# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 11 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 313.03 _exptl_crystal_F_000 916.00 _reflns_d_resolution_high 0.8407 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.7132 _cell_length_b 12.7143 _cell_length_c 14.8822 _cell_angle_alpha 65.790 _cell_angle_beta 88.276 _cell_angle_gamma 70.437 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9651.44 9854.87 73.05 o 3 0 0 563.62 569.07 23.16 o 4 0 0 3472.22 3377.10 44.71 o 5 0 0 7044.80 6982.53 121.28 o 6 0 0 6698.96 6599.76 66.23 o 7 0 0 4064.30 4156.79 54.45 o 8 0 0 413.55 389.61 19.79 o 9 0 0 319.31 257.20 29.75 o 10 0 0 481.11 452.86 39.05 o 11 0 0 1220.29 1348.22 63.86 o 12 0 0 687.28 761.44 84.09 o 13 0 0 515.94 548.05 80.68 o -12 1 0 451.07 528.08 67.00 o -11 1 0 44.31 36.09 20.09 o -10 1 0 271.59 212.22 32.54 o -9 1 0 934.49 994.36 51.12 o -8 1 0 1742.53 1773.53 63.86 o -7 1 0 3604.81 3495.61 49.11 o -6 1 0 2934.45 3008.54 50.84 o -5 1 0 1727.23 1985.22 46.66 o -4 1 0 2731.37 2858.40 41.36 o -3 1 0 13383.25 13539.20 104.27 o -2 1 0 5732.25 5954.67 72.56 o -1 1 0 34292.14 34760.83 364.33 o 2 1 0 5371.19 5493.93 48.42 o 3 1 0 5906.80 5798.57 50.90 o 4 1 0 7049.20 7157.64 59.64 o 5 1 0 8425.64 8591.00 72.63 o 6 1 0 5021.37 5296.92 70.62 o 7 1 0 997.64 991.31 26.42 o 8 1 0 1404.77 1425.62 37.68 o 9 1 0 1818.14 1896.65 50.21 o 10 1 0 1720.17 1787.97 50.84 o 11 1 0 1999.27 2059.70 116.06 o 12 1 0 232.60 148.34 45.20 o 13 1 0 6.92 15.13 32.17 o -12 2 0 14.16 -23.20 18.16 o -11 2 0 150.82 154.45 31.65 o -10 2 0 1131.89 1059.69 59.70 o -9 2 0 2338.20 2385.04 82.23 o -8 2 0 2278.88 2281.96 100.48 o -7 2 0 1723.44 1655.17 60.57 o -6 2 0 202.71 200.22 24.51 o -5 2 0 2389.65 2339.89 105.54 o -4 2 0 18758.61 19057.25 163.51 o -3 2 0 13713.20 13431.39 106.53 o -2 2 0 9109.08 9114.39 105.32 o -1 2 0 89.26 99.60 10.37 o 0 2 0 2525.44 2286.65 37.18 o 1 2 0 8178.87 8028.37 78.83 o 2 2 0 1706.87 1665.39 25.84 o 3 2 0 2467.26 2452.26 35.49 o 4 2 0 8497.81 8374.79 65.53 o 5 2 0 422.25 408.46 20.48 o 6 2 0 1885.23 1898.88 32.97 o 7 2 0 2501.03 2473.81 41.10 o 8 2 0 4103.57 4029.04 80.19 o 9 2 0 1635.84 1676.00 39.12 o 10 2 0 3438.75 3310.23 193.64 o 11 2 0 1698.63 1647.13 63.76 o 12 2 0 239.64 88.60 40.09 o 13 2 0 266.64 327.05 64.45 o -11 3 0 880.50 846.20 62.52 o -10 3 0 1137.33 1072.88 62.92 o -9 3 0 1468.73 1295.94 64.12 o -8 3 0 1065.11 1039.88 77.73 o -7 3 0 63.56 68.12 18.46 o -6 3 0 2242.15 2234.55 70.01 o -5 3 0 7308.59 7296.01 189.93 o -4 3 0 4549.83 3996.69 50.61 o -3 3 0 10902.04 11142.74 126.06 o -2 3 0 3177.51 3339.24 83.34 o -1 3 0 2603.87 2635.96 38.64 o 0 3 0 2320.41 2339.27 31.92 o 1 3 0 3270.33 3162.16 37.36 o 2 3 0 115.52 156.04 24.46 o 3 3 0 7776.01 7834.22 76.22 o 4 3 0 29.04 31.29 7.52 o 5 3 0 2986.79 2809.06 35.49 o 6 3 0 3609.65 3568.35 47.80 o 7 3 0 2639.88 2420.51 39.95 o 8 3 0 1916.86 1859.66 37.79 o 9 3 0 277.87 284.99 28.46 o 10 3 0 75.15 77.47 20.02 o 11 3 0 276.35 270.10 32.01 o 12 3 0 383.33 518.34 48.61 o 13 3 0 1095.09 1157.94 101.63 o -11 4 0 550.55 673.84 65.25 o -10 4 0 417.70 420.33 58.28 o -9 4 0 276.95 207.99 35.58 o -8 4 0 1579.64 1490.12 103.64 o -7 4 0 6773.24 6725.22 204.57 o -6 4 0 4809.68 4967.48 110.73 o -5 4 0 3589.23 3561.11 87.22 o -4 4 0 2094.20 2082.73 62.73 o -3 4 0 1211.15 1301.05 26.17 o -2 4 0 570.31 687.34 20.01 o -1 4 0 4778.55 4854.60 55.70 o 0 4 0 10174.16 10463.18 91.47 o 1 4 0 7955.54 7609.70 72.41 o 2 4 0 3508.13 3566.25 50.49 o 3 4 0 2332.84 2711.45 119.12 o 4 4 0 1936.23 1796.72 45.77 o 5 4 0 7308.40 7071.24 83.94 o 6 4 0 10295.69 10144.91 110.13 o 7 4 0 3394.45 3498.31 71.29 o 8 4 0 58.74 79.65 17.68 o 9 4 0 52.94 73.68 23.60 o 10 4 0 560.84 516.57 38.64 o 11 4 0 1112.39 1133.49 55.40 o 12 4 0 1754.14 1727.10 70.61 o 13 4 0 287.36 299.86 38.54 o -10 5 0 130.80 106.52 37.69 o -9 5 0 798.15 693.27 56.77 o -8 5 0 3210.06 3296.85 103.90 o -7 5 0 1685.28 1798.96 74.02 o -6 5 0 967.99 968.03 75.37 o -5 5 0 1.83 -13.46 8.97 o -4 5 0 657.55 689.02 40.99 o -3 5 0 2746.82 2579.69 141.07 o -2 5 0 6076.51 6021.85 85.38 o -1 5 0 8276.76 8860.70 88.78 o 0 5 0 3814.32 3751.46 52.24 o 1 5 0 500.14 549.46 35.62 o 2 5 0 640.51 625.45 20.10 o 3 5 0 560.38 523.18 18.50 o 4 5 0 7727.95 7559.08 107.63 o 5 5 0 4904.34 4888.22 87.52 o 6 5 0 2291.88 2296.75 61.51 o 7 5 0 24.42 14.23 11.74 o 8 5 0 118.93 94.26 24.71 o 9 5 0 2786.27 2565.73 75.10 o 10 5 0 1358.99 1439.38 103.24 o 11 5 0 1684.18 1775.86 69.73 o 12 5 0 521.08 536.31 45.04 o 13 5 0 68.21 62.84 25.17 o -9 6 0 1052.55 1083.60 71.72 o -8 6 0 449.77 478.84 48.66 o -7 6 0 312.44 333.20 40.32 o -6 6 0 104.67 102.65 31.32 o -5 6 0 