# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' dobbie in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 326.02 _exptl_crystal_F_000 948.00 _reflns_d_resolution_high 0.7202 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.8934 _cell_length_b 12.3039 _cell_length_c 16.8933 _cell_angle_alpha 81.743 _cell_angle_beta 83.286 _cell_angle_gamma 69.965 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3866.19 3861.83 34.31 o 2 0 0 21996.06 22487.17 99.86 o 3 0 0 26725.36 28945.38 87.37 o 4 0 0 1515.92 1520.27 16.94 o 5 0 0 17527.57 17634.03 249.44 o 6 0 0 101.23 100.04 11.06 o 7 0 0 5741.35 5849.69 55.52 o 8 0 0 1230.97 1351.42 44.94 o 9 0 0 1877.32 1984.46 68.93 o 10 0 0 1191.37 1205.32 69.93 o 11 0 0 522.62 549.58 91.12 o 12 0 0 487.55 406.34 123.21 o -12 1 0 1031.10 1162.72 138.72 o -11 1 0 35.11 34.64 105.03 o -10 1 0 2276.31 2267.69 93.48 o -9 1 0 110.67 106.57 56.16 o -8 1 0 3854.54 3603.71 72.84 o -7 1 0 6158.21 6056.24 60.99 o -6 1 0 2919.06 3106.74 42.55 o -5 1 0 7888.45 8052.52 59.29 o -4 1 0 355.34 318.84 25.19 o -3 1 0 5712.69 6178.33 44.19 o -2 1 0 3606.12 4252.22 25.27 o -1 1 0 28357.07 34337.00 150.92 o 1 1 0 18421.60 19080.15 74.81 o 3 1 0 2429.89 2554.44 20.93 o 4 1 0 7206.52 7792.33 38.37 o 5 1 0 835.85 953.90 22.43 o 6 1 0 12687.94 12750.68 75.12 o 7 1 0 4731.01 4936.03 51.75 o 8 1 0 233.11 228.29 33.02 o 9 1 0 1848.99 1932.78 67.90 o 10 1 0 35.24 20.18 64.34 o 11 1 0 2060.48 2064.02 94.75 o 12 1 0 71.52 -22.62 111.66 o -12 2 0 12.75 48.39 149.10 o -11 2 0 1546.30 1695.08 135.82 o -10 2 0 434.13 386.27 71.15 o -9 2 0 1675.31 1587.75 75.42 o -8 2 0 3856.25 3938.05 72.41 o -7 2 0 572.76 694.06 38.13 o -6 2 0 9830.45 9942.03 73.38 o -5 2 0 59.33 34.61 22.67 o -4 2 0 32548.08 34955.99 124.18 o -3 2 0 7534.85 7860.98 68.48 o -2 2 0 10108.34 11594.91 54.99 o -1 2 0 70217.11 74771.35 590.89 o 0 2 0 4848.97 4727.88 25.30 o 1 2 0 12435.85 14575.92 88.63 o 2 2 0 5591.29 5604.97 29.32 o 3 2 0 1761.66 1757.78 23.41 o 4 2 0 12043.11 13292.76 95.26 o 5 2 0 10057.60 10834.82 50.64 o 6 2 0 4495.45 4510.89 43.74 o 7 2 0 9.53 13.86 21.67 o 8 2 0 5044.39 5001.60 51.11 o 9 2 0 305.85 317.13 50.83 o 10 2 0 1803.46 1838.89 85.23 o 11 2 0 635.39 572.80 77.70 o 12 2 0 296.10 292.65 82.81 o 13 2 0 838.13 873.86 246.21 o -11 3 0 1582.23 1499.87 116.65 o -10 3 0 70.55 