# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' NS-78 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 175.48 _exptl_crystal_F_000 730.00 _reflns_d_resolution_high 0.7238 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.8982 _cell_length_b 11.6936 _cell_length_c 15.9293 _cell_angle_alpha 106.041 _cell_angle_beta 107.408 _cell_angle_gamma 99.040 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2532.37 2610.48 29.75 o 2 0 0 18170.80 18065.89 173.87 o 3 0 0 6604.05 6552.44 69.84 o 4 0 0 3.40 19.87 10.41 o 5 0 0 3019.86 3136.55 42.09 o 6 0 0 1744.83 1788.21 43.62 o 7 0 0 754.47 810.57 42.10 o 8 0 0 132.31 155.55 28.36 o 9 0 0 118.68 123.02 32.50 o 10 0 0 80.79 174.90 77.36 o 11 0 0 6.35 16.07 38.74 o 12 0 0 50.71 30.02 42.89 o -12 1 0 4.86 -10.66 72.42 o -11 1 0 486.23 492.18 62.98 o -10 1 0 18.81 47.28 36.88 o -9 1 0 248.15 156.77 30.24 o -8 1 0 335.11 373.61 35.17 o -7 1 0 1267.53 1171.77 49.30 o -6 1 0 1959.19 1904.77 39.39 o -5 1 0 126.06 178.96 13.54 o -4 1 0 11.03 5.50 8.84 o -3 1 0 5299.63 5309.36 54.84 o -2 1 0 13179.89 12892.72 139.40 o -1 1 0 648.04 708.17 21.43 o 0 1 0 103.51 105.89 4.66 o 1 1 0 1547.72 1366.22 37.06 o 2 1 0 312.76 327.71 13.71 o 3 1 0 2056.32 2144.60 31.37 o 4 1 0 601.88 663.98 17.73 o 5 1 0 1977.26 1958.24 29.29 o 6 1 0 235.32 215.99 20.23 o 7 1 0 341.58 369.24 29.25 o 8 1 0 112.47 142.94 32.31 o 9 1 0 297.66 277.72 40.39 o 10 1 0 781.36 837.05 74.12 o 11 1 0 616.60 599.88 103.84 o 12 1 0 4.81 21.10 78.96 o -12 2 0 0.35 -18.41 38.22 o -11 2 0 56.92 66.26 41.62 o -10 2 0 26.39 77.16 37.93 o -9 2 0 2016.28 2246.47 117.59 o -8 2 0 3.05 -17.63 18.88 o -7 2 0 1433.72 1480.61 49.40 o -6 2 0 2989.98 3015.57 40.63 o -5 2 0 401.92 402.17 16.02 o -4 2 0 2104.55 2165.21 32.39 o -3 2 0 445.13 509.14 16.17 o -2 2 0 23.19 4.84 10.37 o -1 2 0 195.85 200.23 13.18 o 0 2 0 5604.56 5439.08 63.24 o 1 2 0 5852.82 5908.45 59.95 o 2 2 0 1605.91 1628.00 40.18 o 3 2 0 4700.19 4530.88 56.49 o 4 2 0 3.29 25.62 11.71 o 5 2 0 951.68 948.23 25.69 o 6 2 0 249.79 291.72 25.35 o 7 2 0 765.53 736.08 49.52 o 8 2 0 393.17 329.69 39.43 o 9 2 0 151.60 123.94 35.03 o 10 2 0 3.75 70.31 40.38 o 11 2 0 14.68 -13.61 37.33 o 12 2 0 540.45 546.29 72.41 o -13 3 0 65.61 72.10 72.42 o -12 3 0 11.88 16.41 42.14 o -11 3 0 894.85 770.94 72.31 o -10 3 0 152.11 153.70 34.84 o -9 3 0 555.49 614.30 50.36 o -8 3 0 539.44 545.50 43.74 o -7 3 0 187.50 214.36 26.19 o -6 3 0 125.24 190.24 14.48 o -5 3 0 84.81 61.28 11.84 o -4 3 0 3063.08 2881.27 40.78 o -3 3 0 1369.36 1317.47 25.51 o -2 3 0 