Acta Cryst. (2010). E66, m46-m47  [ doi:10.1107/S1600536809052763 ]

(Carbonato-²O,O')bis(1,10-phenanthroline-²N,N')cobalt(III) nitrate monohydrate

Ö. Andaç, Z. Yolcu and O. Büyükgüngör

Online 12 December 2009

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.003 Å
• R factor = 0.036
• wR factor = 0.102
• Data-to-parameter ratio = 16.4

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT432_ALERT_2_C Short Inter X...Y Contact  O6     ..  C10     ..       2.97 Ang. 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600          3      
PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF ....          2      
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of          N5     
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         35      

Alert level G
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          3      
PLAT128_ALERT_4_G Non-standard setting of Space-group P21/c   ....      P21/n      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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