99.62 83.74 o -9 3 0 2108.54 2220.49 91.51 o -8 3 0 144.20 167.36 44.94 o -7 3 0 3232.40 3090.04 61.21 o -6 3 0 1554.32 1595.69 38.18 o -5 3 0 3233.86 3341.80 43.41 o -4 3 0 5035.00 5240.53 59.88 o -3 3 0 1010.18 1255.10 15.79 o -2 3 0 25233.20 27166.19 182.37 o -1 3 0 11353.60 12079.87 66.20 o 1 3 0 1195.67 1151.54 19.19 o 2 3 0 9631.61 9668.54 81.10 o 3 3 0 8373.34 9748.03 84.63 o 4 3 0 61.59 181.17 28.88 o 5 3 0 13565.97 13374.73 145.62 o 6 3 0 25.50 59.28 22.38 o 7 3 0 7366.98 7204.05 63.72 o 8 3 0 1489.91 1578.81 43.41 o 9 3 0 1324.14 1445.34 76.57 o 10 3 0 2252.74 2159.48 89.22 o 11 3 0 48.06 29.42 71.07 o 12 3 0 1304.88 1269.82 106.52 o 13 3 0 2.63 28.19 113.07 o -11 4 0 25.22 8.32 126.33 o -10 4 0 2191.09 2146.61 141.31 o -9 4 0 1345.62 1432.73 88.27 o -8 4 0 1377.35 1382.62 79.59 o -7 4 0 2157.80 2220.85 66.85 o -6 4 0 1605.24 1706.41 67.86 o -5 4 0 6845.99 6646.58 148.83 o -4 4 0 14.05 16.63 10.64 o -3 4 0 17178.33 17539.45 57.07 o -2 4 0 4775.43 4917.60 30.58 o -1 4 0 19584.65 21561.67 208.99 o 0 4 0 9140.31 8510.17 44.23 o 1 4 0 250.49 210.64 17.60 o 2 4 0 12436.16 13753.69 63.68 o 3 4 0 2295.15 2105.17 50.76 o 4 4 0 14659.62 15202.80 106.52 o 5 4 0 2974.20 3088.35 54.83 o 6 4 0 2322.14 2382.67 52.10 o 7 4 0 4261.49 4323.25 63.95 o 8 4 0 90.28 88.85 26.21 o 9 4 0 2413.66 2261.92 60.00 o 10 4 0 31.25 8.55 66.66 o 11 4 0 1206.16 1254.47 86.27 o 12 4 0 348.53 282.17 94.01 o 13 4 0 719.85 651.99 121.20 o -10 5 0 1322.32 1496.90 134.67 o -9 5 0 215.22 218.96 104.22 o -8 5 0 2410.89 2603.92 130.03 o -7 5 0 236.89 239.33 82.61 o -6 5 0 5980.56 5885.60 117.92 o -5 5 0 477.22 471.83 22.37 o -4 5 0 2437.01 2492.07 31.86 o -3 5 0 7915.10 8143.43 44.64 o -2 5 0 1769.62 1794.07 26.28 o -1 5 0 7938.90 8339.83 65.35 o 0 5 0 9.34 3.66 16.16 o 1 5 0 14811.68 15833.10 73.92 o 2 5 0 1639.49 1488.78 31.52 o 3 5 0 13627.46 13294.06 91.50 o 4 5 0 9538.97 9869.20 102.92 o 5 5 0 1158.38 1111.87 47.75 o 6 5 0 9317.59 8810.08 99.46 o 7 5 0 368.70 340.31 44.47 o 8 5 0 1451.82 1373.44 53.27 o 9 5 0 706.67 720.45 57.10 o 10 5 0 972.14 1064.32 89.42 o 11 5 0 1894.11 1770.23 107.55 o 12 5 0 320.63 343.41 112.43 o 13 5 0 1025.20 1025.61 131.88 o -10 6 0 24.59 92.85 119.01 o -9 6 0 1810.05 1889.19 137.71 o -8 6 0 611.17 643.35 131.35 o -7 6 0 2252.06 2469.24 123.68 o -6 6 0 5280.48 5403.29 