# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' fdr004 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 487.47 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.2992 _cell_length_b 14.0353 _cell_length_c 15.6441 _cell_angle_alpha 81.137 _cell_angle_beta 82.323 _cell_angle_gamma 89.292 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 25.24 -34.34 38.35 o 2 0 0 17937.61 19306.66 1256.11 o 3 0 0 414.84 388.31 98.32 o 4 0 0 7584.96 9228.22 317.09 o 5 0 0 80.14 74.10 113.10 o 7 0 0 72.94 -217.33 160.60 o 8 0 0 39106.30 52815.38 1801.39 o 9 0 0 42.38 -288.60 192.40 o 10 0 0 19008.85 21604.97 771.14 o 11 0 0 623.06 417.14 312.59 o 12 0 0 11707.05 13729.33 2314.00 o 13 0 0 24.47 -283.14 458.79 o 14 0 0 5399.67 6498.19 697.29 o -14 1 0 1159.96 1061.04 643.48 o -13 1 0 6682.95 7641.50 1400.48 o -12 1 0 4608.36 4835.75 445.33 o -11 1 0 4357.96 5128.95 438.07 o -10 1 0 2387.13 2335.81 346.65 o -9 1 0 13582.47 16318.02 484.35 o -8 1 0 2758.17 2726.09 241.29 o -7 1 0 43797.25 52719.47 3150.92 o -6 1 0 826.58 865.57 171.01 o -5 1 0 7633.11 9649.10 340.74 o -4 1 0 260.58 194.02 102.49 o -3 1 0 12066.65 13542.87 509.32 o -2 1 0 115.61 85.10 59.43 o -1 1 0 61417.67 59822.84 1407.81 o 0 1 0 43.30 6.84 47.23 o 1 1 0 54821.13 50051.01 3961.09 o 2 1 0 534.54 588.09 72.80 o 3 1 0 20016.55 22868.54 704.24 o 4 1 0 1778.38 2298.15 146.19 o 5 1 0 20286.80 21351.31 691.92 o 6 1 0 7970.06 9036.49 277.93 o 7 1 0 27731.17 31949.77 1671.26 o 8 1 0 4864.49 5409.62 297.34 o 9 1 0 19170.78 19903.94 482.22 o 10 1 0 1771.29 1854.94 291.06 o 11 1 0 5319.97 5640.41 520.47 o 12 1 0 2220.23 2644.12 728.01 o 13 1 0 5329.04 5152.44 882.73 o 14 1 0 1402.19 1623.98 553.13 o -14 2 0 23.33 -328.78 499.81 o -13 2 0 1422.30 1072.47 527.59 o -12 2 0 677.01 614.25 358.02 o -11 2 0 1859.65 1980.79 374.16 o -10 2 0 118.05 85.70 293.09 o -9 2 0 12651.93 14028.93 706.19 o -8 2 0 39.94 4.65 185.78 o -7 2 0 2400.32 2492.13 222.19 o -6 2 0 83.05 165.48 169.25 o -5 2 0 4174.14 4961.59 212.95 o -4 2 0 614.08 624.92 113.60 o -3 2 0 1588.72 2046.14 129.98 o -2 2 0 7425.66 6512.87 222.91 o -1 2 0 24815.14 21230.94 2169.04 o 0 2 0 410.73 544.42 65.07 o 1 2 0 96.61 281.96 103.01 o 2 2 0 661.75 696.88 95.03 o 3 2 0 2838.99 3703.93 153.94 o 4 2 0 259.88 456.37 109.94 o 5 2 0 2566.93 3016.42 178.11 o 6 2 0 1158.54 1423.39 158.47 o 7 2 0 4105.73 4408.84 250.27 o 8 2 0 308.19 443.56 197.62 o 9 2 0 6494.29 6731.99 366.23 o 10 2 0 696.41 640.37 251.71 o 11 2 0 5691.54 6670.90 469.85 o 12 2 0 34.13 -219.22 393.71 o 13 2 0 4874.48 4844.68 617.60 o 14 2 0 16.79 -650.68 449.63 o -14 3 0 1153.57 1298.37 732.90 o -13 3 0 3906.92 4079.01 482.78 o -12 3 0 1382.75 1259.54 368.26 o -11 3 0 1822.22 1487.53 366.81 o -10 3 0 4885.10 4694.85 452.00 o -9 3 0 12633.66 15107.50 