# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 9Tjv1_0m in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 192.91 _exptl_crystal_F_000 652.00 _reflns_d_resolution_high 0.7569 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.7090 _cell_length_b 10.1860 _cell_length_c 15.3930 _cell_angle_alpha 77.499 _cell_angle_beta 85.045 _cell_angle_gamma 70.279 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 26.11 -1.63 0.82 o 2 0 0 11084.92 12164.80 162.08 o 3 0 0 328.00 360.87 12.94 o 4 0 0 9014.58 9743.65 131.72 o 5 0 0 784.58 829.05 22.48 o 6 0 0 822.80 684.98 32.83 o 7 0 0 750.51 798.41 43.61 o 8 0 0 294.72 301.32 33.49 o 9 0 0 519.81 412.37 49.70 o 10 0 0 677.47 678.36 67.91 o 11 0 0 627.42 644.62 104.37 o 12 0 0 62.17 92.68 54.63 o -11 1 0 772.99 871.10 150.72 o -10 1 0 164.53 159.97 37.52 o -9 1 0 1535.84 1342.98 91.47 o -8 1 0 76.06 68.86 18.87 o -7 1 0 2419.07 2543.84 54.55 o -6 1 0 32.55 17.23 8.57 o -5 1 0 4295.70 4399.19 120.64 o -4 1 0 1737.54 1818.01 46.41 o -3 1 0 10192.85 11289.75 154.45 o -2 1 0 6191.33 6860.92 94.98 o -1 1 0 14773.83 15652.82 344.41 o 0 1 0 1287.89 -1.43 0.72 o 1 1 0 10014.82 -2.99 1.50 o 2 1 0 5979.77 6384.30 142.92 o 3 1 0 1080.64 1134.35 30.27 o 4 1 0 1555.22 1701.90 49.26 o 5 1 0 795.35 860.18 35.02 o 6 1 0 9169.20 10144.39 174.65 o 7 1 0 0.02 16.42 8.09 o 8 1 0 1514.57 1659.41 59.53 o 9 1 0 104.45 88.91 22.89 o 10 1 0 1240.02 1317.65 85.64 o 11 1 0 11.64 6.25 22.98 o 12 1 0 671.63 687.62 112.70 o -11 2 0 168.58 115.01 55.12 o -10 2 0 1501.97 1492.97 108.17 o -9 2 0 94.54 67.39 17.14 o -8 2 0 1968.01 2148.65 73.48 o -7 2 0 2001.95 2044.84 74.75 o -6 2 0 1933.24 2068.73 61.23 o -5 2 0 1338.98 1365.58 67.24 o -4 2 0 3464.73 3900.38 75.87 o -3 2 0 7392.20 7798.39 112.78 o -2 2 0 244.31 210.74 13.72 o -1 2 0 24787.81 27983.40 318.01 o 0 2 0 9667.12 10817.09 138.99 o 1 2 0 2122.49 2225.77 41.58 o 2 2 0 3996.20 4370.10 84.84 o 3 2 0 3725.25 4104.96 208.89 o 4 2 0 1362.85 1423.26 40.78 o 5 2 0 1610.07 1615.05 41.70 o 6 2 0 1028.51 955.99 75.13 o 7 2 0 669.17 701.36 54.41 o 8 2 0 1044.30 895.84 68.14 o 9 2 0 548.72 588.71 50.60 o 10 2 0 334.24 323.18 41.69 o 11 2 0 0.34 -20.87 19.68 o 12 2 0 75.03 81.46 52.55 o -10 3 0 591.53 630.04 70.27 o -9 3 0 124.82 154.97 30.31 o -8 3 0 507.00 539.14 64.48 o -7 3 0 572.12 544.10 58.48 o -6 3 0 1523.38 