1785.29 1711.23 68.63 o -4 6 0 2745.83 2779.90 82.67 o -3 6 0 4352.08 4454.86 268.86 o -2 6 0 1662.75 1706.55 58.47 o -1 6 0 7.34 2.22 8.15 o 0 6 0 458.07 505.37 26.16 o 1 6 0 7085.51 6999.68 80.97 o 2 6 0 11100.90 11323.39 107.81 o 3 6 0 6796.87 6918.15 76.86 o 4 6 0 4469.08 4500.65 106.64 o 5 6 0 152.95 174.90 20.98 o 6 6 0 35.99 24.98 17.24 o 7 6 0 2374.13 2352.98 68.07 o 8 6 0 1669.00 1652.35 108.30 o 9 6 0 652.02 584.67 63.90 o 10 6 0 1334.94 1351.90 58.93 o 11 6 0 92.91 90.99 23.42 o 12 6 0 394.92 365.82 40.02 o 13 6 0 784.85 879.81 59.04 o -8 7 0 14.06 43.15 25.67 o -7 7 0 54.00 30.54 25.31 o -6 7 0 602.72 625.12 64.05 o -5 7 0 1983.37 1872.13 75.97 o -4 7 0 1808.45 1836.99 72.25 o -3 7 0 399.96 400.74 37.18 o -2 7 0 64.92 77.22 20.09 o -1 7 0 1376.28 1359.32 53.74 o 0 7 0 2158.23 2221.82 46.54 o 1 7 0 4844.09 4982.23 71.62 o 2 7 0 7927.81 7929.39 92.24 o 3 7 0 3433.30 3520.66 57.74 o 4 7 0 72.23 60.04 10.31 o 5 7 0 73.71 52.87 15.50 o 6 7 0 2683.46 2602.78 184.47 o 7 7 0 2494.03 2398.24 114.11 o 8 7 0 2147.75 2036.55 68.17 o 9 7 0 1360.74 1419.90 59.99 o 10 7 0 7.36 10.36 14.27 o 11 7 0 907.14 938.47 55.52 o 12 7 0 1159.67 1258.23 164.38 o 13 7 0 580.50 594.03 53.25 o -7 8 0 837.62 856.59 66.90 o -6 8 0 1161.82 1259.45 108.05 o -5 8 0 2017.75 1921.32 81.52 o -4 8 0 533.78 506.90 45.83 o -3 8 0 360.43 354.55 38.50 o -2 8 0 3961.13 3881.44 100.58 o -1 8 0 2080.00 2108.58 70.75 o 0 8 0 2658.21 2842.65 79.48 o 1 8 0 1042.33 1026.42 34.79 o 2 8 0 881.76 890.92 84.27 o 3 8 0 41.48 34.22 15.68 o 4 8 0 776.13 704.15 38.34 o 5 8 0 7061.54 7203.31 125.95 o 6 8 0 2860.23 2774.40 77.80 o 7 8 0 1272.52 1296.51 95.97 o 8 8 0 117.69 104.17 20.54 o 9 8 0 445.49 378.77 46.21 o 10 8 0 1018.70 1060.76 167.88 o 11 8 0 1046.77 1135.01 61.56 o 12 8 0 1239.15 1344.36 162.47 o 13 8 0 169.54 191.01 35.89 o -6 9 0 426.58 404.71 51.43 o -5 9 0 221.88 179.64 36.90 o -4 9 0 144.78 186.37 35.48 o -3 9 0 1948.73 1968.70 79.41 o -2 9 0 2669.86 2735.12 90.84 o -1 9 0 5611.43 5645.07 248.62 o 0 9 0 87.17 112.83 24.05 o 1 9 0 58.69 54.46 19.30 o 2 9 0 817.43 789.47 32.79 o 3 9 0 2592.60 2510.33 72.69 o 4 9 0 5197.39 4967.01 105.13 o 5 9 0 2835.70 2692.45 78.20 o 6 9 0 1142.92 1182.26 53.33 o 7 9 0 7.64 23.83 13.06 o 8 9 0 1249.23 1150.06 55.01 o 9 9 0 819.75 819.23 49.98 o 10 9 0 1217.67 1210.88 