# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 8ftivi4_0m in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 258.78 _exptl_crystal_F_000 944.00 _reflns_d_resolution_high 0.7828 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.3323 _cell_length_b 12.5539 _cell_length_c 15.7126 _cell_angle_alpha 69.746 _cell_angle_beta 69.700 _cell_angle_gamma 75.787 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2774.81 1445.73 86.22 o 2 0 0 3336.98 3152.85 127.96 o 3 0 0 300.12 210.88 26.79 o 4 0 0 1087.07 1428.35 100.37 o 5 0 0 16430.17 16736.12 497.58 o 6 0 0 2758.97 2749.48 123.40 o 7 0 0 585.46 589.75 79.08 o 8 0 0 4826.35 4918.94 245.29 o 9 0 0 5.36 -5.34 37.40 o 10 0 0 3146.24 3302.99 208.12 o 11 0 0 1561.67 1829.53 170.14 o 12 0 0 2111.37 2080.73 303.89 o 13 0 0 4449.27 5476.22 331.42 o -13 1 0 18.46 79.80 101.89 o -12 1 0 3796.62 3901.26 259.36 o -11 1 0 3644.19 3876.42 346.65 o -10 1 0 315.42 348.51 96.90 o -9 1 0 3910.10 3877.68 221.94 o -8 1 0 261.89 180.44 55.38 o -7 1 0 5166.45 5178.65 283.23 o -6 1 0 4561.94 4270.42 204.67 o -5 1 0 48.08 30.56 17.95 o -4 1 0 19378.12 20203.63 508.23 o -3 1 0 437.03 404.72 26.45 o -2 1 0 10326.98 10239.00 227.80 o -1 1 0 25359.37 24955.34 527.39 o 0 1 0 77.10 1.44 32.42 o 1 1 0 18827.44 19740.68 466.13 o 2 1 0 11037.78 11507.65 278.41 o 3 1 0 1848.63 1963.39 65.80 o 4 1 0 3351.61 3203.97 102.66 o 5 1 0 81.61 96.48 22.24 o 6 1 0 7192.46 6969.54 288.24 o 7 1 0 10831.40 10917.10 429.86 o 8 1 0 48.85 95.91 44.43 o 9 1 0 9154.50 9157.44 399.07 o 10 1 0 610.45 757.12 109.15 o 11 1 0 2016.46 2250.89 506.61 o 12 1 0 2374.91 2582.76 210.78 o 13 1 0 302.55 319.02 101.05 o -13 2 0 2429.98 3022.56 347.72 o -12 2 0 1176.14 1378.04 230.86 o -11 2 0 1779.01 1705.70 171.63 o -10 2 0 1775.39 1370.16 239.77 o -9 2 0 50.64 3.15 39.78 o -8 2 0 5448.96 5647.61 277.22 o -7 2 0 4584.39 4078.42 360.18 o -6 2 0 3487.97 3670.88 153.88 o -5 2 0 12576.92 12939.93 401.00 o -4 2 0 189.57 193.32 26.17 o -3 2 0 9323.03 8637.90 387.14 o -2 2 0 5048.56 4949.54 109.35 o -1 2 0 1466.99 1364.84 35.11 o 0 2 0 10090.90 10107.73 268.57 o 1 2 0 2520.45 2442.79 62.92 o 2 2 0 16290.40 17614.32 369.24 o 3 2 0 7869.94 7935.13 201.97 o 4 2 0 12.67 13.47 14.25 o 5 2 0 13526.99 13331.03 483.88 o 6 2 0 1886.32 1698.84 88.17 o 7 2 0 6186.74 6158.45 223.62 o 8 2 0 