1559.23 66.78 o -5 3 0 27.68 18.53 10.03 o -4 3 0 5769.56 6236.17 160.19 o -3 3 0 170.65 204.72 19.03 o -2 3 0 13008.51 14481.02 187.26 o -1 3 0 5687.26 6702.82 96.89 o 0 3 0 5963.63 6632.51 90.29 o 1 3 0 31.33 40.47 4.54 o 2 3 0 1978.61 1959.62 44.18 o 3 3 0 2134.13 2179.42 74.93 o 4 3 0 1082.58 1150.78 58.52 o 5 3 0 1474.64 1475.77 46.69 o 6 3 0 54.31 52.93 10.81 o 7 3 0 1281.94 1321.34 43.59 o 8 3 0 46.70 46.56 11.58 o 9 3 0 739.53 681.49 67.28 o 10 3 0 54.61 54.92 16.68 o 11 3 0 28.96 20.35 19.20 o 12 3 0 191.20 179.18 44.71 o -10 4 0 12.02 -19.33 53.36 o -9 4 0 332.35 312.29 45.07 o -8 4 0 70.54 75.77 25.78 o -7 4 0 185.75 130.98 28.60 o -6 4 0 2742.67 2870.96 105.57 o -5 4 0 871.28 824.85 48.37 o -4 4 0 1981.31 1969.60 67.62 o -3 4 0 105.88 79.89 13.05 o -2 4 0 2603.10 2746.31 59.87 o -1 4 0 2022.80 2433.96 51.63 o 0 4 0 391.30 558.83 21.02 o 1 4 0 113.74 117.98 9.32 o 2 4 0 4438.30 4679.51 66.07 o 3 4 0 167.14 190.20 21.24 o 4 4 0 260.08 251.23 22.38 o 5 4 0 468.30 432.68 38.91 o 6 4 0 1462.17 1453.63 72.95 o 7 4 0 1799.40 1838.71 60.36 o 8 4 0 42.67 44.32 10.09 o 9 4 0 1418.47 1458.75 65.59 o 10 4 0 24.35 11.30 17.57 o 11 4 0 501.68 519.91 49.43 o 12 4 0 227.54 184.48 41.70 o -9 5 0 440.33 360.48 85.02 o -8 5 0 99.80 35.48 32.22 o -7 5 0 566.40 632.12 60.70 o -6 5 0 1076.20 1046.10 70.13 o -5 5 0 1138.53 1146.60 60.21 o -4 5 0 298.78 255.99 28.17 o -3 5 0 265.84 270.92 26.25 o -2 5 0 38.93 18.74 8.51 o -1 5 0 99.56 42.72 12.62 o 0 5 0 3455.34 3893.57 74.02 o 1 5 0 59.78 35.09 7.48 o 2 5 0 1860.13 1955.34 39.96 o 3 5 0 1.92 2.36 4.37 o 4 5 0 2585.64 2675.98 80.48 o 5 5 0 39.86 38.79 7.37 o 6 5 0 7016.74 7528.78 172.93 o 7 5 0 227.56 245.12 17.97 o 8 5 0 1918.21 1991.76 65.07 o 9 5 0 64.81 53.11 14.75 o 10 5 0 5.34 -5.86 15.07 o 11 5 0 256.69 267.85 103.18 o 12 5 0 207.07 245.95 64.86 o -8 6 0 374.02 326.06 78.17 o -7 6 0 277.30 215.56 43.26 o -6 6 0 1433.45 1450.79 126.57 o -5 6 0 511.63 633.89 56.63 o -4 6 0 25.81 5.69 12.32 o -3 6 0 941.21 882.65 51.76 o -2 6 0 45.17 31.40 13.78 o -1 6 0 16.31 7.91 7.01 o 0 6 0 22.40 19.31 6.86 o 1 6 0 2540.96 2679.40 65.88 o 2 6 0 270.48 257.43 24.58 o 3 6 0 1112.98 1026.98 79.39 o 4 6 0 201.35 161.67 15.04 o 5 6 0 2155.09 2222.99 83.32 o 6 6 0 126.36 110.11 28.57 o 7 6 0 1535.81 1651.43 81.33 o 8 6 0 788.85 850.49 41.03 o 9 6 0 12.67 14.28 10.70 