 o 2 -5 1 230.23 296.50 23.38 o 3 -5 1 5385.85 5611.00 96.11 o 4 -5 1 4966.50 5061.23 92.90 o 5 -5 1 1142.94 1082.31 39.88 o 6 -5 1 8.26 -13.58 17.36 o 7 -5 1 1218.00 1220.88 47.14 o 8 -5 1 743.44 653.99 57.32 o 9 -5 1 70.74 45.99 31.72 o 10 -5 1 10.17 -35.94 29.38 o 11 -5 1 17.64 -24.22 29.83 o -11 -4 1 3.56 -8.44 37.27 o -10 -4 1 77.63 71.88 38.94 o -9 -4 1 504.58 513.85 59.38 o -8 -4 1 1358.03 1454.67 86.09 o -7 -4 1 1484.12 1425.59 51.00 o -6 -4 1 1279.70 1254.36 44.72 o -5 -4 1 6.60 -16.29 10.94 o -4 -4 1 263.24 216.99 17.15 o -3 -4 1 1284.46 1203.62 26.64 o -2 -4 1 1703.00 1801.05 31.64 o -1 -4 1 4701.06 4604.02 113.09 o 0 -4 1 8.49 -0.78 8.05 o 1 -4 1 1252.28 1231.00 28.17 o 2 -4 1 5976.58 5854.07 131.31 o 3 -4 1 425.36 354.75 33.74 o 4 -4 1 620.36 702.46 28.57 o 5 -4 1 695.08 629.69 29.22 o 6 -4 1 10.97 -14.32 10.66 o 7 -4 1 1387.49 1319.53 62.29 o 8 -4 1 1945.16 1973.62 63.45 o 9 -4 1 2412.36 2481.98 75.58 o 10 -4 1 249.48 200.80 44.88 o 11 -4 1 4.82 -46.57 31.05 o -11 -3 1 23.41 -8.05 35.05 o -10 -3 1 2.59 -37.33 24.88 o -9 -3 1 43.78 -11.55 25.27 o -8 -3 1 811.96 812.66 42.31 o -7 -3 1 1767.47 1770.50 56.54 o -6 -3 1 1105.59 977.85 39.43 o -5 -3 1 147.09 120.57 16.28 o -4 -3 1 1101.08 1086.51 34.46 o -3 -3 1 590.77 585.15 17.13 o -2 -3 1 492.64 497.04 14.24 o -1 -3 1 6164.89 6453.73 140.08 o 0 -3 1 625.52 637.05 27.38 o 1 -3 1 1.70 -3.78 5.55 o 2 -3 1 3980.85 4019.91 94.70 o 3 -3 1 11516.63 10751.95 308.30 o 4 -3 1 6961.27 6927.28 111.21 o 5 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