# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 090818_0835' _shelx_refln_list_code 4 _shelx_F_calc_maximum 725.54 _exptl_crystal_F_000 1256.00 _reflns_d_resolution_high 0.7672 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 7.7642 _cell_length_b 17.6520 _cell_length_c 14.1240 _cell_angle_alpha 90.000 _cell_angle_beta 98.188 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9.09 42.13 13.56 o 4 0 0 55015.45 55009.31 866.60 o 6 0 0 231.43 185.76 68.25 o 8 0 0 11431.71 11778.99 394.32 o 1 1 0 16276.01 17041.92 192.35 o 2 1 0 60021.26 63050.55 830.64 o 3 1 0 13968.09 13378.28 315.01 o 4 1 0 4260.50 4422.83 95.51 o 5 1 0 6190.43 6204.14 152.50 o 6 1 0 13674.25 13401.92 250.53 o 7 1 0 5506.63 5574.96 162.64 o 8 1 0 3438.63 3409.39 141.12 o 9 1 0 331.15 373.19 80.31 o 0 2 0 13289.93 13568.49 313.43 o 1 2 0 3300.39 3640.23 50.04 o 2 2 0 7723.27 8204.20 119.04 o 3 2 0 366.13 344.99 28.46 o 4 2 0 5705.67 5621.11 113.64 o 5 2 0 11200.70 11305.87 275.82 o 6 2 0 12735.72 12611.60 308.95 o 7 2 0 6824.80 6497.29 175.56 o 8 2 0 6.31 17.09 47.21 o 9 2 0 337.15 391.38 83.41 o 1 3 0 2675.02 2697.81 61.64 o 2 3 0 17877.04 18635.77 224.09 o 3 3 0 7914.98 8054.46 174.74 o 4 3 0 14845.16 15012.83 315.22 o 5 3 0 6134.86 5963.55 182.42 o 6 3 0 2513.32 2566.03 225.91 o 7 3 0 949.90 963.16 95.23 o 8 3 0 5183.92 5156.11 201.22 o 9 3 0 4492.76 4704.41 206.86 o 0 4 0 37744.58 39183.82 864.46 o 1 4 0 26795.57 27869.85 455.25 o 2 4 0 587.31 625.03 43.15 o 3 4 0 23686.00 23432.62 257.56 o 4 4 0 54251.23 55096.85 638.66 o 5 4 0 41920.70 41103.20 520.99 o 6 4 0 679.63 635.91 70.05 o 7 4 0 1971.51 1942.19 135.80 o 8 4 0 2221.14 2395.97 362.29 o 9 4 0 3667.81 4128.05 211.27 o 1 5 0 67720.30 69975.05 873.41 o 2 5 0 63.48 102.24 17.94 o 3 5 0 80585.20 81411.08 784.77 o 4 5 0 10612.51 10443.73 176.94 o 5 5 0 10107.32 10068.47 377.24 o 6 5 0 1441.55 1458.83 242.66 o 7 5 0 13159.81 12986.92 391.31 o 8 5 0 7.61 -10.38 44.33 o 9 5 0 12.57 101.47 62.23 o 0 6 0 109649.53 109548.88 2310.28 o 1 6 0 18241.16 18794.89 287.82 o 2 6 0 0.97 3.37 13.86 o 3 6 0 154.11 172.76 18.66 o 4 6 0 2113.05 2178.45 70.37 o 5 6 0 5218.72 5140.94 173.89 o 6 6 0 38.29 48.03 42.90 o 7 6 0 9656.65 9631.96 409.48 o 8 6 0 3319.52 3523.48 196.90 o 9 6 0 1323.50 1346.25 133.40 o 1 7 0 8390.78 8729.22 210.54 o 2 7 0 7.68 23.15 15.95 o 3 7 0 3954.08 4246.06 100.26 o 4 7 0 840.32 825.15 47.60 o 5 7 0 8728.58 8590.07 213.01 o 6 7 0 511.65 483.50 61.59 o 7 7 0 10057.07 9516.12 330.29 