o 10 6 0 332.74 431.18 44.00 o 11 6 0 2.33 -43.80 23.58 o 12 6 0 1725.22 1959.62 148.25 o -7 7 0 48.25 79.07 30.85 o -6 7 0 527.58 510.08 67.37 o -5 7 0 137.57 66.43 25.94 o -4 7 0 1112.49 1067.14 85.21 o -3 7 0 1072.36 1254.71 117.41 o -2 7 0 976.70 956.65 61.08 o -1 7 0 943.58 875.19 49.78 o 0 7 0 2545.70 2797.91 72.37 o 1 7 0 1782.46 1864.76 55.12 o 2 7 0 856.60 778.67 31.59 o 3 7 0 1480.48 1543.35 40.28 o 4 7 0 1308.71 1222.51 50.94 o 5 7 0 2047.10 2090.24 61.95 o 6 7 0 635.29 659.06 37.94 o 7 7 0 1267.02 1393.42 43.54 o 8 7 0 8.13 19.86 8.27 o 9 7 0 942.59 993.92 68.23 o 10 7 0 130.01 119.19 30.32 o 11 7 0 1058.98 1147.22 92.65 o 12 7 0 20.21 18.11 33.27 o -7 8 0 730.86 1055.86 211.21 o -6 8 0 86.56 42.93 56.22 o -5 8 0 5.73 26.81 29.28 o -4 8 0 1079.59 1008.55 86.89 o -3 8 0 214.27 173.31 38.96 o -2 8 0 612.71 737.58 67.34 o -1 8 0 156.64 132.40 32.92 o 0 8 0 2120.87 2339.55 72.98 o 1 8 0 783.12 684.39 46.33 o 2 8 0 1457.54 1540.54 56.29 o 3 8 0 13.44 13.28 6.26 o 4 8 0 5063.27 4962.23 127.74 o 5 8 0 134.40 109.87 19.33 o 6 8 0 1876.08 1910.97 82.49 o 7 8 0 27.13 44.81 13.66 o 8 8 0 1046.20 1064.38 93.71 o 9 8 0 286.27 257.98 52.85 o 10 8 0 545.25 555.50 56.86 o 11 8 0 642.78 744.18 68.65 o 12 8 0 274.34 245.95 46.33 o -5 9 0 512.92 725.01 108.47 o -4 9 0 2.41 19.16 29.78 o -3 9 0 2120.97 2161.20 147.97 o -2 9 0 152.80 113.53 37.52 o -1 9 0 949.21 1165.02 100.73 o 0 9 0 379.12 367.72 55.38 o 1 9 0 2426.33 2468.45 195.20 o 2 9 0 1066.86 1010.88 60.42 o 3 9 0 1832.14 1941.94 198.78 o 4 9 0 5.57 5.63 12.43 o 5 9 0 1707.91 1573.67 87.69 o 6 9 0 76.88 55.92 24.14 o 7 9 0 516.47 465.89 38.20 o 8 9 0 169.76 105.71 60.65 o 9 9 0 253.11 207.91 78.97 o 10 9 0 975.72 1087.43 245.53 o 11 9 0 3.79 25.69 24.85 o -4 10 0 1104.09 1152.69 175.62 o -3 10 0 235.58 289.40 54.78 o -2 10 0 1350.33 1192.24 118.14 o -1 10 0 1235.27 1179.92 108.33 o 0 10 0 2385.51 2090.11 126.62 o 1 10 0 673.04 685.10 64.85 o 2 10 0 675.50 549.02 32.02 o 3 10 0 3001.66 2975.86 227.00 o 4 10 0 108.32 95.49 36.43 o 5 10 0 395.23 448.12 108.66 o 6 10 0 1.43 -15.04 18.62 o 7 10 0 1392.29 1509.95 211.21 o 8 10 0 5.83 18.57 18.47 o 9 10 0 521.96 535.30 44.86 o 10 10 0 0.88 -10.44 21.56 o 11 10 0 534.14 462.42 61.07 o -3 11 0 600.02 491.91 116.66 o -2 11 0 1047.30 947.17 176.04 o -1 11 0 105.29 95.52 47.20 o 0 11 0 1875.47 