# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' a in Pc' _shelx_refln_list_code 4 _shelx_F_calc_maximum 302.62 _exptl_crystal_F_000 1172.00 _reflns_d_resolution_high 0.7330 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' _cell_length_a 11.8534 _cell_length_b 12.6329 _cell_length_c 15.3332 _cell_angle_alpha 90.000 _cell_angle_beta 98.926 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -2 0 -20 579.54 639.33 126.36 o -1 0 -20 719.71 679.61 122.02 o 0 0 -20 449.38 435.17 106.62 o 1 0 -20 1078.34 1127.02 136.24 o 2 0 -20 1373.88 1486.76 151.64 o -2 1 -20 142.13 112.45 58.28 o -1 1 -20 108.73 145.10 58.07 o 0 1 -20 813.71 748.00 88.50 o 1 1 -20 1133.92 1305.99 101.80 o 2 1 -20 800.30 736.08 120.84 o 3 1 -20 1407.55 1648.27 155.19 o -1 2 -20 356.91 393.57 74.78 o 0 2 -20 119.88 100.30 52.36 o 1 2 -20 1029.21 1193.62 101.40 o 2 2 -20 597.87 611.29 115.31 o 3 2 -20 133.75 115.70 78.19 o 6 2 -20 40.88 23.69 75.42 o -1 3 -20 42.18 40.77 51.77 o 0 3 -20 198.91 161.11 57.19 o 1 3 -20 264.27 174.94 82.14 o 2 3 -20 145.65 124.79 71.87 o 3 3 -20 928.88 1017.24 134.66 o 4 3 -20 70.93 146.50 77.00 o 5 3 -20 778.27 830.06 135.84 o 6 3 -20 871.91 927.60 141.37 o 0 4 -20 2.67 -18.16 73.84 o 1 4 -20 34.62 -7.11 65.16 o 2 4 -20 504.13 441.09 107.41 o 3 4 -20 18.35 -12.24 65.95 o 4 4 -20 115.78 66.34 74.63 o 5 4 -20 106.31 13.82 76.61 o 2 5 -20 90.25 93.19 81.35 o 3 5 -20 361.58 379.88 104.65 o -4 1 -19 222.42 257.85 66.04 o -3 1 -19 330.92 347.65 71.81 o -2 1 -19 13.17 21.94 44.52 o -1 1 -19 26.48 8.47 42.37 o 0 1 -19 56.28 12.18 45.34 o 1 1 -19 17.28 32.78 42.96 o 2 1 -19 359.11 369.52 64.87 o 3 1 -19 262.00 274.45 78.98 o 6 1 -19 12.45 30.01 69.50 o 7 1 -19 7.64 -17.77 65.16 o 8 1 -19 15.61 48.10 50.26 o -4 2 -19 68.72 97.79 54.71 o -3 2 -19 100.31 68.48 52.49 o -2 2 -19 417.37 344.92 68.36 o -1 2 -19 62.55 86.31 48.44 o 0 2 -19 292.73 246.42 58.92 o 1 2 -19 70.40 39.41 46.35 o 2 2 -19 290.56 222.30 53.17 o 3 2 -19 100.02 73.45 67.92 o 4 2 -19 389.61 387.78 88.06 o 5 2 -19 16.19 -16.98 63.18 o 6 2 -19 40.28 26.85 65.55 o 7 2 -19 27.41 22.90 71.87 o 8 2 -19 168.46 133.08 78.98 o -3 3 -19 193.64 172.02 61.74 o -2 3 -19 30.65 -0.05 47.32 o -1 3 -19 476.66 468.01 74.55 o 0 3 -19 305.76 301.08 63.45 o 1 3 -19 19.77 -8.88 41.45 o 2 3 -19 46.03 25.27 59.23 o 3 3 -19 528.97 