o 8 7 0 1364.13 1350.63 125.05 o 9 7 0 2746.55 3101.80 298.57 o 0 8 0 22033.63 23375.82 631.92 o 1 8 0 32024.86 31872.16 614.22 o 2 8 0 4418.46 4786.08 127.88 o 3 8 0 4980.68 4804.55 113.16 o 4 8 0 34.79 30.12 25.94 o 5 8 0 10760.32 10296.71 243.48 o 6 8 0 2393.31 2330.38 124.85 o 7 8 0 559.66 637.61 103.66 o 8 8 0 117.51 142.59 60.24 o 9 8 0 9501.42 9979.12 515.64 o 1 9 0 41497.24 41357.37 720.13 o 2 9 0 75300.06 76318.98 1002.40 o 3 9 0 10470.10 10160.12 192.32 o 4 9 0 4118.70 4153.98 141.66 o 5 9 0 3961.81 3968.92 196.72 o 6 9 0 13110.62 13150.79 304.05 o 7 9 0 7035.23 6919.39 281.31 o 8 9 0 1407.68 1509.11 135.92 o 9 9 0 70.70 195.25 94.27 o 0 10 0 17720.72 18467.10 566.20 o 1 10 0 1820.69 1913.14 105.41 o 2 10 0 1656.89 1615.07 214.85 o 3 10 0 45.22 23.27 20.36 o 4 10 0 45638.64 45411.50 691.47 o 5 10 0 3532.65 3713.46 146.35 o 6 10 0 4320.61 4331.28 167.99 o 7 10 0 34.46 64.46 56.86 o 8 10 0 5042.12 4791.68 508.06 o 9 10 0 1097.55 1107.12 232.54 o 1 11 0 1650.74 1617.96 119.39 o 2 11 0 3622.57 3442.68 197.16 o 3 11 0 12054.70 11932.27 223.53 o 4 11 0 1797.09 1828.13 118.52 o 5 11 0 650.13 560.89 107.18 o 6 11 0 2087.95 2073.00 137.54 o 7 11 0 9.10 44.37 63.16 o 8 11 0 6408.59 6316.26 307.36 o 0 12 0 599.25 647.08 111.22 o 1 12 0 356.22 399.52 64.05 o 2 12 0 4184.23 3836.99 222.43 o 3 12 0 1976.35 2111.44 153.59 o 4 12 0 6414.23 6615.51 204.19 o 5 12 0 2165.04 2097.44 136.73 o 6 12 0 6421.46 6715.93 358.08 o 7 12 0 1587.76 1663.91 173.34 o 8 12 0 1269.74 1165.64 160.38 o 1 13 0 311.96 303.01 136.49 o 2 13 0 31944.64 31775.69 640.75 o 3 13 0 429.75 463.38 75.47 o 4 13 0 2371.96 2280.48 141.66 o 5 13 0 139.54 109.17 70.78 o 6 13 0 16618.35 16809.00 388.43 o 7 13 0 4931.84 5611.41 399.37 o 8 13 0 1932.45 1745.62 331.12 o 0 14 0 10427.91 10783.01 460.03 o 1 14 0 28853.91 30756.59 894.79 o 2 14 0 1614.52 1491.32 197.16 o 3 14 0 1304.59 1201.84 128.38 o 4 14 0 17660.86 18211.31 479.00 o 5 14 0 14225.26 14116.92 442.64 o 6 14 0 677.47 540.15 85.00 o 7 14 0 25.48 35.39 101.11 o 1 15 0 11308.12 11550.99 341.23 o 2 15 0 1320.23 1276.19 124.50 o 3 15 0 8913.42 8900.14 392.56 o 4 15 0 3157.55 3548.34 198.18 o 5 15 0 7.05 36.65 56.86 o 6 15 0 927.71 982.75 187.05 o 7 15 0 7260.09 6440.48 449.92 o 0 16 0 23.15 85.94 65.72 o 1 16 0 1543.83 1598.06 144.48 o 2 16 0 6.23 -5.06 42.90 o 3 16 0 611.31 543.57 98.25 o 4 16 0 2114.04 1910.19 175.05 o 5 16 0 152.29 103.33 73.30 o 6 16 0 107.64 45.50 111.22 o 7 16 0 111.37 20.22 111.22 o 1 