1876.83 127.99 o 1 11 0 27.81 23.19 30.72 o 2 11 0 1157.99 1055.89 72.65 o 3 11 0 13.68 57.28 37.48 o 4 11 0 87.88 86.21 31.15 o 5 11 0 136.50 88.39 46.96 o 6 11 0 807.08 715.64 88.82 o 7 11 0 104.67 80.85 40.85 o 8 11 0 142.16 176.04 95.18 o 9 11 0 390.92 343.97 56.98 o 10 11 0 30.74 6.07 33.80 o -1 12 0 555.84 196.26 133.93 o 0 12 0 295.40 298.60 131.40 o 1 12 0 126.74 77.91 43.98 o 2 12 0 455.37 469.58 126.77 o 3 12 0 164.21 134.35 84.65 o 4 12 0 122.23 73.74 45.83 o 5 12 0 51.56 36.05 37.14 o 6 12 0 757.07 720.81 102.50 o 7 12 0 3.35 36.23 36.15 o 8 12 0 276.99 336.50 122.98 o 3 13 0 287.83 194.90 73.32 o 4 13 0 439.01 319.55 89.05 o 5 13 0 167.77 77.55 48.25 o -8 -12 1 861.77 935.48 143.19 o -7 -12 1 80.88 26.95 63.59 o -6 -12 1 511.94 554.93 96.86 o -5 -12 1 284.79 325.37 74.02 o -4 -12 1 264.12 199.36 63.85 o -3 -12 1 257.54 229.11 111.18 o -2 -12 1 193.39 150.77 96.44 o -1 -12 1 537.03 561.29 70.57 o 0 -12 1 10.16 126.35 122.13 o -9 -11 1 585.47 796.74 87.66 o -8 -11 1 261.74 345.52 84.65 o -7 -11 1 0.68 5.42 26.80 o -6 -11 1 573.99 581.28 83.46 o -5 -11 1 0.14 -22.53 21.14 o -4 -11 1 672.62 539.52 83.10 o -3 -11 1 35.93 46.75 45.48 o -2 -11 1 434.66 373.67 35.91 o -1 -11 1 419.57 453.38 60.43 o 0 -11 1 353.94 329.40 63.01 o 1 -11 1 190.99 158.34 112.87 o 2 -11 1 87.38 80.44 56.86 o -10 -10 1 6.63 15.42 37.69 o -9 -10 1 952.43 1173.76 156.04 o -8 -10 1 94.43 54.68 28.35 o -7 -10 1 242.24 236.97 53.28 o -6 -10 1 3.81 12.00 22.91 o -5 -10 1 129.27 133.13 39.16 o -4 -10 1 441.24 479.39 72.19 o -3 -10 1 79.46 123.40 53.49 o -2 -10 1 1586.46 1733.54 298.81 o -1 -10 1 36.40 14.91 23.37 o 0 -10 1 2353.29 2172.33 139.19 o 1 -10 1 16.01 -31.09 32.43 o 2 -10 1 582.31 651.10 92.28 o 3 -10 1 153.83 185.15 59.10 o -11 -9 1 497.66 518.44 67.38 o -10 -9 1 135.97 88.94 30.72 o -9 -9 1 562.12 710.74 125.50 o -8 -9 1 4.95 -3.38 12.92 o -7 -9 1 657.78 664.81 60.11 o -6 -9 1 67.54 28.05 24.06 o -5 -9 1 3140.92 3180.77 118.58 o -4 -9 1 2.63 -0.66 12.74 o -3 -9 1 1766.46 1983.63 170.15 o -2 -9 1 617.69 743.63 193.31 o -1 -9 1 2597.48 2667.47 222.37 o 0 -9 1 182.36 207.42 39.96 o 1 -9 1 1912.09 1943.73 127.55 o 2 -9 1 990.13 910.13 96.71 o 3 -9 1 515.11 457.43 74.15 o 4 -9 1 722.65 771.18 142.35 o 5 -9 1 405.62 417.78 122.98 o -11 -8 1 0.79 -9.27 25.69 o -10 -8 1 897.85 848.20 75.81 o -9 -8 1 577.92 