10862.59 9936.06 460.13 o 9 2 0 10.51 42.24 39.85 o 10 2 0 2295.42 2496.46 171.36 o 11 2 0 1318.02 1215.08 661.59 o 12 2 0 557.17 678.99 121.43 o 13 2 0 3523.34 3652.09 258.22 o -12 3 0 3573.21 2937.05 328.48 o -11 3 0 2759.80 3084.55 322.06 o -10 3 0 630.87 757.59 117.55 o -9 3 0 2903.52 2899.75 190.45 o -8 3 0 2295.38 2391.12 160.44 o -7 3 0 2710.23 2671.99 226.58 o -6 3 0 7959.11 8246.29 348.42 o -5 3 0 727.69 917.51 84.64 o -4 3 0 16153.66 16088.73 577.63 o -3 3 0 6647.08 6505.30 211.78 o -2 3 0 4700.85 4804.54 98.90 o -1 3 0 13028.77 13288.36 259.54 o 0 3 0 1176.01 1363.51 58.21 o 1 3 0 35771.29 35832.48 1581.11 o 2 3 0 3233.19 2984.21 95.81 o 3 3 0 170.50 136.80 13.93 o 4 3 0 11582.67 11589.06 289.59 o 5 3 0 2071.19 1931.63 87.16 o 6 3 0 10041.58 10431.58 397.05 o 7 3 0 6226.44 6756.97 238.61 o 8 3 0 411.31 382.49 99.96 o 9 3 0 6883.72 6250.48 1147.53 o 10 3 0 443.04 432.36 82.59 o 11 3 0 1067.73 1247.21 137.30 o 12 3 0 1602.34 1642.70 165.74 o 13 3 0 40.66 69.10 73.10 o -12 4 0 1519.55 1111.55 219.46 o -11 4 0 1670.96 1237.67 215.90 o -10 4 0 3643.01 3319.68 310.66 o -9 4 0 51.25 18.66 41.78 o -8 4 0 2321.66 2467.00 171.53 o -7 4 0 2423.92 2527.30 158.95 o -6 4 0 1028.67 1071.08 95.09 o -5 4 0 11287.83 11475.52 365.76 o -4 4 0 293.31 172.74 32.36 o -3 4 0 15127.81 15746.81 393.10 o -2 4 0 14797.10 14490.50 296.45 o -1 4 0 703.65 714.50 27.69 o 0 4 0 11854.22 11728.25 386.30 o 1 4 0 1794.68 1576.12 111.87 o 2 4 0 19054.38 20535.79 657.18 o 3 4 0 27900.35 29361.44 784.09 o 4 4 0 151.57 172.55 16.11 o 5 4 0 3062.11 3184.41 118.32 o 6 4 0 6794.41 6942.07 279.65 o 7 4 0 2362.09 2475.69 115.20 o 8 4 0 9582.16 9739.00 393.45 o 9 4 0 1261.99 1393.45 121.11 o 10 4 0 1020.48 1074.75 117.47 o 11 4 0 2191.10 2386.09 180.56 o 12 4 0 2734.28 2747.88 209.38 o 13 4 0 2828.60 2925.65 342.01 o -12 5 0 952.24 1177.81 233.71 o -11 5 0 847.93 898.50 200.93 o -10 5 0 675.75 522.29 146.07 o -9 5 0 4852.09 4156.91 342.01 o -8 5 0 1742.15 1452.25 134.15 o -7 5 0 895.62 996.45 104.72 o -6 5 0 5748.78 5839.38 222.62 o -5 5 0 54.87 49.87 22.83 o -4 5 0 7159.38 6833.57 233.98 o -3 5 0 310.11 273.58 26.05 o -2 5 0 12048.07 12272.28 265.97 o -1 5 0 13776.85 13374.22 288.02 o 0 5 0 45.99 57.39 16.50 o 1 5 0 19758.75 19956.57 922.02 o 2 5 0 2810.45 2748.38 107.14 o 3 5 0 7277.73 7558.24 265.15 o 