146.47 o -5 6 0 770.59 880.63 87.26 o -4 6 0 10865.14 11019.99 88.82 o -3 6 0 800.39 723.41 25.51 o -2 6 0 5134.58 4962.69 42.69 o -1 6 0 4885.00 4695.29 55.92 o 0 6 0 3386.58 3448.18 38.22 o 1 6 0 3280.22 2835.51 41.02 o 2 6 0 2683.85 2851.82 39.91 o 3 6 0 4905.61 5041.05 58.93 o 4 6 0 16.31 -2.30 26.24 o 5 6 0 3483.35 3354.76 69.91 o 6 6 0 1405.82 1413.52 57.24 o 7 6 0 2459.36 2376.04 68.64 o 8 6 0 1299.12 1319.24 61.41 o 9 6 0 205.20 216.37 49.53 o 10 6 0 2758.32 2633.17 84.28 o 11 6 0 52.66 -24.54 101.47 o 12 6 0 1354.61 1190.35 126.07 o 13 6 0 314.98 296.46 125.41 o -9 7 0 1334.92 1585.59 141.04 o -8 7 0 176.42 180.55 128.33 o -7 7 0 2868.96 2990.63 138.66 o -6 7 0 23.47 22.11 88.55 o -5 7 0 5432.03 5107.98 143.72 o -4 7 0 2819.75 2731.80 51.10 o -3 7 0 2804.43 2564.56 50.33 o -2 7 0 3442.65 3303.90 45.23 o -1 7 0 1385.65 1259.48 31.58 o 0 7 0 9447.73 8929.10 101.46 o 1 7 0 64.16 74.97 25.22 o 2 7 0 10895.35 11316.83 80.98 o 3 7 0 1691.08 1372.77 37.67 o 4 7 0 1762.57 1644.17 47.45 o 5 7 0 3916.96 3765.19 83.23 o 6 7 0 464.05 450.01 50.08 o 7 7 0 4073.28 3825.74 85.11 o 8 7 0 3.20 16.97 52.54 o 9 7 0 4012.11 3992.95 93.86 o 10 7 0 1442.94 1302.47 71.46 o 11 7 0 1196.30 1200.46 119.57 o 12 7 0 953.02 836.11 120.14 o 13 7 0 77.21 80.26 119.67 o -9 8 0 184.68 215.65 149.78 o -8 8 0 1532.79 1642.50 171.34 o -7 8 0 587.59 525.16 108.62 o -6 8 0 1016.70 987.11 107.18 o -5 8 0 3950.26 3687.31 187.34 o -4 8 0 592.34 544.19 44.13 o -3 8 0 3147.38 3027.59 58.22 o -2 8 0 107.68 87.03 26.49 o -1 8 0 2914.70 2836.27 87.07 o 0 8 0 1561.78 1474.26 36.54 o 1 8 0 4583.85 4660.81 68.39 o 2 8 0 6197.77 5952.40 65.35 o 3 8 0 23.04 19.50 32.96 o 4 8 0 2381.01 2279.51 52.00 o 5 8 0 283.68 312.16 37.50 o 6 8 0 5309.65 5142.95 96.26 o 7 8 0 822.80 764.46 60.54 o 8 8 0 1047.22 1086.55 66.63 o 9 8 0 3700.10 3547.59 95.53 o 10 8 0 364.10 391.76 63.51 o 11 8 0 1465.86 1408.46 100.04 o 12 8 0 12.87 19.12 111.66 o 13 8 0 614.37 584.38 194.59 o -8 9 0 1390.77 1515.66 176.93 o -7 9 0 277.87 227.04 91.59 o -6 9 0 1862.74 1768.91 127.89 o -5 9 0 94.67 130.36 92.47 o -4 9 0 3661.29 3401.03 135.08 o -3 9 0 503.25 519.05 43.20 o -2 9 0 584.17 595.99 46.06 o -1 9 0 484.56 497.21 45.16 o 0 9 0 1962.96 1759.75 68.24 o 1 9 0 7819.36 7581.78 95.64 o 2 9 0 306.68 390.47 42.54 o 3 9 0 5922.54 5983.48 97.41 o 4 