604.01 83.39 o -8 -8 1 533.16 651.49 60.44 o -7 -8 1 752.50 677.68 53.33 o -6 -8 1 558.25 622.61 49.72 o -5 -8 1 491.04 546.30 36.22 o -4 -8 1 1187.63 1247.19 42.07 o -3 -8 1 3912.81 4149.34 89.62 o -2 -8 1 430.14 425.56 26.75 o -1 -8 1 801.81 795.43 37.32 o 0 -8 1 872.18 1066.96 63.95 o 1 -8 1 3246.79 3277.62 129.35 o 2 -8 1 37.17 23.29 18.91 o 3 -8 1 1370.38 1452.71 268.35 o 4 -8 1 23.43 35.07 22.05 o 5 -8 1 1647.76 1584.73 211.42 o 6 -8 1 251.34 339.45 102.76 o -12 -7 1 583.76 561.82 88.44 o -11 -7 1 671.22 644.78 77.07 o -10 -7 1 638.17 610.25 66.96 o -9 -7 1 43.27 15.16 18.11 o -8 -7 1 1142.78 1141.52 42.89 o -7 -7 1 352.41 360.11 23.56 o -6 -7 1 3352.61 3559.46 100.79 o -5 -7 1 283.65 269.96 20.51 o -4 -7 1 2817.43 2775.17 83.83 o -3 -7 1 5.91 10.54 5.78 o -2 -7 1 8606.55 9113.81 233.67 o -1 -7 1 1.23 5.68 6.78 o 0 -7 1 3009.72 3134.66 78.49 o 1 -7 1 155.13 176.92 30.62 o 2 -7 1 2079.99 1883.92 98.37 o 3 -7 1 1286.04 1327.60 86.87 o 4 -7 1 539.80 639.05 67.16 o 5 -7 1 389.35 408.49 55.32 o 6 -7 1 251.04 380.05 121.71 o 7 -7 1 905.24 925.45 112.99 o -12 -6 1 421.30 534.02 89.71 o -11 -6 1 403.98 469.16 76.23 o -10 -6 1 2.22 3.37 14.59 o -9 -6 1 1963.21 2300.09 94.69 o -8 -6 1 0.01 -5.21 7.74 o -7 -6 1 2349.19 2644.93 86.05 o -6 -6 1 980.31 1015.56 43.48 o -5 -6 1 2821.68 2941.01 64.24 o -4 -6 1 157.03 106.25 16.48 o -3 -6 1 4420.35 4657.29 82.06 o -2 -6 1 751.11 763.55 29.06 o -1 -6 1 2145.37 2215.23 53.81 o 0 -6 1 1768.28 1858.99 53.45 o 1 -6 1 1175.91 1118.76 50.53 o 2 -6 1 551.06 550.22 35.88 o 3 -6 1 1048.27 1155.02 60.75 o 4 -6 1 2145.30 2260.19 83.91 o 5 -6 1 132.34 99.04 23.27 o 6 -6 1 793.65 927.31 114.13 o 7 -6 1 3.16 -0.10 25.78 o 8 -6 1 317.74 361.46 86.64 o -12 -5 1 206.13 349.98 75.81 o -11 -5 1 559.46 550.75 82.97 o -10 -5 1 914.28 829.92 77.70 o -9 -5 1 2243.20 2177.10 98.40 o -8 -5 1 980.16 1004.97 37.46 o -7 -5 1 1177.97 1218.72 43.76 o -6 -5 1 1797.84 1904.03 53.24 o -5 -5 1 1013.39 937.86 29.68 o -4 -5 1 175.27 161.87 13.11 o -3 -5 1 3802.42 3794.89 69.56 o -2 -5 1 3740.46 4079.55 75.07 o -1 -5 1 2655.31 2703.93 53.31 o 0 -5 1 468.21 578.23 25.83 o 1 -5 1 1545.48 1399.18 48.01 o 2 -5 1 44.16 47.60 10.98 o 3 -5 1 2039.77 2197.35 78.07 o 4 -5 1 2134.48 2229.52 77.82 o 5 -5 1 719.95 770.29 57.23 o 6 -5 1 1798.30 1738.87 86.46 o 7 -5 1 37.80 47.83 23.99 o 8 -5 1 16.75 