1422.05 o -8 3 0 6339.49 6278.24 466.05 o -7 3 0 25822.91 27446.28 1293.58 o -6 3 0 5458.52 5847.81 481.30 o -5 3 0 18611.49 18000.08 705.89 o -4 3 0 2933.24 2806.47 218.25 o -3 3 0 9675.16 8923.90 456.19 o -2 3 0 7084.42 6960.98 280.40 o -1 3 0 58658.93 58575.77 3943.51 o 0 3 0 31.63 -11.76 97.22 o 1 3 0 49751.45 44020.20 3183.03 o 2 3 0 8796.72 9201.68 527.42 o 3 3 0 18526.81 21058.31 1065.18 o 4 3 0 5565.30 4907.13 406.87 o 5 3 0 16446.95 14988.68 888.13 o 6 3 0 1074.20 852.73 158.98 o 7 3 0 12437.44 13073.28 301.39 o 8 3 0 1682.74 1740.91 239.33 o 9 3 0 5151.72 5535.63 571.47 o 10 3 0 2859.18 3369.69 374.55 o 11 3 0 5686.88 6126.52 580.61 o 12 3 0 5063.59 6159.20 641.45 o 13 3 0 4154.11 4345.19 900.49 o 14 3 0 2518.61 2698.11 615.60 o -14 4 0 7381.29 7196.72 981.76 o -13 4 0 11.33 -297.48 392.96 o -12 4 0 7103.84 8383.27 846.17 o -11 4 0 233.28 309.55 341.46 o -10 4 0 15457.15 14542.83 612.87 o -9 4 0 40.01 -45.20 277.44 o -8 4 0 41348.02 39452.78 2003.36 o -7 4 0 2.59 -66.74 225.32 o -6 4 0 54813.75 46267.96 1736.75 o -5 4 0 8.36 -62.32 120.19 o -4 4 0 13824.21 13163.76 961.24 o -3 4 0 88.42 6.43 118.13 o -2 4 0 53050.09 51444.18 2563.56 o -1 4 0 57.08 20.17 111.05 o 0 4 0 180498.23 166333.97 6583.58 o 1 4 0 1.77 0.52 131.89 o 2 4 0 46172.73 45740.73 2336.66 o 3 4 0 43.15 -22.02 117.01 o 4 4 0 50987.86 48059.91 1749.72 o 5 4 0 65.53 40.35 126.56 o 6 4 0 40271.55 36710.04 2784.32 o 7 4 0 285.06 199.24 162.85 o 8 4 0 15342.27 14141.65 666.61 o 9 4 0 874.24 1061.01 292.90 o 10 4 0 16835.37 16968.70 760.24 o 11 4 0 131.79 233.15 313.38 o 12 4 0 10523.12 11574.93 1221.59 o 13 4 0 555.42 952.11 723.45 o 14 4 0 3340.67 3511.72 892.18 o -13 5 0 5054.13 5211.79 594.86 o -12 5 0 230.24 236.64 371.53 o -11 5 0 4315.69 3612.29 414.79 o -10 5 0 2495.18 2232.13 376.62 o -9 5 0 16598.63 15982.00 1317.77 o -8 5 0 2027.39 1795.69 474.49 o -7 5 0 34794.32 33363.29 1995.59 o -6 5 0 79.16 69.37 218.74 o -5 5 0 14470.19 13031.62 541.49 o -4 5 0 91.68 172.82 128.50 o -3 5 0 30505.44 28514.71 661.55 o -2 5 0 1723.91 1786.95 268.41 o -1 5 0 38922.38 38605.62 1773.57 o 0 5 0 52.86 -26.49 122.22 o 1 5 0 35185.64 31509.73 746.65 o 2 5 0 119.92 144.86 131.33 o 3 5 0 38219.33 38390.53 607.18 o 4 5 0 1274.59 1429.81 239.40 o 5 5 0 23625.09 26521.91 691.83 o 6 5 0 338.19 307.96 176.75 o 7 5 0 18872.67 18888.11 519.28 o 8 5 0 1889.59 2087.92 353.33 o 9 5 0 15867.58 16244.41 766.26 o 10 5 0 643.97 705.59 318.84 o 11 5 0 10969.38 11309.90 706.95 o 12 5 0 3167.38 2894.25 540.30 o 13 5 0 3930.08 3587.54 587.83 o -13 6 0 1002.09 1179.46 387.18 o -12 6 0 265.02 448.45 436.23 o -11 6 0 2110.24 1889.55 411.28 o -10 6 0 447.97 414.59 346.26 o -9 6 0 13487.56 12600.22 1081.94 o -8 6 0 1163.78 1039.06 320.94 o -7 6 0 1932.42 1991.10 314.87 o -6 6 0 842.55 763.12 217.51 o -5 6 0 102.42 300.56 173.35 o -4 6 0 1367.03 1121.68 180.43 o -3 6 0 2052.22 2085.96 191.74 o -2 6 0 3708.31 3559.90 216.41 o -1 6 0 78.97 548.05 155.25 o 0 6 0 1006.05 859.69 172.78 o 1 6 0 606.81 757.12 166.60 o 2 6 0 2485.56 2166.10 200.60 o 3 6 0 740.00 730.68 176.54 o 4 6 0 4823.81 5449.22 479.13 o 5 6 0 6342.86 6956.74 287.89 o 6 6 0 2498.12 2133.00 220.08 o 7 6 0 4800.62 5155.02 341.57 o 8 6 0 1077.58 1104.68 277.16 o 9 6 0 456.97 293.58 281.56 o 10 6 0 1409.14 1186.78 454.29 o 11 6 0 2477.86 2696.53 495.40 o 12 6 0 36.04 -401.56 440.66 o 13 6 0 5768.03 5863.17 668.41 o -13 7 0 2773.57 2190.80 485.98 o -12 7 0 908.19 913.09 410.35 o -11 7 0 1636.00 1491.99 436.67 o -10 7 0 2725.36 2549.29 399.30 o -9 7 0 3703.84 3410.17 396.67 o -8 7 0 3864.28 3280.52 389.54 o -7 7 0 13111.86 11808.04 663.48 o -6 7 0 692.32 596.46 278.30 o -5 7 0 14247.93 13535.32 649.79 o -4 7 0 119.60 160.64 180.92 o -3 7 0 8927.97 8020.41 302.36 o -2 7 0 381.09 380.81 170.93 o -1 7 0 13463.82 12581.38 457.93 o 0 7 0 64.67 -86.14 172.28 o 1 7 0 12557.56 12331.60 380.94 o 2 7 0 61.89 103.52 181.26 o 3 7 0 10935.48 11268.03 553.37 o 4 7 0 2660.09 2923.38 229.24 o 5 7 0 13269.37 13807.13 599.82 o 6 7 0 5375.26 5283.86 287.96 o 7 7 0 2923.62 2413.77 288.36 o 8 7 0 1899.56 1618.04 426.63 o 9 7 0 2460.45 2141.85 436.61 o 10 7 0 2081.50 2140.93 472.56 o 11 7 0 3898.21 2680.37 518.87 o 12 7 0 6017.80 5736.33 601.78 o 13 7 0 1014.45 719.32 497.67 o -12 8 0 5796.30 5593.32 600.52 o -11 8 0 156.92 57.06 360.90 o -10 8 0 12341.14 10094.98 1000.34 o -9 8 0 356.24 272.52 313.30 o -8 8 0 19805.92 17323.30 645.46 o -7 8 0 232.06 320.30 294.14 o -6 8 0 26336.56 22967.39 1053.59 o -4 8 0 19822.10 17974.71 641.99 o -3 8 0 1420.82 1289.67 218.26 o -2 8 0 42551.89 39697.78 2039.29 o -1 8 0 378.84 462.19 196.50 o 0 8 0 36320.23 34093.36 1984.10 o 1 8 0 254.45 143.55 239.92 o 2 8 0 41031.46 38098.47 1054.68 o 3 8 0 254.65 123.72 267.89 o 4 8 0 33716.38 34506.91 926.44 o 5 8 0 925.92 988.12 215.54 o 6 8 0 16996.41 17205.33 763.43 o 7 8 0 154.95 -498.65 332.43 o 8 8 0 6077.42 6437.21 600.88 o 9 8 0 38.53 61.76 422.71 o 10 8 0 16668.51 16230.10 846.47 o 11 8 0 28.28 -294.25 420.35 o 12 8 0 6136.87 5970.46 648.21 o -12 9 0 53.39 242.67 388.93 o -11 9 0 4226.47 3770.86 538.96 o -10 9 0 827.96 910.80 407.97 o -9 9 0 12285.72 11142.03 838.54 o -8 9 0 1265.27 1615.90 362.34 o -7 9 0 22668.54 22747.66 758.05 o -6 9 0 6.29 -12.43 269.50 o -5 9 0 23572.41 24637.13 735.31 o -4 9 0 3.08 -184.06 255.58 o -3 9 0 23459.18 23652.23 1144.17 o -2 9 0 1099.96 1106.01 228.80 o -1 9 0 18625.41 18303.54 1735.34 o 0 9 0 3.04 -47.74 210.63 o 1 9 0 15282.40 15367.24 473.79 o 2 9 0 439.87 231.07 224.66 o 3 9 0 42809.50 44062.21 880.88 o 4 9 0 407.00 219.35 