94.62 o 11 9 0 805.78 845.63 57.80 o 12 9 0 91.49 42.92 37.89 o 13 9 0 0.53 -1.51 24.46 o -5 10 0 414.28 359.62 49.79 o -4 10 0 1570.64 1746.90 83.65 o -3 10 0 1193.74 1164.51 67.93 o -2 10 0 882.20 805.12 57.04 o -1 10 0 32.56 47.16 33.18 o 0 10 0 102.61 58.93 30.52 o 1 10 0 1926.69 1879.85 103.24 o 2 10 0 2246.51 2380.04 77.42 o 3 10 0 2994.31 3058.17 85.23 o 4 10 0 1117.03 1158.12 53.86 o 5 10 0 93.82 59.94 28.01 o 6 10 0 6.38 -10.13 10.78 o 7 10 0 1443.41 1480.15 102.03 o 8 10 0 2619.27 2712.01 88.86 o 9 10 0 1669.11 1722.57 72.77 o 10 10 0 583.51 491.64 47.96 o 11 10 0 7.20 10.26 18.35 o 12 10 0 158.95 114.44 31.33 o -3 11 0 373.76 385.25 74.92 o -2 11 0 0.17 -30.13 24.36 o -1 11 0 197.54 184.67 36.03 o 0 11 0 951.62 954.04 79.78 o 1 11 0 2845.77 2991.03 151.14 o 2 11 0 2869.08 2970.08 148.64 o 3 11 0 399.88 339.27 62.74 o 4 11 0 240.39 211.79 45.10 o 5 11 0 353.19 459.50 39.99 o 6 11 0 331.24 304.31 35.27 o 7 11 0 730.41 739.07 94.01 o 8 11 0 685.29 691.50 51.16 o 9 11 0 386.73 441.04 130.65 o 10 11 0 206.25 190.12 32.15 o 11 11 0 814.08 803.39 59.21 o -2 12 0 825.47 858.45 67.45 o -1 12 0 1152.82 1301.47 75.40 o 0 12 0 1238.81 1484.79 119.67 o 1 12 0 762.93 725.46 90.01 o 2 12 0 29.09 2.31 32.17 o 3 12 0 256.70 136.41 51.82 o 4 12 0 955.68 963.40 96.42 o 5 12 0 976.16 1002.39 57.77 o 6 12 0 468.64 527.91 45.73 o 7 12 0 284.68 311.93 38.89 o 8 12 0 3.83 4.94 16.54 o 9 12 0 533.04 554.33 50.85 o 10 12 0 599.32 577.38 52.27 o 1 13 0 34.13 46.00 44.80 o 2 13 0 290.98 359.92 73.97 o 3 13 0 846.62 900.96 100.63 o 4 13 0 1131.04 1038.27 105.84 o 5 13 0 973.42 1052.60 106.94 o 6 13 0 153.77 201.44 40.39 o 7 13 0 125.71 144.96 33.03 o 8 13 0 819.93 814.90 59.99 o -7 -13 1 136.88 131.97 30.97 o -6 -13 1 120.04 151.49 33.87 o -5 -13 1 249.02 219.30 61.14 o -4 -13 1 541.89 601.17 87.60 o -3 -13 1 662.09 885.22 102.83 o -2 -13 1 378.85 323.04 73.27 o -10 -12 1 954.04 979.02 66.37 o -9 -12 1 1101.51 1050.55 69.01 o -8 -12 1 434.23 402.87 45.36 o -7 -12 1 80.64 89.44 24.59 o -6 -12 1 224.90 189.41 35.28 o -5 -12 1 1294.17 1352.19 66.70 o -4 -12 1 1594.96 1628.82 115.76 o -3 -12 1 506.05 467.27 74.77 o -2 -12 1 19.13 -24.16 35.48 o -1 -12 1 74.82 55.93 42.60 o 0 -12 1 623.14 554.97 85.70 o 1 -12 1 1094.98 1130.21 73.98 o -11 -11 1 930.76 940.56 64.60 o -10 -11 1 80.42 47.06 