4 5 0 26432.21 27370.36 920.65 o 5 5 0 10883.63 12014.40 300.94 o 6 5 0 3858.54 3938.25 123.27 o 7 5 0 11053.18 11501.96 436.29 o 8 5 0 171.05 221.67 46.08 o 9 5 0 2997.52 2786.10 413.98 o 10 5 0 296.30 228.16 198.80 o 11 5 0 4399.79 4174.33 681.18 o 12 5 0 2562.96 2915.68 304.96 o 13 5 0 51.31 121.84 116.86 o -11 6 0 1066.57 1026.76 208.77 o -10 6 0 2827.48 2847.27 309.95 o -9 6 0 65.13 70.54 72.68 o -8 6 0 8915.36 9018.51 569.31 o -7 6 0 4625.89 4145.92 178.44 o -6 6 0 984.59 967.52 82.88 o -5 6 0 7744.17 7592.80 232.33 o -4 6 0 533.48 501.43 43.68 o -3 6 0 7456.36 7197.38 180.27 o -2 6 0 3196.25 3023.46 98.33 o -1 6 0 1529.45 1546.44 56.74 o 0 6 0 22234.24 22094.37 715.54 o 1 6 0 1645.16 1657.35 133.24 o 2 6 0 2788.37 2801.67 189.53 o 3 6 0 2089.93 1792.63 74.25 o 4 6 0 287.56 433.05 109.02 o 5 6 0 12981.85 13569.67 644.69 o 6 6 0 6980.36 7089.39 275.36 o 7 6 0 1042.90 1021.68 59.67 o 8 6 0 2869.82 2776.66 143.47 o 9 6 0 143.61 153.51 51.53 o 10 6 0 6785.65 7006.32 488.08 o 11 6 0 2343.41 2218.82 259.36 o 12 6 0 135.04 119.71 109.73 o 13 6 0 1635.12 1762.09 275.75 o -10 7 0 95.45 168.13 75.17 o -9 7 0 4057.79 3882.24 229.76 o -8 7 0 1612.14 1631.44 143.80 o -7 7 0 3498.93 3582.13 384.77 o -6 7 0 1469.04 1282.34 114.76 o -5 7 0 405.28 376.86 45.24 o -4 7 0 2918.61 2946.72 108.52 o -3 7 0 3671.29 3683.82 216.14 o -2 7 0 3282.39 3304.53 107.70 o -1 7 0 12746.06 12987.87 325.05 o 0 7 0 1738.17 2066.68 63.59 o 1 7 0 7504.55 6955.02 384.05 o 2 7 0 6339.31 6580.22 368.38 o 3 7 0 4660.84 5091.75 250.10 o 4 7 0 7435.85 6760.28 1026.40 o 5 7 0 334.00 320.03 43.32 o 6 7 0 3444.58 3618.15 146.60 o 7 7 0 8121.38 7926.02 308.01 o 8 7 0 212.07 245.82 83.37 o 9 7 0 8027.31 6441.28 442.48 o 10 7 0 415.97 485.23 128.26 o 11 7 0 2029.68 1933.81 242.26 o 12 7 0 3428.83 3303.29 328.48 o -10 8 0 1988.24 1980.14 178.45 o -9 8 0 335.41 379.82 89.34 o -8 8 0 3040.64 3007.64 194.65 o -7 8 0 2478.66 2442.72 169.64 o -6 8 0 358.16 501.93 82.61 o -5 8 0 5965.86 5827.54 265.24 o -4 8 0 404.34 470.42 56.81 o -3 8 0 3752.74 3856.88 131.38 o -2 8 0 3476.60 2520.90 381.23 o -1 8 0 1221.97 1318.53 56.78 o 0 8 0 10001.33 9762.09 247.35 o 1 8 0 3080.22 2875.06 210.20 o 2 8 0 3056.64 2711.18 202.36 o 3 8 0 7313.94 8077.80 289.81 o 4 8 0 2.75 10.15 18.17 o 5 8 0 6963.93 6415.24 1017.49 o 6 8 0 3393.65 