1716.65 1751.12 25.28 o -1 3 0 8744.48 7951.70 65.23 o 0 3 0 2953.32 3085.43 34.91 o 1 3 0 1876.30 1864.80 23.84 o 2 3 0 987.37 1153.27 25.77 o 3 3 0 748.11 865.96 28.85 o 4 3 0 4468.28 4482.76 62.20 o 5 3 0 923.30 978.27 32.44 o 6 3 0 14.58 -20.92 20.92 o 7 3 0 1.16 -15.03 23.65 o 8 3 0 196.13 174.76 36.03 o 9 3 0 43.76 58.77 34.65 o 10 3 0 736.98 837.85 121.39 o 11 3 0 28.53 12.26 40.58 o -13 4 0 10.49 2.88 44.95 o -12 4 0 442.76 383.36 62.08 o -11 4 0 8.78 2.45 36.30 o -10 4 0 233.89 284.30 63.78 o -9 4 0 141.79 168.53 33.81 o -8 4 0 613.91 599.15 47.38 o -7 4 0 490.74 460.08 33.72 o -6 4 0 2241.33 2074.90 38.71 o -5 4 0 225.51 230.65 15.90 o -4 4 0 476.40 521.70 22.80 o -3 4 0 8281.13 8040.80 75.96 o -2 4 0 248.09 314.08 12.61 o -1 4 0 32.30 17.59 6.40 o 0 4 0 201.58 242.40 10.84 o 1 4 0 681.26 784.73 18.74 o 2 4 0 3713.74 3376.29 40.45 o 3 4 0 2520.27 2536.41 33.35 o 4 4 0 256.18 227.10 21.10 o 5 4 0 416.42 374.56 27.24 o 6 4 0 2.08 13.78 23.21 o 7 4 0 776.87 810.50 60.35 o 8 4 0 810.03 755.84 75.02 o 9 4 0 96.48 106.41 35.01 o 10 4 0 202.31 180.14 48.05 o 11 4 0 0.66 59.66 77.52 o -12 5 0 2.72 7.17 41.56 o -11 5 0 17.88 -28.96 35.42 o -10 5 0 282.90 284.56 41.97 o -9 5 0 1141.12 1125.01 78.62 o -8 5 0 1099.17 1071.20 60.23 o -7 5 0 18.68 51.18 28.28 o -6 5 0 69.90 67.94 14.00 o -5 5 0 8855.45 8846.21 89.55 o -4 5 0 3981.63 3906.36 62.99 o -2 5 0 572.74 636.75 20.73 o -1 5 0 2.02 -0.86 9.23 o 0 5 0 886.63 892.15 21.24 o 1 5 0 846.76 798.77 21.35 o 2 5 0 175.89 210.40 14.05 o 3 5 0 133.28 136.46 13.17 o 4 5 0 15.81 -2.67 13.85 o 5 5 0 194.28 173.51 30.44 o 6 5 0 597.93 675.32 50.67 o 7 5 0 101.19 107.91 31.50 o 8 5 0 52.93 87.21 33.26 o 9 5 0 0.74 -15.25 41.94 o 10 5 0 4.63 -60.93 60.93 o -12 6 0 499.20 605.96 69.30 o -11 6 0 0.90 33.81 31.76 o -10 6 0 70.41 99.11 34.54 o -9 6 0 340.14 352.55 51.14 o -8 6 0 181.70 122.28 29.94 o -7 6 0 1554.17 1496.36 72.52 o -6 6 0 1456.83 1515.62 49.24 o -5 6 0 255.08 237.32 18.67 o -4 6 0 1149.12 1094.37 24.53 o -3 6 0 137.16 158.12 13.31 o -2 6 0 1313.83 1358.59 27.83 o -1 6 0 1012.95 927.38 22.88 o 0 6 0 3450.32 3432.83 41.85 o 1 6 0 345.37 372.69 16.44 o 2 6 0 28.02 31.50 10.32 o 3 6 0 10.57 45.72 14.48 o 4 6 0 1054.70 990.35 42.10 o 5 6 0 1605.89 1556.27 87.47 o 6 6 0 1562.97 1641.37 69.66 o 7 6 0 20.77 39.39 29.90 o 8 6 0 36.43 13.88 30.05 o 9 6 0 84.71 65.97 69.07 o 10 6 0 62.89 -30.94 73.37 o -12 7 0 37.22 95.73 46.86 o -11 7 0 183.22 153.00 37.17 o -10 7 0 196.03 263.12 36.87 o -9 7 0 1084.75 956.15 61.21 o -8 7 0 2.60 57.04 27.74 o -7 