9 0 3267.33 2928.28 61.81 o 5 9 0 3353.75 3171.92 80.94 o 6 9 0 3783.58 3581.14 96.58 o 7 9 0 560.51 495.03 61.34 o 8 9 0 3123.40 3024.66 90.58 o 9 9 0 59.82 56.66 62.01 o 10 9 0 2338.86 2354.92 91.92 o 11 9 0 503.11 478.04 71.56 o 12 9 0 391.86 337.51 117.93 o -7 10 0 2009.04 2125.09 127.70 o -6 10 0 592.51 618.23 119.72 o -5 10 0 1235.33 1261.45 120.23 o -4 10 0 2462.43 2541.92 140.73 o -3 10 0 250.41 215.03 51.49 o -2 10 0 3451.78 3268.79 74.25 o -1 10 0 345.19 342.00 47.46 o 0 10 0 1719.90 1677.54 68.07 o 1 10 0 888.24 866.55 51.03 o 2 10 0 915.47 959.74 52.50 o 3 10 0 3177.44 2970.94 68.64 o 4 10 0 304.24 256.53 44.72 o 5 10 0 3937.40 4057.13 73.48 o 6 10 0 209.28 149.97 49.17 o 7 10 0 4320.24 4425.26 104.13 o 8 10 0 494.11 540.96 69.52 o 9 10 0 1202.55 1227.64 80.82 o 10 10 0 1182.05 1286.32 84.36 o 11 10 0 294.32 234.59 74.73 o 12 10 0 904.90 766.19 129.05 o -6 11 0 118.81 52.03 119.27 o -5 11 0 1172.04 1252.30 130.83 o -4 11 0 25.76 1.09 103.02 o -3 11 0 2326.55 2449.99 132.35 o -2 11 0 744.47 705.45 64.11 o -1 11 0 3171.93 3198.35 80.25 o 0 11 0 4885.67 5140.21 102.82 o 1 11 0 324.22 346.60 57.33 o 2 11 0 2629.23 2522.06 69.54 o 3 11 0 379.45 341.17 48.62 o 4 11 0 2891.97 2901.67 72.12 o 5 11 0 679.36 587.11 50.86 o 6 11 0 1238.32 1265.05 67.23 o 7 11 0 1607.01 1506.96 82.70 o 8 11 0 930.96 879.49 78.93 o 9 11 0 1619.21 1690.61 91.47 o 10 11 0 22.60 27.79 83.65 o 11 11 0 1020.80 989.30 92.02 o 12 11 0 266.70 208.35 126.54 o -5 12 0 235.71 242.66 121.95 o -4 12 0 458.95 443.95 120.88 o -3 12 0 1015.29 976.51 119.12 o -2 12 0 156.06 129.52 58.57 o -1 12 0 2435.47 2457.26 78.09 o 0 12 0 29.38 39.75 54.43 o 1 12 0 2196.29 2252.54 85.18 o 2 12 0 22.85 16.51 49.01 o 3 12 0 2959.21 2741.60 76.61 o 4 12 0 1308.76 1228.19 62.59 o 5 12 0 461.29 406.12 63.03 o 6 12 0 2714.66 2695.65 105.92 o 7 12 0 8.91 -11.05 76.49 o 8 12 0 1469.56 1515.11 90.87 o 9 12 0 167.44 95.16 76.47 o 10 12 0 475.17 406.49 82.54 o 11 12 0 816.38 844.48 93.56 o 12 12 0 88.97 145.57 96.16 o -4 13 0 1284.42 1379.01 147.15 o -3 13 0 63.91 87.63 114.25 o -2 13 0 1618.96 1712.00 133.39 o -1 13 0 731.09 693.14 74.55 o 0 13 0 1132.80 1126.33 71.03 o 1 13 0 1472.63 1431.72 82.05 o 2 13 0 445.85 388.37 69.92 o 3 13 0 2207.08 2225.38 87.19 o 4 13 0 109.86 103.00 55.17 o 5 13 0 2693.19 2917.83 153.80 o 6 13 0 