3381.67 230.86 o 7 8 0 305.55 292.14 77.67 o 8 8 0 6971.73 7264.25 460.30 o 9 8 0 276.68 384.05 111.15 o 10 8 0 2999.47 3366.71 294.28 o 11 8 0 1342.46 1817.67 231.57 o 12 8 0 54.90 6.41 99.75 o -9 9 0 1176.94 1293.79 147.92 o -8 9 0 2067.28 2224.27 175.85 o -7 9 0 2245.29 1934.16 158.19 o -6 9 0 9102.27 8942.01 381.39 o -5 9 0 64.12 31.98 60.57 o -4 9 0 4642.59 4493.55 220.27 o -3 9 0 721.07 712.36 64.84 o -2 9 0 3028.75 2983.44 106.53 o -1 9 0 5998.10 5957.64 170.19 o 0 9 0 4.08 3.12 12.56 o 1 9 0 6375.25 6354.47 238.11 o 2 9 0 3348.82 3065.31 233.00 o 3 9 0 142.50 -19.24 44.89 o 4 9 0 9815.06 9962.02 347.07 o 5 9 0 497.07 442.37 46.82 o 6 9 0 6498.45 6397.82 377.64 o 7 9 0 7181.98 7035.53 426.81 o 8 9 0 3.10 -46.31 47.74 o 9 9 0 2575.46 3009.02 263.64 o 10 9 0 773.67 888.53 159.61 o 11 9 0 1262.33 1135.06 189.53 o -8 10 0 1191.64 1151.84 138.22 o -7 10 0 1860.58 1941.40 163.40 o -6 10 0 442.08 208.15 64.17 o -5 10 0 6705.09 6246.11 293.21 o -4 10 0 811.29 805.14 95.35 o -3 10 0 2814.10 2544.26 150.96 o -2 10 0 3016.43 3098.04 135.37 o -1 10 0 227.68 211.14 29.38 o 0 10 0 2400.81 2414.07 72.16 o 1 10 0 780.80 772.08 107.95 o 2 10 0 1566.68 1827.64 184.55 o 3 10 0 12950.01 14170.82 743.17 o 4 10 0 66.35 54.15 27.08 o 5 10 0 6041.56 6261.72 351.28 o 6 10 0 3686.67 3695.19 245.11 o 7 10 0 2855.91 2751.08 213.05 o 8 10 0 8879.70 8877.42 537.25 o 9 10 0 373.74 225.87 92.63 o 10 10 0 1279.30 1382.31 191.67 o 11 10 0 1176.12 1325.31 206.63 o -7 11 0 1904.84 1912.54 169.02 o -6 11 0 2384.46 2280.70 173.73 o -5 11 0 214.98 202.36 82.30 o -4 11 0 4088.77 3946.85 213.40 o -3 11 0 2719.30 2677.70 161.23 o -2 11 0 129.03 211.25 50.22 o -1 11 0 6763.68 6742.14 228.27 o 0 11 0 471.09 467.41 42.27 o 1 11 0 3157.65 3569.46 226.58 o 2 11 0 2679.47 2506.68 227.30 o 3 11 0 886.73 921.30 150.34 o 5 11 0 105.99 153.19 44.18 o 6 11 0 1923.17 1920.27 155.33 o 7 11 0 1383.24 1559.73 151.06 o 8 11 0 35.62 30.64 59.85 o 9 11 0 3687.71 3784.25 303.54 o 10 11 0 680.94 513.02 131.11 o -6 12 0 585.42 689.93 109.54 o -5 12 0 2091.93 2263.66 169.91 o -4 12 0 607.70 622.47 94.96 o -3 12 0 1052.21 1023.13 105.04 o -2 12 0 3943.91 3812.32 269.69 o -1 12 0 111.39 94.00 39.01 o 0 12 0 2039.67 2223.83 99.51 o 1 12 0 536.41 590.97 62.84 o 2 12 0 1617.44 1922.41 213.76 o 3 12 0 5196.86 5745.85 399.02 o 5 12 0 