17 0 5929.45 5995.85 568.72 o 2 17 0 70.42 128.91 56.86 o 3 17 0 1899.54 1860.36 247.71 o 4 17 0 310.32 312.42 89.15 o 5 17 0 6.84 0.00 96.05 o 6 17 0 3604.19 3776.33 384.20 o 0 18 0 8.32 20.22 75.83 o 1 18 0 12374.82 12203.11 1018.65 o 2 18 0 1.91 4.04 52.20 o 3 18 0 1066.90 1213.28 212.32 o 4 18 0 6912.98 7125.33 312.77 o 5 18 0 20259.88 19877.54 818.96 o 6 18 0 868.33 889.74 212.32 o 1 19 0 1327.36 1076.76 135.27 o 2 19 0 11247.29 11617.62 563.67 o 3 19 0 2128.33 2105.73 224.96 o 4 19 0 2533.65 2285.01 298.26 o 5 19 0 430.17 510.59 171.88 o 0 20 0 8329.58 8740.66 475.20 o 1 20 0 994.92 809.47 235.07 o 2 20 0 531.59 590.07 262.88 o 3 20 0 377.57 374.36 101.83 o 4 20 0 3504.90 3720.72 399.37 o 1 21 0 55.04 35.25 66.06 o 2 21 0 728.15 859.06 136.49 o 3 21 0 3505.59 3109.02 353.87 o 4 21 0 1602.12 1546.93 278.04 o 0 22 0 8915.61 9145.08 515.64 o 1 22 0 425.60 455.98 108.98 o 2 22 0 54.48 35.39 111.22 o -9 0 1 1194.68 1248.67 227.49 o -7 0 1 9755.31 9554.31 309.46 o -5 0 1 25623.88 24129.07 722.91 o -3 0 1 54463.64 55594.98 968.10 o -1 0 1 429.06 446.73 27.80 o 1 0 1 57693.69 60479.82 947.78 o 3 0 1 16572.17 15949.41 299.11 o 5 0 1 26041.28 26286.19 528.90 o 7 0 1 10197.69 10168.54 324.76 o 9 0 1 14410.39 15560.29 687.52 o -10 1 1 3072.32 2930.44 252.77 o -9 1 1 1795.75 1832.83 148.68 o -8 1 1 2386.87 2274.10 129.09 o -7 1 1 3724.77 3999.38 136.63 o -6 1 1 9849.28 8983.69 287.74 o -5 1 1 3335.68 3145.03 148.32 o -4 1 1 7288.20 7462.02 181.03 o -3 1 1 3998.21 3875.38 142.28 o -2 1 1 9169.58 9034.29 148.75 o -1 1 1 5442.41 5515.21 75.48 o 0 1 1 572.88 529.40 22.97 o 1 1 1 194.82 248.28 13.56 o 2 1 1 7081.41 7084.17 86.44 o 3 1 1 12867.04 12720.28 157.00 o 4 1 1 29918.80 30753.42 309.28 o 5 1 1 1567.32 1557.16 80.37 o 6 1 1 6197.30 6106.22 180.05 o 7 1 1 5.59 -21.68 29.04 o 8 1 1 11247.96 11632.53 265.63 o 9 1 1 6016.92 6002.85 230.32 o -10 2 1 1762.47 1994.58 257.82 o -9 2 1 1032.43 1122.04 120.73 o -8 2 1 761.75 718.58 139.58 o -7 2 1 4222.08 4303.16 161.11 o -6 2 1 7682.99 7677.30 207.24 o -5 2 1 2029.43 2059.61 93.43 o -4 2 1 4.92 19.72 18.33 o -3 2 1 7651.92 7415.83 258.64 o -2 2 1 28903.38 31617.24 513.82 o -1 2 1 1449.80 1536.84 35.98 o 0 2 1 30852.67 32469.12 398.77 o 1 2 1 9986.70 10168.75 115.01 o 2 2 1 5.50 1.19 7.90 o 3 2 1 1020.22 1139.30 35.60 o 4 2 1 1086.64 1222.54 55.01 o 5 2 1 1514.42 1537.71 68.84 o 6 2 1 950.27 1029.06 74.47 o 7 2 1 3026.62 2976.64 122.01 o 8 2 1 1003.72 894.82 101.15 o 9 2 1 3395.38 3191.98 