426.60 397.24 79.87 o 7 13 0 820.08 834.93 93.13 o 8 13 0 1099.01 1041.82 90.26 o 9 13 0 152.27 169.56 81.17 o 10 13 0 863.56 958.30 95.40 o 11 13 0 54.85 37.58 86.91 o -3 14 0 640.22 673.22 221.89 o -2 14 0 897.68 994.98 131.91 o -1 14 0 137.04 157.20 73.29 o 0 14 0 1585.35 1552.59 92.19 o 1 14 0 13.26 2.50 64.27 o 2 14 0 1708.68 1721.76 90.90 o 3 14 0 498.78 413.74 72.26 o 4 14 0 764.21 824.44 89.58 o 5 14 0 911.50 933.45 111.59 o 6 14 0 465.38 519.47 89.34 o 7 14 0 922.61 935.73 98.61 o 8 14 0 0.27 8.66 83.70 o 9 14 0 634.06 703.06 96.08 o 10 14 0 98.08 109.21 90.28 o -1 15 0 1185.62 1364.88 176.88 o 0 15 0 341.64 319.30 83.25 o 1 15 0 535.85 550.61 85.16 o 2 15 0 1019.81 1018.81 89.58 o 3 15 0 147.78 189.94 86.69 o 4 15 0 1265.23 1229.58 122.32 o 5 15 0 0.31 12.83 102.84 o 6 15 0 991.41 1072.40 123.00 o 7 15 0 149.34 51.15 109.02 o 8 15 0 403.16 615.96 108.65 o 9 15 0 321.66 285.67 93.27 o 1 16 0 542.21 568.21 90.18 o 2 16 0 0.65 -17.42 73.69 o 3 16 0 901.79 973.06 107.07 o 4 16 0 214.01 200.08 111.81 o 5 16 0 477.18 472.35 120.30 o 6 16 0 306.88 271.01 116.22 o -6 -16 1 660.17 801.02 159.42 o -5 -16 1 25.07 70.39 115.76 o -4 -16 1 1129.14 1257.87 131.43 o -3 -16 1 132.12 160.19 111.12 o -2 -16 1 430.49 309.05 86.74 o -1 -16 1 483.89 491.75 90.92 o -9 -15 1 600.58 549.05 171.01 o -8 -15 1 50.83 61.88 88.18 o -7 -15 1 1116.69 1256.91 130.29 o -6 -15 1 121.27 94.08 104.49 o -5 -15 1 530.64 645.95 115.72 o -4 -15 1 627.96 763.68 116.47 o -3 -15 1 388.98 402.53 91.50 o -2 -15 1 950.68 1029.62 88.64 o -1 -15 1 11.11 -1.02 85.82 o 0 -15 1 1037.17 1031.28 93.54 o 1 -15 1 73.12 40.11 145.75 o -10 -14 1 443.19 484.34 97.15 o -9 -14 1 82.88 149.11 87.12 o -8 -14 1 686.15 675.42 94.72 o -7 -14 1 543.53 540.79 92.09 o -6 -14 1 467.67 354.15 88.58 o -5 -14 1 1354.09 1419.89 99.99 o -4 -14 1 58.38 37.03 77.83 o -3 -14 1 1681.18 1616.58 86.80 o -2 -14 1 198.13 204.12 73.30 o -1 -14 1 1271.54 1294.25 87.60 o 0 -14 1 769.59 788.37 83.36 o 1 -14 1 292.09 332.44 77.80 o 2 -14 1 1087.54 1091.91 132.32 o -11 -13 1 520.89 541.63 101.66 o -10 -13 1 450.45 489.54 90.58 o -9 -13 1 132.02 145.17 80.22 o -8 -13 1 898.59 979.91 90.66 o -7 -13 1 29.45 37.61 81.55 o -6 -13 1 1997.75 2032.45 107.05 o -5 -13 1 94.78 138.02 75.85 o -4 -13 1 1543.98 1540.57 71.50 o -3 -13 1 703.54 781.01 65.01 o -2 -13 