271.75 o 5 9 0 21339.48 20000.14 1586.15 o 6 9 0 879.45 1105.80 434.59 o 7 9 0 10323.17 8816.83 655.70 o 8 9 0 27.48 -328.14 411.94 o 9 9 0 7985.35 8559.76 687.23 o 10 9 0 295.41 266.42 452.97 o 11 9 0 6849.33 7567.27 993.97 o 12 9 0 697.71 -4.40 509.32 o -11 10 0 1090.09 1006.40 438.32 o -10 10 0 2723.53 2844.18 593.48 o -9 10 0 5535.76 5706.83 565.47 o -8 10 0 205.68 548.51 332.24 o -7 10 0 1170.62 1452.46 341.22 o -6 10 0 1401.06 1311.78 374.45 o -5 10 0 2176.80 2184.74 371.35 o -4 10 0 3114.02 3290.80 378.88 o -3 10 0 2.76 129.91 274.68 o -2 10 0 5756.34 5833.28 356.02 o -1 10 0 877.79 868.38 263.12 o 0 10 0 3522.96 3736.35 362.74 o 1 10 0 386.15 629.10 256.12 o 2 10 0 4971.42 4479.05 329.29 o 3 10 0 319.57 -39.23 311.68 o 4 10 0 4744.79 5198.29 410.36 o 5 10 0 6914.67 7200.95 620.25 o 6 10 0 1243.45 1192.36 418.49 o 7 10 0 2387.87 2677.82 527.12 o 8 10 0 1190.63 1046.86 485.64 o 9 10 0 936.22 841.02 501.69 o 10 10 0 1079.09 611.06 489.85 o 11 10 0 1717.95 787.30 515.79 o -10 11 0 2522.23 2483.12 530.22 o -9 11 0 1353.82 1996.05 709.77 o -8 11 0 381.03 616.04 411.20 o -7 11 0 1963.20 2407.62 407.55 o -6 11 0 361.02 521.74 341.79 o -5 11 0 5078.04 5280.80 447.68 o -4 11 0 36.41 -31.32 300.70 o -3 11 0 5535.80 6549.58 473.83 o -2 11 0 352.27 800.28 287.01 o -1 11 0 2828.60 3369.73 337.59 o 0 11 0 94.96 52.55 264.22 o 1 11 0 2293.32 3018.61 396.70 o 2 11 0 374.11 300.31 340.61 o 3 11 0 7792.65 7911.24 548.15 o 4 11 0 2218.68 2341.90 500.79 o 5 11 0 3306.07 3292.26 501.94 o 6 11 0 3760.59 4228.33 586.50 o 7 11 0 580.22 -123.95 421.94 o 8 11 0 374.64 713.71 478.76 o 9 11 0 1146.60 568.69 497.48 o 10 11 0 1057.69 1069.93 499.68 o -10 12 0 8648.59 8589.10 724.40 o -9 12 0 311.02 -1.66 441.41 o -8 12 0 8113.09 8498.76 670.12 o -7 12 0 5.98 324.99 363.37 o -6 12 0 11359.59 13101.74 639.15 o -5 12 0 397.45 309.17 357.56 o -4 12 0 18556.36 24066.93 806.68 o -3 12 0 267.48 136.41 314.71 o -2 12 0 17643.18 22469.10 765.52 o -1 12 0 94.32 -155.40 289.67 o 0 12 0 6849.37 8543.49 526.85 o 1 12 0 7.66 -251.01 337.73 o 2 12 0 15240.68 15992.80 893.82 o 3 12 0 274.44 387.37 335.05 o 4 12 0 24197.97 24250.90 1415.14 o 5 12 0 250.12 133.63 473.11 o 6 12 0 5861.82 5325.37 593.81 o 7 12 0 172.16 390.75 448.63 o 8 12 0 4694.48 5684.28 674.04 o 9 12 0 310.07 227.18 470.07 o -9 13 0 7318.33 8640.23 734.63 o -8 13 0 247.49 -233.98 433.43 o -7 13 0 7036.29 7653.24 688.42 o -6 13 0 101.19 93.12 381.33 o -5 13 0 15385.93 18495.72 767.33 o -4 13 0 9.05 -124.10 349.89 o -3 13 0 27168.84 32115.91 964.47 o -2 13 0 120.12 -222.40 419.12 o -1 13 0 9771.15 12901.23 781.52 o 0 13 0 21.83 -17.37 344.32 o 1 13 0 10284.71 11547.69 606.52 o 2 13 0 142.14 214.78 349.77 o 3 13 0 18468.55 20302.91 3086.15 o 4 13 0 50.82 -375.48 480.13 o 5 13 0 