195.88 o -9 3 1 258.73 278.01 74.52 o -8 3 1 6382.84 6353.02 225.35 o -7 3 1 4041.09 3873.33 200.18 o -6 3 1 285.51 245.39 45.87 o -5 3 1 2653.27 2564.46 85.05 o -4 3 1 11294.45 10704.34 330.73 o -3 3 1 3022.17 3074.32 89.25 o -2 3 1 9183.08 10097.82 140.65 o -1 3 1 11577.35 11391.65 170.70 o 0 3 1 234.89 276.97 26.63 o 1 3 1 891.20 938.32 30.46 o 2 3 1 12162.78 12199.62 146.12 o 3 3 1 8981.57 8855.65 121.64 o 4 3 1 3.54 13.16 10.97 o 5 3 1 3824.69 3942.85 96.11 o 6 3 1 336.72 299.97 46.70 o 7 3 1 635.30 626.45 66.52 o 8 3 1 203.13 206.31 62.91 o 9 3 1 574.07 557.43 93.11 o -9 4 1 2614.33 2844.09 188.18 o -8 4 1 6866.41 6465.30 284.17 o -7 4 1 4349.09 4518.58 217.97 o -6 4 1 110.31 83.28 35.01 o -5 4 1 2208.26 2458.61 127.46 o -4 4 1 5105.56 5083.92 109.43 o -3 4 1 20807.00 21086.98 234.57 o -2 4 1 10881.35 10885.38 148.25 o -1 4 1 100.44 103.61 31.57 o 0 4 1 24721.07 24644.87 409.29 o 1 4 1 46966.48 49311.61 698.98 o 2 4 1 11795.76 12045.42 191.46 o 3 4 1 6279.45 6351.23 157.05 o 4 4 1 8445.65 8878.55 133.60 o 5 4 1 19357.76 19980.49 295.93 o 6 4 1 14373.46 14381.66 264.30 o 7 4 1 2337.08 2051.16 137.40 o 8 4 1 75.21 138.33 55.73 o 9 4 1 3094.65 3127.82 301.13 o -9 5 1 1279.78 1154.66 126.06 o -8 5 1 566.49 513.63 106.16 o -7 5 1 300.61 214.60 70.43 o -6 5 1 20806.16 20590.19 496.72 o -5 5 1 4101.41 3831.98 104.26 o -4 5 1 3017.85 3007.71 94.46 o -3 5 1 2324.18 2447.94 105.27 o -2 5 1 54647.73 54606.45 612.61 o -1 5 1 8908.99 9304.09 163.07 o 0 5 1 45947.71 46765.68 821.49 o 1 5 1 152.93 123.86 37.91 o 2 5 1 16772.72 17384.10 278.74 o 3 5 1 3766.15 3711.84 91.62 o 4 5 1 47743.77 47977.92 526.98 o 5 5 1 1740.99 1706.79 98.51 o 6 5 1 7968.68 8096.50 225.35 o 7 5 1 3830.83 3593.26 157.56 o 8 5 1 14979.76 14992.10 763.06 o 9 5 1 200.46 54.16 80.89 o -9 6 1 68.89 44.50 60.74 o -8 6 1 20.96 22.28 56.86 o -7 6 1 8824.30 8546.89 312.40 o -6 6 1 6269.05 6024.34 310.90 o -5 6 1 4015.56 3850.76 131.97 o -4 6 1 14106.63 14634.81 588.54 o -3 6 1 6826.26 6711.74 101.66 o -2 6 1 47.78 100.23 19.49 o -1 6 1 608.71 718.89 46.84 o 0 6 1 4440.16 4943.13 232.54 o 1 6 1 4182.75 4074.59 124.96 o 2 6 1 7845.87 8309.32 142.45 o 3 6 1 3187.77 3171.08 68.59 o 4 6 1 1953.67 2045.84 57.21 o 5 6 1 13279.29 13576.99 239.60 o 6 6 1 772.14 650.60 109.26 o 7 6 1 2607.40 2483.60 153.70 o 8 6 1 7.08 15.39 49.45 o 9 6 1 4669.17 3831.28 271.60 o -9 7 1 1656.92 1893.07 291.37 o -8 7 1 9442.52 9218.56 351.98 o -7 7 1 3268.27 2997.98 208.55 o -6 7 1 754.98 