Received 10 January 2010
Accepted 13 January 2010
Online 16 January 2010
|Single-crystal X-ray study|
|T = 299 K|
|Mean (C-C) = 0.005 Å|
|R = 0.068|
|wR = 0.136|
|Data-to-parameter ratio = 12.0|
aDepartment of Chemistry, Mangalore University, Mangalagangotri 574 199, Mangalore, India, and bInstitute of Materials Science, Darmstadt University of Technology, Petersenstrasse 23, D-64287 Darmstadt, Germany
Correspondence e-mail: email@example.com
In the molecule of the title compound, C11H11NO2, the dihedral angle between the aromatic ring and the amide segment is 57.3 (1)°.
For a related structure, see: Saraswathi et al. (2010).
Mr = 189.21
Monoclinic, P 21 /c
a = 13.543 (3) Å
b = 5.6539 (9) Å
c = 13.365 (3) Å
= 109.35 (2)°
V = 965.6 (3) Å3
Z = 4
Mo K radiation
= 0.09 mm-1
T = 299 K
0.44 × 0.24 × 0.08 mm
Oxford Diffraction Xcalibur diffractometer with a Sapphire CCD detector
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) Tmin = 0.961, Tmax = 0.993
3389 measured reflections
1924 independent reflections
1262 reflections with I > 2(I)
Rint = 0.020
Data collection: CrysAlis CCD (Oxford Diffraction, 2009); cell refinement: CrysAlis RED (Oxford Diffraction, 2009); data reduction: CrysAlis RED; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: PLATON (Spek, 2009); software used to prepare material for publication: SHELXL97.
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: NG2719 ).
BSS thanks the University Grants Commission, Government of India, New Delhi, for the award of a research fellowship under its faculty improvement program.
Oxford Diffraction (2009). CrysAlis CCD and CrysAlis RED. Oxford Diffraction Ltd, Yarnton, England.
Saraswathi, B. S., Gowda, B. T., Foro, S. & Fuess, H. (2010). Acta Cryst. E66, o325.
Sheldrick, G. M. (2008). Acta Cryst. A64, 112-122.
Spek, A. L. (2009). Acta Cryst. D65, 148-155.