520.47 102.28 o 4 3 -19 135.82 113.33 66.34 o 5 3 -19 312.30 233.37 57.99 o 6 3 -19 218.93 169.80 80.95 o 7 3 -19 93.68 36.33 73.45 o 8 3 -19 18.24 4.74 77.00 o -3 4 -19 6.25 7.29 49.84 o -2 4 -19 343.83 320.28 68.93 o -1 4 -19 105.54 128.66 56.18 o 0 4 -19 96.81 46.81 47.91 o 1 4 -19 320.88 386.60 97.93 o 2 4 -19 87.70 51.34 65.55 o 3 4 -19 32.42 37.12 68.32 o 4 4 -19 482.11 549.37 78.19 o 5 4 -19 68.27 58.98 45.65 o 6 4 -19 756.27 743.97 129.13 o 7 4 -19 832.18 860.07 133.87 o -2 5 -19 10.75 15.24 51.03 o -1 5 -19 8.35 0.79 48.03 o 0 5 -19 553.18 642.49 119.26 o 1 5 -19 15.45 -6.32 63.58 o 2 5 -19 351.43 370.01 98.33 o 3 5 -19 210.38 137.03 76.61 o 4 5 -19 33.35 55.57 48.93 o 5 5 -19 779.87 744.63 89.76 o 6 5 -19 638.10 647.22 83.93 o 7 5 -19 352.28 429.25 112.94 o -1 6 -19 76.62 93.43 57.11 o 0 6 -19 14.92 -23.69 63.97 o 1 6 -19 1133.35 1207.97 157.96 o 2 6 -19 158.59 137.42 75.82 o 3 6 -19 25.63 25.81 50.37 o 4 6 -19 260.09 207.11 61.70 o 5 6 -19 211.76 220.72 64.22 o 1 7 -19 80.88 23.69 71.87 o 2 7 -19 212.27 261.42 98.72 o 3 7 -19 70.57 109.64 59.32 o -5 0 -18 76.30 150.85 79.77 o -4 0 -18 1015.74 949.32 139.00 o -3 0 -18 164.25 146.90 74.24 o -2 0 -18 1953.69 2244.95 180.07 o -1 0 -18 318.86 383.83 90.43 o 0 0 -18 1129.93 1222.19 130.31 o 1 0 -18 1883.66 2036.45 157.56 o 2 0 -18 13.39 0.00 53.31 o 3 0 -18 2380.70 2737.38 171.78 o 6 0 -18 1791.58 1968.92 168.62 o 7 0 -18 228.58 191.92 79.37 o 8 0 -18 90.53 25.27 65.16 o 9 0 -18 974.62 1062.26 140.19 o 10 0 -18 413.45 501.12 116.10 o -5 1 -18 178.04 217.04 61.25 o -4 1 -18 342.39 239.78 61.31 o -3 1 -18 1363.35 1393.66 103.69 o -2 1 -18 187.67 137.72 51.24 o -1 1 -18 548.14 454.76 67.62 o 0 1 -18 759.50 720.42 77.76 o 1 1 -18 181.75 123.63 48.42 o 2 1 -18 2137.51 2281.40 114.76 o 3 1 -18 864.42 917.63 77.60 o 4 1 -18 205.97 195.87 68.32 o 5 1 -18 1237.98 1409.76 144.92 o 6 1 -18 9.13 -3.55 57.26 o 7 1 -18 767.42 705.29 83.34 o 8 1 -18 562.80 551.70 78.31 o 9 1 -18 103.83 166.87 58.59 o 10 1 -18 1598.16 1712.91 120.87 o -5 2 -18 138.65 127.90 59.62 o -4 2 -18 996.39 1009.67 108.40 o -3 2 -18 86.52 128.53 52.63 o -2 2 -18 372.54 345.63 64.05 o -1 2 -18 1090.19 1108.44 91.43 o 0 2 -18 1231.77 1331.23 96.73 o 1 2 -18 449.58 357.59 59.84 o 2 2 -18 37.50 14.49 38.12 o 3 2 -18 1362.30 1322.49 130.71 o 4 2 -18 1410.97 