3672.99 3801.35 229.43 o 6 12 0 1215.67 1232.68 118.99 o 7 12 0 26.03 41.33 54.86 o 8 12 0 3061.91 3489.26 272.90 o 9 12 0 206.71 244.40 101.89 o -5 13 0 0.38 -0.65 53.64 o -4 13 0 2039.91 2188.94 163.97 o -3 13 0 1842.33 1688.23 136.93 o -2 13 0 226.35 177.13 53.84 o -1 13 0 3402.41 3458.78 179.79 o 0 13 0 13.87 60.57 73.39 o 1 13 0 3049.81 3049.63 275.75 o 2 13 0 2734.74 2786.71 270.05 o 3 13 0 70.18 96.90 79.80 o 5 13 0 693.32 705.41 76.24 o 6 13 0 2403.67 2455.38 180.98 o 7 13 0 2763.64 2685.53 212.33 o 8 13 0 236.32 153.91 81.94 o -3 14 0 668.14 874.75 107.16 o -2 14 0 2683.97 2751.23 237.99 o -1 14 0 275.54 128.26 100.47 o 0 14 0 3238.55 3762.16 327.76 o 1 14 0 1586.92 1673.02 222.31 o 2 14 0 1534.87 1807.69 228.72 o 6 14 0 2304.30 2571.52 187.40 o 1 15 0 1483.55 1545.48 231.57 o 2 15 0 1326.28 1637.40 233.00 o -5 -14 1 76.35 79.09 50.59 o -2 -14 1 265.32 127.54 99.75 o -1 -14 1 4626.90 5302.66 403.29 o 0 -14 1 762.74 730.34 161.74 o 1 -14 1 1241.95 1531.23 219.46 o 2 -14 1 1535.66 1489.90 219.46 o -7 -13 1 2201.54 2191.03 191.67 o -6 -13 1 429.61 406.14 84.08 o -5 -13 1 3314.33 3559.09 225.87 o -2 -13 1 3702.79 3903.96 324.91 o -1 -13 1 0.70 58.43 81.23 o 0 -13 1 2087.92 2136.88 240.12 o 1 -13 1 464.44 452.51 68.06 o 2 -13 1 1244.78 1220.40 146.43 o 3 -13 1 3007.35 3068.82 183.36 o 4 -13 1 3.44 -49.17 48.80 o -9 -12 1 2100.68 2191.03 231.57 o -8 -12 1 361.49 371.23 102.60 o -7 -12 1 1962.65 2059.21 182.41 o -6 -12 1 1475.26 1392.29 135.38 o -5 -12 1 428.95 356.27 66.27 o -4 -12 1 3825.23 3844.78 217.68 o -2 -12 1 24.63 101.89 74.10 o -1 -12 1 3411.03 3492.89 301.04 o 0 -12 1 938.42 951.34 77.99 o 1 -12 1 3197.64 3300.07 257.58 o 2 -12 1 3014.58 2974.10 167.77 o 3 -12 1 342.08 221.14 60.94 o 4 -12 1 2913.62 2891.82 240.48 o 5 -12 1 781.89 1002.13 121.40 o 6 -12 1 379.48 387.68 112.94 o -10 -11 1 1918.40 2000.79 237.27 o -9 -11 1 28.15 52.73 78.38 o -8 -11 1 1710.91 2030.00 196.66 o -7 -11 1 2929.12 2987.64 232.29 o -6 -11 1 43.51 16.39 49.16 o -5 -11 1 3335.85 3540.47 159.21 o -4 -11 1 1946.60 1989.94 94.47 o -2 -11 1 6537.58 6557.42 416.83 o -1 -11 1 11.70 18.15 26.99 o 0 -11 1 3428.84 3478.31 175.90 o 1 -11 1 2069.81 2193.51 103.66 o 2 -11 1 1700.22 1728.62 120.77 o 3 -11 1 2383.94 2438.91 150.66 o 4 -11 1 4.59 13.96 41.77 o 5 -11 1 2020.30 2148.48 256.51 o 6 -11 