813.31 111.87 o -5 7 1 844.48 791.65 73.23 o -4 7 1 1105.36 1085.10 101.83 o -3 7 1 1925.54 2106.21 69.67 o -2 7 1 863.03 1023.83 57.01 o -1 7 1 36646.80 37248.39 1195.58 o 0 7 1 1939.65 1969.78 89.37 o 1 7 1 403.47 623.28 60.77 o 2 7 1 6375.51 6620.80 171.47 o 3 7 1 678.60 726.70 59.10 o 4 7 1 1752.99 1937.27 57.49 o 5 7 1 2831.99 2826.01 132.24 o 6 7 1 6613.20 6276.62 186.08 o 7 7 1 432.77 470.15 73.68 o 8 7 1 240.21 199.19 63.07 o 9 7 1 3351.84 3701.81 581.36 o -9 8 1 2360.74 2482.44 182.71 o -8 8 1 2465.60 2559.08 209.80 o -7 8 1 5833.33 5667.13 254.67 o -6 8 1 1911.48 1801.14 118.28 o -5 8 1 4314.47 4029.48 145.20 o -4 8 1 13403.16 12889.46 576.31 o -3 8 1 1945.88 2066.60 71.82 o -2 8 1 350.81 464.08 45.28 o -1 8 1 54.45 94.20 45.50 o 0 8 1 960.15 891.70 78.36 o 1 8 1 209.80 255.77 40.99 o 2 8 1 11434.44 11021.75 218.06 o 3 8 1 55.82 86.06 22.38 o 4 8 1 5337.27 5563.10 160.17 o 5 8 1 4196.10 4349.75 192.35 o 6 8 1 15677.50 15388.46 417.05 o 7 8 1 3033.44 2971.68 171.90 o 8 8 1 241.98 158.24 76.30 o 9 8 1 1416.03 1461.91 275.52 o -9 9 1 272.24 368.13 86.19 o -8 9 1 283.17 192.10 118.80 o -7 9 1 1073.35 980.38 126.86 o -6 9 1 12346.43 12180.32 288.58 o -5 9 1 20988.33 21135.80 397.87 o -4 9 1 470.00 472.81 71.23 o -3 9 1 7240.62 7508.10 159.53 o -2 9 1 6574.73 6695.13 166.38 o -1 9 1 57645.61 56561.96 936.23 o 0 9 1 14195.08 14295.55 323.37 o 1 9 1 1659.97 1827.74 128.91 o 2 9 1 6794.61 6733.69 199.32 o 3 9 1 37147.94 38027.41 488.64 o 4 9 1 13332.82 13631.98 298.41 o 5 9 1 978.26 891.67 81.62 o 6 9 1 728.27 677.76 78.09 o 7 9 1 6702.99 6773.71 239.40 o 8 9 1 5436.45 5351.03 277.02 o 9 9 1 637.21 656.00 135.27 o -9 10 1 2501.72 2419.24 232.02 o -8 10 1 1179.61 1516.08 169.09 o -7 10 1 3964.94 4239.02 224.86 o -6 10 1 516.13 376.54 79.22 o -5 10 1 400.14 397.79 59.74 o -4 10 1 299.51 441.50 74.81 o -3 10 1 23560.94 23684.30 453.13 o -2 10 1 9070.33 8797.52 199.33 o -1 10 1 1011.98 969.58 87.09 o 0 10 1 2396.16 2133.34 110.81 o 1 10 1 49756.75 49185.39 848.84 o 2 10 1 502.18 552.02 68.25 o 3 10 1 44.98 43.41 22.38 o 4 10 1 270.25 212.71 64.43 o 5 10 1 21894.83 21728.77 411.97 o 6 10 1 1803.60 1860.34 125.83 o 7 10 1 2616.52 2628.92 210.90 o 8 10 1 926.38 759.02 130.44 o -8 11 1 189.25 193.75 87.52 o -7 11 1 6596.77 6029.54 482.78 o -6 11 1 1082.67 1036.32 103.67 o -5 11 1 9058.13 9050.58 245.99 o -4 11 1 231.98 180.98 66.97 o -3 11 1 8292.39 8070.78 209.42 o -2 11 1 1642.44 1674.15 108.07 o -1 11 1 276.54 255.93 131.44 