1399.35 96.70 o 5 2 -18 1.31 -12.31 36.26 o 6 2 -18 466.28 534.29 102.28 o 7 2 -18 457.04 467.16 98.72 o 8 2 -18 146.10 106.39 53.43 o 9 2 -18 548.12 593.37 99.91 o 10 2 -18 37.90 12.14 52.90 o -5 3 -18 83.37 91.36 55.28 o -4 3 -18 477.82 479.30 87.07 o -3 3 -18 1898.38 2159.23 126.49 o -2 3 -18 534.84 446.11 71.16 o -1 3 -18 113.02 64.15 44.11 o 0 3 -18 653.64 645.97 76.23 o 1 3 -18 21.97 6.15 39.26 o 2 3 -18 402.02 346.71 83.32 o 3 3 -18 1011.59 996.70 116.89 o 4 3 -18 568.84 598.89 72.99 o 5 3 -18 982.12 966.20 87.36 o 6 3 -18 111.73 125.97 68.32 o 7 3 -18 319.67 287.48 86.88 o 8 3 -18 204.61 167.83 79.77 o 9 3 -18 246.77 303.94 67.49 o -5 4 -18 156.39 117.41 59.05 o -4 4 -18 524.21 465.31 76.91 o -3 4 -18 11.73 -4.04 45.54 o -2 4 -18 370.78 310.64 66.02 o -1 4 -18 557.79 567.76 76.50 o 0 4 -18 142.54 127.98 53.51 o 1 4 -18 429.39 534.98 69.95 o 2 4 -18 132.97 132.29 74.63 o 3 4 -18 537.30 547.20 73.16 o 4 4 -18 1046.86 1092.52 89.97 o 5 4 -18 43.17 35.73 42.68 o 6 4 -18 416.01 368.50 67.36 o 7 4 -18 54.29 29.62 66.74 o 8 4 -18 56.02 34.36 62.39 o 9 4 -18 14.49 23.30 69.90 o -4 5 -18 114.17 104.76 55.19 o -3 5 -18 129.01 59.00 51.27 o -2 5 -18 259.77 192.05 57.16 o -1 5 -18 29.12 3.15 44.91 o 0 5 -18 40.83 1.51 43.04 o 1 5 -18 46.09 28.43 60.81 o 2 5 -18 150.40 75.03 64.76 o 3 5 -18 348.62 265.03 81.15 o 4 5 -18 75.25 40.20 47.58 o 5 5 -18 386.70 355.27 66.31 o 6 5 -18 110.27 89.39 47.69 o 7 5 -18 473.89 465.97 105.83 o 8 5 -18 159.71 251.55 92.40 o -3 6 -18 85.96 39.26 51.75 o -2 6 -18 5.58 37.73 48.35 o -1 6 -18 146.03 149.02 55.43 o 0 6 -18 22.89 3.16 64.37 o 1 6 -18 76.72 55.28 66.34 o 2 6 -18 1.38 25.67 61.60 o 3 6 -18 54.75 53.43 46.63 o 4 6 -18 246.46 206.26 56.89 o 5 6 -18 233.31 151.15 56.12 o 6 6 -18 410.21 325.47 68.40 o 7 6 -18 318.14 233.59 60.93 o 8 6 -18 10.04 42.65 75.42 o -2 7 -18 29.92 -17.00 48.58 o -1 7 -18 43.00 -31.59 65.55 o 0 7 -18 414.00 426.88 102.28 o 1 7 -18 34.66 -16.98 63.58 o 2 7 -18 56.98 37.91 75.42 o 3 7 -18 56.57 12.11 46.91 o 4 7 -18 53.20 23.59 50.09 o 5 7 -18 77.61 84.41 51.21 o 6 7 -18 225.11 212.71 62.02 o 7 7 -18 332.72 299.45 68.89 o -1 8 -18 26.25 -18.16 67.53 o 0 8 -18 163.88 133.08 83.32 o 1 8 -18 809.03 869.55 140.19 o 2 8 -18 102.12 85.30 54.93 o 3 8 -18 64.37 14.05 47.74 o 4 8 -18 18.95 -18.81 48.84 o 5 8 -18 0.57 -8.60 48.86 o -7 1 -17 46.85 52.05 51.64 o -6 1 -17 8.55 22.71 46.94 o -5 1 -17 3.08 12.94 44.36 o -4 1 -17 228.40 192.57 54.99 o -3 1 -17 77.55 56.76 43.80 o -2 1 -17 55.44 55.02 41.45 o -1 1 -17 115.07 114.73 42.84 o 0 1 -17 111.23 62.00 38.25 o 1 1 -17 10.89 -3.15 33.22 o 2 1 -17 246.08 190.01 44.78 o 3 1 -17 175.24 168.75 44.52 o 4 1 -17 553.01 439.06 61.12 o 5 1 -17 205.10 151.96 47.16 o 6 1 -17 21.02 9.47 37.93 o 7 1 -17 63.58 79.34 44.25 o 8 1 -17 255.66 237.23 58.62 o 9 1 -17 246.80 316.45 61.57 o 10 1 -17 24.13 47.99 50.50 o 11 1 -17 107.40 94.13 54.87 o -7 2 -17 124.80 102.36 58.88 o -6 2 -17 66.53 80.24 52.33 o -5 2 -17 241.19 216.40 58.35 o -4 2 -17 123.39 107.01 48.58 o -3 2 -17 79.92 43.46 43.74 o -2 2 -17 3.20 13.86 38.61 o -1 2 -17 22.25 8.67 37.21 o 0 2 -17 870.88 941.08 81.45 o 1 2 -17 89.90 73.06 38.05 o 2 2 -17 1.87 -0.20 34.26 o 3 2 -17 529.03 481.61 59.18 o 4 2 -17 224.97 139.01 46.59 o 5 2 -17 399.81 417.73 77.00 o 6 2 -17 49.23 57.26 56.07 o 7 2 -17 42.66 57.43 42.56 o 8 2 -17 368.11 425.28 68.20 o 9 2 -17 395.42 356.78 66.75 o 10 2 -17 12.24 16.27 47.43 o 11 2 -17 16.42 -21.29 49.98 o -6 3 -17 170.06 122.69 55.98 o -5 3 -17 70.67 36.03 47.99 o -4 3 -17 238.03 208.28 77.60 o -3 3 -17 231.13 218.78 55.99 o -2 3 -17 89.52 81.93 47.19 o -1 3 -17 965.98 844.20 82.48 o 0 3 -17 305.92 290.36 57.23 o 1 3 -17 135.72 121.82 43.00 o 2 3 -17 1438.67 1489.99 147.69 o 3 3 -17 109.06 118.13 43.87 o 4 3 -17 139.69 125.51 46.48 o 5 3 -17 498.26 502.87 65.20 o 6 3 -17 247.67 219.37 51.06 o 7 3 -17 458.37 476.63 98.33 o 8 3 -17 393.99 401.08 68.47 o 9 3 -17 189.83 172.15 57.65 o 10 3 -17 170.28 86.90 55.08 o -6 4 -17 18.41 30.33 48.90 o -5 4 -17 761.76 852.59 115.31 o -4 4 -17 113.78 80.48 51.06 o -3 4 -17 87.26 86.44 46.71 o -2 4 -17 1463.90 1559.87 104.52 o -1 4 -17 192.47 136.71 48.56 o 0 4 -17 1060.32 1060.00 83.63 o 1 4 -17 563.70 565.99 67.98 o 2 4 -17 124.79 134.26 62.00 o 3 4 -17 361.10 295.23 55.28 o 4 4 -17 14.80 14.15 35.30 o 5 4 -17 106.69 112.46 46.07 o 6 4 -17 1672.64 1864.20 110.88 o 7 4 -17 44.74 63.18 61.21 o 8 4 -17 118.28 129.52 73.84 o 9 4 -17 244.06 280.77 93.19 o 10 4 -17 56.00 14.61 70.69 o -6 5 -17 958.44 1070.05 142.16 o -5 5 -17 56.95 42.23 50.61 o -4 5 -17 188.85 171.88 56.89 o -3 5 -17 157.42 152.14 55.79 o -2 5 -17 353.49 373.70 66.34 