1 2766.34 2991.80 196.16 o 7 -11 1 89.14 10.78 56.28 o -10 -10 1 0.26 15.68 76.95 o -9 -10 1 2359.06 2449.68 236.56 o -8 -10 1 1401.87 1910.30 187.40 o -7 -10 1 855.52 874.28 121.13 o -6 -10 1 5823.01 6171.23 372.65 o -5 -10 1 65.19 77.39 29.45 o -4 -10 1 5386.00 4987.75 232.64 o -2 -10 1 1084.79 1013.93 142.51 o -1 -10 1 4877.25 4786.36 150.62 o 0 -10 1 396.83 386.63 37.70 o 1 -10 1 2496.40 2435.47 238.32 o 2 -10 1 2941.86 2897.29 296.56 o 3 -10 1 2.43 0.33 31.37 o 4 -10 1 5176.29 5247.24 250.79 o 5 -10 1 1351.73 1399.66 157.47 o 6 -10 1 951.14 956.11 162.10 o 7 -10 1 2385.37 2648.16 254.37 o 8 -10 1 1.08 52.51 58.42 o -11 -9 1 52.60 42.04 86.22 o -10 -9 1 1980.27 2281.52 250.81 o -9 -9 1 1406.01 1546.90 189.53 o -8 -9 1 3338.05 3261.97 261.50 o -7 -9 1 5431.75 4999.83 333.46 o -6 -9 1 28.31 23.22 30.98 o -5 -9 1 4797.59 4775.30 202.53 o -4 -9 1 2901.00 2961.71 134.31 o -3 -9 1 5547.20 5960.32 289.29 o -2 -9 1 3169.69 3210.67 241.55 o -1 -9 1 2.05 1.77 12.07 o 0 -9 1 4168.53 3962.16 160.44 o 1 -9 1 2630.78 2568.61 90.87 o 2 -9 1 782.32 891.59 65.49 o 3 -9 1 6713.69 7087.20 244.40 o 4 -9 1 958.66 968.79 224.09 o 5 -9 1 2335.11 2477.67 160.22 o 6 -9 1 4388.73 4447.01 235.13 o 7 -9 1 109.64 58.27 113.29 o 8 -9 1 3080.32 3325.18 210.96 o 9 -9 1 29.93 36.09 60.96 o -12 -8 1 1016.78 1153.59 212.33 o -11 -8 1 1032.48 1295.38 210.20 o -10 -8 1 406.90 379.07 123.98 o -9 -8 1 3864.51 3846.96 310.66 o -8 -8 1 2303.57 2238.77 208.06 o -7 -8 1 508.11 495.21 96.90 o -6 -8 1 6960.46 7272.53 301.04 o -5 -8 1 1616.12 1606.41 75.66 o -4 -8 1 6234.58 6441.66 240.02 o -3 -8 1 2356.37 2276.73 91.95 o -2 -8 1 15.39 17.10 43.46 o -1 -8 1 10385.79 10649.44 296.35 o 0 -8 1 1128.98 1085.08 38.97 o 1 -8 1 3627.78 3297.35 176.17 o 2 -8 1 8861.56 9066.31 417.19 o 3 -8 1 360.95 397.68 49.36 o 4 -8 1 4458.56 4035.80 308.68 o 5 -8 1 688.97 592.95 92.63 o 6 -8 1 373.59 282.87 69.47 o 7 -8 1 6556.80 6969.68 320.80 o 8 -8 1 15.06 93.15 63.06 o 9 -8 1 6524.91 6019.04 332.75 o 10 -8 1 876.41 866.90 124.84 o -12 -7 1 1154.94 1118.67 210.20 o -11 -7 1 93.14 84.79 96.19 o -10 -7 1 3137.37 2220.25 247.25 o -9 -7 1 816.35 818.70 145.36 o -8 -7 1 4631.64 4317.94 317.79 o -7 -7 1 1160.67 1149.86 209.84 o -6 -7 1 611.44 574.73 39.98 o -5 -7 1 7371.85 7702.53 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