o 0 11 1 6466.52 6112.83 358.93 o 1 11 1 213.27 179.18 47.37 o 2 11 1 2052.12 2114.23 123.87 o 3 11 1 5642.22 5479.22 158.17 o 4 11 1 4138.29 4194.29 205.33 o 5 11 1 8249.62 7909.00 255.60 o 6 11 1 77.55 68.63 48.17 o 7 11 1 695.70 533.43 108.98 o 8 11 1 1157.25 1012.05 323.54 o -8 12 1 65.77 32.80 73.22 o -7 12 1 5917.15 5562.35 269.44 o -6 12 1 2993.81 2950.30 158.40 o -5 12 1 3367.27 3412.83 150.44 o -4 12 1 2.10 20.45 33.07 o -3 12 1 20.22 20.22 23.75 o -2 12 1 13796.21 13794.48 346.87 o -1 12 1 1484.69 1554.77 121.54 o 0 12 1 12086.63 11963.51 318.14 o 1 12 1 89.13 67.89 36.40 o 2 12 1 2107.03 1896.57 135.93 o 3 12 1 6099.80 6211.96 177.78 o 4 12 1 3291.04 3271.74 138.87 o 5 12 1 735.22 810.97 88.89 o 6 12 1 164.16 117.86 50.21 o 7 12 1 2989.56 2880.98 226.80 o 8 12 1 214.67 128.70 84.90 o -8 13 1 1186.17 889.74 197.16 o -7 13 1 1043.89 1055.63 176.94 o -6 13 1 28.76 53.38 44.33 o -5 13 1 2182.99 2166.56 218.57 o -4 13 1 2977.55 3030.34 160.34 o -3 13 1 137.39 63.38 35.43 o -2 13 1 2.37 -7.58 28.60 o -1 13 1 36183.07 35338.56 692.79 o 0 13 1 22.00 9.86 35.21 o 1 13 1 341.35 315.88 62.48 o 2 13 1 17400.48 17442.36 421.40 o 3 13 1 16310.61 16304.50 331.25 o 4 13 1 379.06 446.95 81.98 o 5 13 1 1599.30 1565.15 122.59 o 6 13 1 785.88 713.22 207.27 o 7 13 1 7034.78 7265.08 323.37 o 8 13 1 32.89 23.51 76.30 o -7 14 1 3573.34 3213.48 246.57 o -6 14 1 3420.25 3541.59 318.82 o -5 14 1 722.16 622.03 92.99 o -4 14 1 25765.05 26345.96 630.90 o -3 14 1 2409.97 2581.73 153.37 o -2 14 1 14559.09 14619.01 381.24 o -1 14 1 925.46 859.90 101.46 o 0 14 1 23265.12 22681.32 516.53 o 1 14 1 2864.16 2898.68 303.32 o 2 14 1 20818.15 20408.69 481.59 o 3 14 1 908.40 1035.54 89.78 o 4 14 1 8442.21 8491.56 300.02 o 5 14 1 10477.11 10545.13 290.38 o 6 14 1 2464.12 2616.95 210.09 o 7 14 1 107.78 88.52 80.37 o -7 15 1 516.59 601.58 176.94 o -6 15 1 6033.51 6156.31 418.49 o -5 15 1 1460.22 1585.27 130.21 o -4 15 1 111.22 75.83 60.77 o -3 15 1 99.08 77.51 75.83 o -2 15 1 5292.02 5198.57 447.40 o -1 15 1 1694.32 1448.22 290.68 o 0 15 1 3813.07 3668.76 182.20 o 1 15 1 251.43 299.04 69.64 o 2 15 1 2877.80 2965.34 187.05 o 3 15 1 398.60 344.89 61.96 o 4 15 1 7109.78 7603.41 293.06 o 5 15 1 91.48 171.88 96.05 o 6 15 1 608.71 703.06 97.90 o 7 15 1 3941.76 4215.56 294.50 o -7 16 1 18.87 5.06 111.22 o -6 16 1 5124.18 5552.85 305.53 o -5 16 1 159.85 88.28 73.22 o -4 16 1 26.46 50.40 58.90 o -3 16 1 56.72 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