66.96 50.96 o 9 -5 1 9.08 -14.12 48.07 o -12 -4 1 111.33 123.50 32.48 o -11 -4 1 477.19 432.08 59.10 o -10 -4 1 472.95 575.72 63.83 o -9 -4 1 1531.64 1626.80 89.13 o -8 -4 1 3118.94 3251.94 82.13 o -7 -4 1 17.40 19.38 7.04 o -6 -4 1 3064.41 3113.88 84.50 o -5 -4 1 30.48 40.03 8.63 o -4 -4 1 4739.00 5070.22 79.84 o -3 -4 1 750.57 810.45 28.03 o -2 -4 1 2474.21 2673.96 40.95 o -1 -4 1 235.06 197.91 12.15 o 0 -4 1 9.29 4.76 4.30 o 1 -4 1 42.59 46.22 8.63 o 2 -4 1 650.15 659.18 30.45 o 3 -4 1 1836.18 1938.57 58.45 o 4 -4 1 360.78 329.29 49.19 o 5 -4 1 448.63 392.77 35.06 o 6 -4 1 101.64 61.01 25.11 o 7 -4 1 1196.71 1260.02 87.92 o 8 -4 1 79.01 74.75 36.64 o 9 -4 1 94.48 104.01 30.62 o 10 -4 1 620.86 814.67 177.73 o -12 -3 1 0.75 9.47 28.81 o -11 -3 1 657.28 650.83 60.39 o -10 -3 1 79.91 58.11 53.91 o -9 -3 1 1193.64 1185.47 83.28 o -8 -3 1 351.98 345.18 27.68 o -7 -3 1 641.60 686.49 32.58 o -6 -3 1 366.15 358.48 19.87 o -5 -3 1 3937.51 4039.62 97.66 o -4 -3 1 2302.36 2469.78 52.54 o -3 -3 1 1301.53 1414.05 33.09 o -2 -3 1 183.47 163.88 7.65 o -1 -3 1 431.38 450.74 14.73 o 0 -3 1 2614.76 2662.88 50.42 o 1 -3 1 1.85 -0.60 3.70 o 2 -3 1 2327.13 2418.58 51.51 o 3 -3 1 1902.06 1984.71 51.55 o 4 -3 1 1437.35 1368.43 48.15 o 5 -3 1 827.45 871.55 54.72 o 6 -3 1 282.50 308.13 34.06 o 7 -3 1 186.90 232.02 52.32 o 8 -3 1 36.73 41.15 18.52 o 9 -3 1 583.77 669.94 54.79 o 10 -3 1 139.16 106.53 38.16 o -12 -2 1 139.33 115.27 40.73 o -11 -2 1 565.27 628.38 64.50 o -10 -2 1 398.02 350.44 43.75 o -9 -2 1 1207.71 1242.97 69.94 o -8 -2 1 160.32 84.40 33.98 o -7 -2 1 1546.57 1728.32 58.75 o -6 -2 1 80.13 71.68 11.95 o -5 -2 1 742.60 643.10 29.42 o -4 -2 1 1838.44 1857.19 43.47 o -3 -2 1 4542.99 4724.09 82.75 o -2 -2 1 6027.73 6090.68 82.17 o -1 -2 1 2500.22 2532.31 35.09 o 0 -2 1 6393.95 6610.52 91.35 o 1 -2 1 4888.22 5453.06 77.53 o 2 -2 1 13535.76 14674.40 182.69 o 3 -2 1 449.34 496.13 24.10 o 4 -2 1 1787.98 1754.47 50.30 o 5 -2 1 36.68 11.68 7.72 o 6 -2 1 1612.65 1587.89 52.22 o 7 -2 1 83.67 50.18 11.95 o 8 -2 1 464.57 429.04 49.51 o 9 -2 1 983.63 965.28 63.46 o 10 -2 1 666.71 828.30 83.69 o 11 -2 1 993.56 1102.91 111.99 o -12 -1 1 517.73 564.44 86.74 o -11 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486.43 145.30 o 3 4 20 15.25 94.76 90.13 o 1 5 20 433.13 448.11 144.46 o 2 5 20 97.55 93.50 99.81 o