o -1 5 -17 1690.52 1590.05 104.69 o 0 5 -17 300.15 315.60 59.61 o 1 5 -17 721.73 734.18 77.76 o 2 5 -17 783.00 923.77 87.71 o 3 5 -17 103.00 67.31 42.81 o 4 5 -17 131.74 115.77 48.56 o 5 5 -17 390.87 408.14 65.50 o 6 5 -17 29.31 3.36 39.51 o 7 5 -17 849.45 784.61 84.49 o 8 5 -17 37.21 -16.19 63.18 o 9 5 -17 151.34 180.46 82.93 o 10 5 -17 33.13 34.75 73.45 o -5 6 -17 446.93 434.35 75.39 o -4 6 -17 531.39 660.80 85.41 o -3 6 -17 123.65 49.16 49.87 o -2 6 -17 754.25 752.48 85.13 o -1 6 -17 380.74 347.84 64.75 o 0 6 -17 1277.35 1339.64 96.33 o 1 6 -17 214.60 147.69 71.08 o 2 6 -17 44.99 50.45 42.53 o 3 6 -17 574.97 540.64 99.12 o 4 6 -17 17.95 -27.89 36.82 o 5 6 -17 173.04 91.83 49.36 o 6 6 -17 1195.21 1252.14 98.93 o 7 6 -17 455.81 255.74 59.84 o 8 6 -17 895.22 870.34 135.05 o 9 6 -17 330.38 227.06 90.04 o -4 7 -17 23.85 -27.25 47.56 o -3 7 -17 1172.67 1168.18 101.14 o -2 7 -17 94.74 74.28 50.09 o -1 7 -17 1474.21 1521.49 105.67 o 0 7 -17 163.16 103.86 71.48 o 1 7 -17 66.12 26.06 63.97 o 2 7 -17 691.07 696.94 80.86 o 3 7 -17 36.64 34.65 47.17 o 4 7 -17 264.42 260.85 59.91 o 5 7 -17 346.97 392.43 68.30 o 6 7 -17 58.64 23.22 47.59 o 7 7 -17 941.42 959.01 94.99 o 8 7 -17 1124.26 1173.35 98.95 o -3 8 -17 2.42 -16.64 48.46 o -2 8 -17 1052.28 1098.69 103.41 o -1 8 -17 52.08 11.06 64.37 o 0 8 -17 885.48 916.15 136.24 o 1 8 -17 974.44 815.84 129.13 o 2 8 -17 22.87 28.07 45.95 o 3 8 -17 684.34 637.12 81.20 o 4 8 -17 101.11 156.31 56.20 o 5 8 -17 80.88 51.95 48.75 o 6 8 -17 671.86 636.56 83.04 o 7 8 -17 107.42 42.12 50.24 o -2 9 -17 261.93 246.81 92.01 o -1 9 -17 2052.16 2163.60 190.34 o 0 9 -17 82.81 74.63 72.26 o 1 9 -17 918.83 925.62 139.79 o 2 9 -17 2013.52 2229.84 129.99 o 3 9 -17 437.74 393.59 109.58 o 4 9 -17 169.86 164.15 58.23 o 5 9 -17 35.19 45.13 50.60 o 6 9 -17 25.39 24.42 50.95 o 2 10 -17 74.40 27.88 50.63 o -8 0 -16 118.88 139.40 83.32 o -7 0 -16 3.98 -10.66 60.02 o -6 0 -16 584.60 435.56 99.51 o -5 0 -16 222.54 273.66 84.11 o -4 0 -16 35.12 11.06 52.52 o -3 0 -16 2813.53 3006.70 188.36 o -2 0 -16 3863.03 3772.39 206.13 o -1 0 -16 660.00 530.73 91.61 o 0 0 -16 29.28 26.46 44.62 o 1 0 -16 1157.51 1017.24 104.65 o 2 0 -16 853.58 902.72 99.12 o 3 0 -16 849.13 777.93 91.22 o 4 0 -16 110.83 121.42 39.74 o 5 0 -16 1172.19 1318.22 82.47 o 6 0 -16 798.50 887.32 110.57 o 7 