14174.57 14801.50 1629.15 o 6 13 0 470.30 -34.54 508.92 o 7 13 0 7159.75 7142.55 698.39 o 8 13 0 12.56 -396.59 603.42 o -7 14 0 493.51 534.55 477.69 o -6 14 0 1394.83 1650.18 534.23 o -5 14 0 1284.43 2317.24 461.15 o -4 14 0 3524.98 4352.17 621.93 o -3 14 0 3.97 184.66 494.89 o -2 14 0 2435.96 3263.20 572.28 o -1 14 0 572.35 314.61 472.53 o 0 14 0 1813.25 2547.15 433.01 o 1 14 0 16.50 -107.88 373.16 o 2 14 0 3046.33 2956.16 573.77 o 3 14 0 381.58 -145.56 471.29 o 4 14 0 3687.56 3908.38 598.27 o 5 14 0 2758.96 2408.09 604.57 o 6 14 0 2294.54 2077.22 566.41 o 7 14 0 1991.12 1487.08 586.05 o -6 15 0 157.54 -314.33 618.24 o -5 15 0 1889.93 2552.11 751.46 o -4 15 0 304.54 307.00 502.04 o -3 15 0 1914.95 2841.57 742.02 o -2 15 0 259.16 106.46 473.95 o -1 15 0 69.19 465.97 501.68 o 0 15 0 19.62 -356.34 523.61 o 1 15 0 224.67 152.30 518.97 o 2 15 0 16.37 136.62 507.12 o 3 15 0 1934.55 2188.43 548.31 o 4 15 0 499.14 385.31 538.27 o 5 15 0 200.98 411.86 540.42 o -3 16 0 1.66 146.87 528.12 o -2 16 0 8488.97 10194.87 968.40 o -1 16 0 12.64 -321.51 498.89 o 0 16 0 3851.73 4352.10 949.83 o 1 16 0 41.31 -314.33 750.81 o 2 16 0 7678.75 9049.05 1051.14 o 3 16 0 668.69 882.23 549.43 o -2 -16 1 6162.72 7197.37 1014.33 o -1 -16 1 56.44 475.24 751.79 o 0 -16 1 6224.12 7650.01 807.98 o 1 -16 1 11.67 -105.41 532.55 o 2 -16 1 7044.04 9164.96 779.57 o 3 -16 1 211.73 161.35 562.22 o -5 -15 1 1386.66 1469.64 589.27 o -4 -15 1 522.76 285.58 511.82 o -3 -15 1 119.42 510.25 525.49 o -2 -15 1 117.20 140.55 511.85 o -1 -15 1 797.16 683.23 583.55 o 0 -15 1 69.66 597.89 522.05 o 1 -15 1 467.03 52.16 520.21 o 2 -15 1 396.05 444.98 533.75 o 3 -15 1 1712.54 2102.95 597.68 o 4 -15 1 69.94 -22.21 530.18 o 5 -15 1 370.90 1242.77 593.32 o -7 -14 1 1001.45 891.70 776.87 o -6 -14 1 2530.90 2488.82 582.52 o -5 -14 1 3004.53 2617.30 580.39 o -4 -14 1 4468.94 5409.03 666.11 o -3 -14 1 125.79 -212.61 462.99 o -2 -14 1 2522.91 3109.78 592.02 o -1 -14 1 131.61 -96.57 394.13 o 0 -14 1 1230.62 2121.56 550.94 o 1 -14 1 148.13 -243.22 462.14 o 2 -14 1 3322.28 4111.18 602.02 o 3 -14 1 30.42 610.03 523.27 o 4 -14 1 2868.78 4139.79 649.75 o 5 -14 1 963.85 435.86 511.29 o 6 -14 1 3197.54 4691.50 670.03 o 7 -14 1 626.33 708.09 502.84 o -8 -13 1 55.22 -149.30 514.79 o -7 -13 1 7150.01 7637.40 714.86 o -6 -13 1 5.18 -585.28 577.52 o -5 -13 1 9576.88 10122.51 771.61 o -4 -13 1 137.49 38.76 447.04 o -3 -13 1 19684.76 21871.79 3192.99 o -2 -13 1 322.95 163.45 378.42 o -1 -13 1 10200.54 11322.08 698.36 o 0 -13 1 59.23 370.02 360.97 o 1 -13 1 10847.33 13127.87 1157.65 o 2 -13 1 482.39 809.67 500.96 o 3 -13 1 19018.19 23429.01 3993.31 o 4 -13 1 6.83 -132.73 359.31 o 5 -13 1 20271.84 23688.23 1837.70 o 6 -13 1 478.93 260.83 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