22.00 o -9 -11 1 0.77 -11.64 12.77 o -8 -11 1 447.55 395.12 42.57 o -7 -11 1 995.31 1050.73 60.75 o -6 -11 1 996.23 1102.05 84.54 o -5 -11 1 1455.17 1482.65 66.38 o -4 -11 1 752.90 712.21 47.10 o -3 -11 1 133.41 80.98 38.79 o -2 -11 1 170.95 195.15 53.62 o -1 -11 1 1248.55 1356.60 108.25 o 0 -11 1 1468.97 1417.56 107.70 o 1 -11 1 1050.33 1182.28 69.61 o 2 -11 1 468.15 525.18 62.24 o 3 -11 1 71.49 91.62 31.26 o -12 -10 1 470.52 415.86 48.60 o -11 -10 1 38.51 24.45 18.40 o -10 -10 1 81.31 52.58 22.08 o -9 -10 1 1103.59 967.31 57.28 o -8 -10 1 2800.20 2966.66 95.12 o -7 -10 1 1745.73 1877.82 138.42 o -6 -10 1 1023.15 1011.57 75.42 o -5 -10 1 258.15 277.12 32.49 o -4 -10 1 141.84 93.58 21.94 o -3 -10 1 2314.19 2353.73 76.60 o -2 -10 1 6052.72 6025.25 201.66 o -1 -10 1 3484.35 3803.15 102.44 o 0 -10 1 640.52 695.67 126.84 o 1 -10 1 44.12 41.50 39.79 o 2 -10 1 186.11 241.78 38.48 o 3 -10 1 639.31 646.95 59.13 o 4 -10 1 1180.79 1303.29 89.15 o -12 -9 1 0.52 13.57 19.67 o -11 -9 1 212.07 224.12 35.73 o -10 -9 1 652.14 609.52 48.55 o -9 -9 1 783.94 858.32 52.32 o -8 -9 1 1755.45 1658.84 106.49 o -7 -9 1 500.20 497.38 56.43 o -6 -9 1 199.19 211.69 78.43 o -5 -9 1 1981.90 1924.51 67.47 o -4 -9 1 4502.98 4627.31 104.28 o -3 -9 1 4885.23 4847.76 104.56 o -2 -9 1 1193.67 1148.94 39.80 o -1 -9 1 249.44 268.90 32.01 o 0 -9 1 410.49 379.10 52.27 o 1 -9 1 3243.32 3329.56 97.25 o 2 -9 1 1410.69 1490.46 87.35 o 3 -9 1 2919.72 2946.38 99.27 o 4 -9 1 946.46 844.07 60.46 o 5 -9 1 111.94 141.05 35.07 o 6 -9 1 58.11 31.65 28.96 o -13 -8 1 77.04 18.65 21.01 o -12 -8 1 462.68 378.53 43.95 o -11 -8 1 1109.02 1284.26 80.23 o -10 -8 1 486.32 549.84 46.00 o -9 -8 1 167.03 183.08 28.97 o -8 -8 1 97.20 49.77 16.23 o -7 -8 1 587.67 622.55 45.15 o -6 -8 1 2490.19 2424.89 101.33 o -5 -8 1 2953.65 2832.21 79.03 o -4 -8 1 4029.40 3941.17 91.16 o -3 -8 1 732.56 754.05 29.99 o -2 -8 1 53.70 67.15 13.79 o -1 -8 1 1289.63 1259.19 58.70 o 0 -8 1 5411.14 5387.98 153.30 o 1 -8 1 3113.58 3125.14 88.41 o 2 -8 1 7648.67 7566.63 146.94 o 3 -8 1 506.71 483.09 44.05 o 4 -8 1 0.99 -7.70 17.21 o 5 -8 1 735.05 760.24 58.32 o 6 -8 1 793.38 838.64 63.81 o 7 -8 1 1117.09 1230.03 77.35 o -13 -7 1 661.50 649.28 54.98 o -12 -7 1 1079.92 1138.54 62.75 o -11 -7 1 1424.99 1355.75 64.40 o -10 -7 1 978.65 973.25 53.05 o -9 -7 1 40.39 