1 1483.13 1498.08 83.28 o -1 -13 1 2117.98 2245.39 98.47 o 0 -13 1 107.17 102.39 59.39 o 1 -13 1 2142.38 2247.92 93.00 o 2 -13 1 239.01 263.67 107.80 o 3 -13 1 1103.30 1208.70 135.50 o 4 -13 1 895.51 1126.43 245.88 o -12 -12 1 295.61 217.87 104.98 o -11 -12 1 590.07 579.94 89.92 o -10 -12 1 1.56 -0.76 79.00 o -9 -12 1 1355.62 1398.90 93.51 o -8 -12 1 204.75 232.59 74.31 o -7 -12 1 2315.01 2057.69 95.04 o -6 -12 1 1174.53 1309.62 90.56 o -5 -12 1 901.26 788.80 66.76 o -4 -12 1 3045.31 3129.56 79.97 o -3 -12 1 67.79 92.49 51.36 o -2 -12 1 1315.35 1331.96 64.60 o -1 -12 1 9.57 -20.11 60.66 o 0 -12 1 1909.86 1976.74 83.55 o 1 -12 1 516.80 546.89 67.30 o 2 -12 1 882.10 903.22 67.96 o 3 -12 1 1417.55 1469.17 130.10 o 4 -12 1 123.31 98.56 111.82 o 5 -12 1 1487.36 1697.52 148.96 o -12 -11 1 656.39 619.02 232.63 o -11 -11 1 206.07 204.95 80.88 o -10 -11 1 871.47 824.73 84.56 o -9 -11 1 678.14 669.20 78.95 o -8 -11 1 701.72 631.81 77.04 o -7 -11 1 2217.20 2331.82 92.85 o -6 -11 1 272.96 190.96 69.59 o -5 -11 1 2597.82 2728.48 70.04 o -4 -11 1 38.36 7.68 45.57 o -3 -11 1 2908.02 2868.18 73.23 o -2 -11 1 1293.26 1345.44 60.64 o -1 -11 1 531.68 487.74 59.94 o 0 -11 1 2431.02 2541.57 82.55 o 1 -11 1 81.84 51.50 50.61 o 2 -11 1 2626.69 2620.75 80.30 o 3 -11 1 160.33 117.35 100.43 o 4 -11 1 1065.49 1020.10 120.77 o 5 -11 1 627.85 499.62 117.59 o 6 -11 1 595.42 543.79 125.25 o -12 -10 1 398.27 483.43 169.52 o -11 -10 1 218.85 119.48 74.38 o -10 -10 1 1214.41 1146.48 82.34 o -9 -10 1 79.80 52.57 66.55 o -8 -10 1 3113.29 2965.40 97.00 o -7 -10 1 114.69 108.51 61.50 o -6 -10 1 512.52 501.10 51.97 o -5 -10 1 103.81 109.35 42.08 o -4 -10 1 2220.17 1958.70 61.03 o -3 -10 1 1668.53 1652.07 59.38 o -2 -10 1 1023.39 948.03 53.59 o -1 -10 1 2238.14 2326.35 66.34 o 0 -10 1 66.53 41.92 51.40 o 1 -10 1 4527.23 4333.03 89.39 o 2 -10 1 1458.65 1383.57 58.94 o 3 -10 1 2387.13 2402.91 72.45 o 4 -10 1 2144.72 2077.85 128.33 o 5 -10 1 4.80 7.42 118.93 o 6 -10 1 2249.15 2363.99 148.55 o 7 -10 1 10.44 20.57 122.67 o -12 -9 1 119.79 4.54 136.37 o -11 -9 1 1516.84 1471.80 86.27 o -10 -9 1 190.72 215.91 65.66 o -9 -9 1 2449.46 2416.49 91.19 o -8 -9 1 505.61 590.56 66.07 o -7 -9 1 1336.05 1340.41 72.28 o -6 -9 1 829.91 857.96 49.99 o -5 -9 1 537.00 491.19 42.06 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