0 -16 129.99 92.80 62.39 o 8 0 -16 2179.17 2418.31 178.10 o 9 0 -16 467.94 550.48 101.09 o 10 0 -16 868.05 779.51 120.84 o 11 0 -16 2222.94 2384.74 183.23 o 12 0 -16 21.31 112.54 83.32 o -8 1 -16 32.58 3.20 49.11 o -7 1 -16 367.70 344.69 69.01 o -6 1 -16 242.90 265.41 94.58 o -5 1 -16 798.97 705.85 81.66 o -4 1 -16 585.77 636.14 75.94 o -3 1 -16 579.96 639.48 73.08 o -2 1 -16 364.05 404.81 59.38 o -1 1 -16 1344.40 1317.17 103.07 o 0 1 -16 451.86 424.45 57.94 o 1 1 -16 368.13 344.22 51.23 o 2 1 -16 3128.54 3453.47 125.22 o 3 1 -16 369.02 277.55 47.63 o 4 1 -16 2436.09 2546.47 88.68 o 5 1 -16 1960.76 2161.42 96.85 o 6 1 -16 505.62 567.56 70.29 o 7 1 -16 1398.48 1618.32 102.46 o 8 1 -16 10.49 9.68 36.96 o 9 1 -16 1154.32 1077.76 89.77 o 10 1 -16 779.66 912.32 94.18 o 11 1 -16 140.86 141.59 55.03 o 12 1 -16 725.10 732.04 89.48 o -8 2 -16 757.50 832.11 96.88 o -7 2 -16 557.96 522.85 79.13 o -6 2 -16 317.54 327.28 65.31 o -5 2 -16 168.79 135.13 50.37 o -4 2 -16 13.43 -8.48 36.72 o -3 2 -16 951.62 917.63 86.00 o -2 2 -16 2084.92 2269.17 116.15 o -1 2 -16 91.69 57.60 35.60 o 0 2 -16 1089.00 1099.16 79.14 o 1 2 -16 964.42 1005.32 76.35 o 2 2 -16 1378.75 1407.05 120.44 o 3 2 -16 2615.28 2713.87 93.36 o 4 2 -16 382.00 320.92 51.78 o 5 2 -16 970.97 958.95 76.08 o 6 2 -16 532.41 558.65 54.19 o 7 2 -16 84.05 66.55 40.14 o 8 2 -16 2756.44 3034.31 166.64 o 9 2 -16 67.25 46.53 42.71 o 10 2 -16 335.37 363.31 66.39 o 11 2 -16 591.48 626.10 81.91 o 12 2 -16 17.96 -26.66 48.59 o -7 3 -16 926.54 859.15 95.36 o -6 3 -16 745.54 692.87 85.70 o -5 3 -16 7.16 11.73 41.17 o -4 3 -16 567.33 710.49 79.68 o -3 3 -16 73.04 47.96 40.07 o -2 3 -16 72.14 66.77 38.67 o -1 3 -16 342.05 335.19 55.53 o 0 3 -16 112.26 104.02 40.42 o 1 3 -16 470.28 411.37 57.83 o 2 3 -16 883.72 889.44 58.78 o 3 3 -16 708.11 652.77 53.72 o 4 3 -16 3400.06 3484.93 181.85 o 5 3 -16 787.64 707.59 72.47 o 6 3 -16 393.86 291.64 53.84 o 7 3 -16 1390.93 1403.83 96.19 o 8 3 -16 119.86 158.62 49.90 o 9 3 -16 95.86 66.84 43.21 o 10 3 -16 37.98 57.10 48.58 o 11 3 -16 4.72 43.01 49.36 o -7 4 -16 496.67 568.80 83.01 o -6 4 -16 247.74 257.74 61.92 o -5 4 -16 162.81 162.37 53.86 o -4 4 -16 11.32 -11.00 39.47 o -3 4 -16 512.70 511.05 68.91 o -2 4 -16 234.93 200.06 50.52 o -1 4 -16 381.81 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