8.06 13.58 o -8 -7 1 1724.48 1633.15 62.60 o -7 -7 1 4136.01 4052.77 94.66 o -6 -7 1 2455.69 2427.37 70.81 o -5 -7 1 3167.99 3152.98 78.60 o -4 -7 1 1258.69 1305.53 84.34 o -3 -7 1 2511.62 2537.19 48.66 o -2 -7 1 2671.80 2801.91 53.38 o -1 -7 1 6516.59 6514.78 86.06 o 0 -7 1 7939.88 8054.81 98.57 o 1 -7 1 4147.10 4205.48 96.14 o 2 -7 1 283.01 312.01 33.33 o 3 -7 1 260.39 267.43 47.16 o 4 -7 1 2066.23 2120.57 78.55 o 5 -7 1 1807.52 1802.44 158.41 o 6 -7 1 623.55 624.55 60.44 o 7 -7 1 564.73 578.98 54.82 o 8 -7 1 37.32 18.03 22.55 o -13 -6 1 1790.83 1921.46 82.04 o -12 -6 1 403.28 378.53 45.45 o -11 -6 1 168.04 73.08 38.74 o -10 -6 1 979.71 1006.51 58.63 o -9 -6 1 5297.70 5336.70 115.76 o -8 -6 1 6632.32 6263.76 120.77 o -7 -6 1 4914.30 4816.60 150.19 o -6 -6 1 765.86 706.38 38.23 o -5 -6 1 0.93 6.74 10.73 o -4 -6 1 2187.69 2069.75 57.91 o -3 -6 1 5471.62 5387.48 67.38 o -2 -6 1 19404.64 20091.13 163.99 o -1 -6 1 3205.36 3181.49 61.49 o 0 -6 1 2602.15 2651.88 49.60 o 1 -6 1 542.82 618.65 25.56 o 2 -6 1 2193.19 2231.73 68.20 o 3 -6 1 2875.52 2893.72 81.94 o 4 -6 1 4069.31 4076.78 127.64 o 5 -6 1 990.02 916.95 73.22 o 6 -6 1 368.62 345.35 40.44 o 7 -6 1 12.18 -6.21 14.14 o 8 -6 1 408.73 420.34 47.30 o 9 -6 1 496.75 503.95 146.33 o -13 -5 1 198.72 164.15 33.45 o -12 -5 1 220.05 174.03 40.99 o -11 -5 1 1060.07 1123.00 57.27 o -10 -5 1 2138.72 2113.87 72.99 o -9 -5 1 1580.33 1598.43 92.56 o -8 -5 1 1551.71 1453.53 55.57 o -7 -5 1 645.15 679.51 37.17 o -6 -5 1 930.23 941.88 40.50 o -5 -5 1 3433.18 3435.15 102.78 o -4 -5 1 11042.16 11008.07 139.43 o -3 -5 1 24283.33 25072.67 181.07 o -2 -5 1 7753.95 7825.58 81.43 o -1 -5 1 1283.95 1379.95 32.07 o 0 -5 1 276.97 327.66 17.46 o 1 -5 1 2894.59 2830.34 48.06 o 2 -5 1 4520.54 4353.96 73.34 o 3 -5 1 4201.31 4247.65 93.84 o 4 -5 1 1695.16 1742.30 62.96 o 5 -5 1 58.44 17.19 18.54 o 6 -5 1 442.51 520.87 43.60 o 7 -5 1 1230.26 1215.20 62.44 o 8 -5 1 1964.05 1969.11 82.16 o 9 -5 1 1140.10 1147.34 70.86 o 10 -5 1 384.44 449.60 79.03 o -13 -4 1 120.31 107.68 43.50 o -12 -4 1 1958.39 1811.73 88.30 o -11 -4 1 2193.24 2271.90 77.82 o -10 -4 1 1573.78 1617.72 63.04 o -9 -4 1 531.87 508.12 61.69 o -8 -4 1 5.78 20.40 17.64 o -7 -4 1 5324.18 5183.68 97.28 o -6 -4 1 4965.40 4628.45 180.31 o -5 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