7 0 699.36 613.46 47.02 o -6 7 0 16.37 1.52 18.98 o -5 7 0 522.24 575.16 29.49 o -4 7 0 1659.79 1685.48 42.14 o -3 7 0 494.84 484.63 20.35 o -2 7 0 7379.72 6956.28 73.81 o -1 7 0 153.04 175.83 12.24 o 0 7 0 817.36 807.62 22.26 o 1 7 0 126.41 164.67 13.93 o 2 7 0 1071.68 1074.40 30.85 o 3 7 0 998.26 972.35 38.18 o 4 7 0 884.82 903.50 41.47 o 5 7 0 124.46 111.40 47.09 o 6 7 0 448.18 352.35 40.95 o 7 7 0 563.75 486.78 70.30 o 8 7 0 59.03 9.38 45.01 o 9 7 0 15.79 -0.76 49.78 o -12 8 0 33.79 112.93 70.50 o -11 8 0 276.11 210.19 57.74 o -10 8 0 5.66 15.47 28.32 o -9 8 0 451.12 505.08 52.20 o -8 8 0 625.56 574.37 49.34 o -7 8 0 1.53 -17.81 23.51 o -6 8 0 0.85 39.46 22.61 o -5 8 0 52.23 54.04 20.22 o -4 8 0 1254.16 1234.26 41.46 o -3 8 0 111.35 124.60 19.05 o -2 8 0 246.98 208.30 20.89 o -1 8 0 495.40 512.65 24.06 o 0 8 0 20.44 28.02 12.09 o 1 8 0 2056.10 2058.57 42.71 o 2 8 0 10.50 18.93 17.41 o 3 8 0 50.62 49.66 19.78 o 4 8 0 161.19 220.26 32.00 o 5 8 0 590.43 573.33 67.55 o 6 8 0 1008.98 1014.61 150.74 o 7 8 0 84.39 4.75 54.07 o 8 8 0 14.38 0.37 49.84 o 9 8 0 27.73 19.78 76.56 o -12 9 0 57.90 47.85 67.31 o -11 9 0 829.63 799.12 71.58 o -10 9 0 501.15 431.00 53.55 o -9 9 0 46.35 38.58 38.45 o -8 9 0 45.33 -25.61 45.66 o -7 9 0 375.80 380.08 41.06 o -6 9 0 852.26 955.19 48.38 o -5 9 0 751.21 774.03 42.59 o -4 9 0 110.40 68.01 22.33 o -3 9 0 507.43 568.71 33.90 o -2 9 0 937.95 1005.32 40.49 o -1 9 0 246.44 260.06 43.35 o 0 9 0 102.51 124.09 18.13 o 1 9 0 330.48 357.17 26.45 o 2 9 0 1010.40 941.07 50.47 o 3 9 0 1254.51 1229.70 87.35 o 4 9 0 0.14 20.53 43.07 o 5 9 0 113.52 58.75 48.84 o 6 9 0 0.92 -25.89 42.92 o 7 9 0 35.18 -15.92 49.74 o 8 9 0 267.39 158.32 63.48 o -11 10 0 21.57 -10.45 38.29 o -10 10 0 90.09 46.93 35.88 o -9 10 0 1.63 -33.25 33.25 o -8 10 0 77.83 93.49 67.47 o -7 10 0 107.75 51.12 37.10 o -6 10 0 79.92 39.90 35.81 o -5 10 0 155.15 188.75 35.74 o -4 10 0 16.26 -6.34 31.06 o -3 10 0 0.40 -1.65 28.12 o -2 10 0 274.90 220.13 52.33 o -1 10 0 97.65 103.08 28.81 o 0 10 0 1027.18 1150.20 47.89 o 1 10 0 1766.78 1816.47 77.33 o 2 10 0 480.03 383.73 58.14 o 3 10 0 167.54 207.42 53.09 o 4 10 0 65.11 82.05 47.55 o 5 10 0 35.10 105.78 49.13 o 6 10 0 328.52 319.53 67.29 o 7 10 0 44.08 17.03 55.45 o -11 11 0 370.10 317.16 66.68 o -10 11 0 380.29 238.11 50.52 o -9 11 0 275.06 280.12 47.47 o -8 11 0 153.68 262.32 50.75 o -7 11 0 6.58 -23.17 32.71 o -6 11 0 17.88 -4.56 31.60 o -5 11 0 534.54 536.70 62.85 o -4 11 0 160.97 143.31 43.22 o -3 11 0 3.04 5.51 44.39 o -2 11 0 10.01 -17.02 26.13 o -1 11 0 1269.67 1375.90 67.27 o 0 11 0 137.43 109.59 35.76 o 1 11 0 307.02 250.79 52.73 o 2 11 0 76.34 38.06 43.90 o 3 11 0 65.55 7.07 44.55 o 4 11 0 1.93 -26.58 46.44 o 5 11 0 18.05 8.46 51.42 o 6 11 0 0.79 65.74 57.17 o -10 12 0 0.99 2.13 44.07 o -9 12 0 40.94 49.65 40.54 o -8 12 0 149.22 112.93 48.27 o -7 12 0 842.80 896.79 82.64 o -6 12 0 1057.90 1153.53 88.45 o -5 12 0 1.89 -3.22 34.51 o -4 12 0 301.04 291.46 45.02 o -3 12 0 304.13 257.34 55.77 o -2 12 0 47.85 18.41 29.16 o -1 12 0 795.38 826.69 64.53 o 0 12 0 69.58 59.50 42.97 o 1 12 0 0.01 8.81 42.69 o 2 12 0 21.58 38.35 45.23 o 3 12 0 157.36 83.77 50.63 o 4 12 0 163.14 121.50 55.55 o 5 12 0 0.07 23.86 56.27 o -9 13 0 396.73 377.85 67.81 o -8 13 0 930.10 1153.48 98.45 o -7 13 0 14.85 27.93 34.24 o -6 13 0 75.28 38.75 41.02 o -5 13 0 57.86 78.15 36.53 o -4 13 0 172.97 135.20 62.55 o -3 13 0 1854.41 1943.17 93.57 o -2 13 0 0.58 6.58 36.20 o -1 13 0 138.41 192.46 66.83 o 0 13 0 7.35 4.42 43.49 o 1 13 0 6.28 -14.32 43.68 o 2 13 0 191.53 270.36 62.65 o 3 13 0 67.32 117.28 55.67 o -8 14 0 116.41 65.29 46.54 o -7 14 0 85.80 119.53 50.98 o -6 14 0 584.50 598.68 74.67 o -5 14 0 236.45 318.43 71.07 o -4 14 0 43.44 53.20 40.06 o -3 14 0 263.51 256.39 49.85 o -2 14 0 50.69 94.59 87.89 o -1 14 0 82.33 34.20 149.30 o 0 14 0 19.02 48.55 49.60 o 1 14 0 59.21 166.32 56.57 o 2 14 0 80.32 27.56 58.70 o -6 15 0 3.61 90.77 51.87 o -5 15 0 97.93 102.42 50.18 o -4 15 0 622.88 622.88 79.09 o -3 15 0 0.47 17.25 45.16 o -2 15 0 106.44 12.72 82.63 o -1 15 0 85.76 145.65 57.69 o 0 -15 1 2.72 -6.99 46.01 o 1 -15 1 18.84 83.85 89.33 o 2 -15 1 253.38 226.97 61.64 o 3 -15 1 243.35 253.24 50.26 o 4 -15 1 323.87 437.14 70.79 o 5 -15 1 184.19 109.03 52.10 o 6 -15 1 391.32 491.88 75.82 o -2 -14 1 42.29 -8.66 48.04 o -1 -14 1 30.73 92.81 51.95 o 0 -14 1 37.32 20.41 47.21 o 1 -14 1 107.03 135.60 62.53 o 2 -14 1 20.72 -23.58 34.54 o 3 -14 1 8.80 -3.97 35.56 o 4 -14 1 549.48 601.71 81.59 o 5 -14 1 117.10 103.87 42.75 o 6 -14 1 0.08 -37.44 37.44 o 7 -14 1 69.54 25.10 42.92 o 8 -14 1 71.50 37.29 50.27 o -4 -13 1 18.61 55.14 55.49 o -3 -13 1 222.12 152.27 107.99 o -2 -13 1 8.14 21.93 46.89 o -1 -13 1 83.08 46.01 47.95 o 0 -13 1 348.91 341.08 60.30 o 1 -13 1 47.38 76.90 45.46 o 2 -13 1 885.75 886.00 69.39 o 3 -13 1 1278.54 1260.22 93.70 o 4 -13 1 0.24 -34.38 34.38 o 5 -13 1 108.31 89.00 46.69 o 6 -13 1 58.94 14.77 40.59 o 7 -13 1 434.91 478.05 70.02 o 8 -13 1 35.05 45.42 86.14 o 9 -13 1 30.80 102.76 52.80 o -5 -12 1 97.92 134.39 60.13 o -4 -12 1 3.61 -45.76 57.10 o -3 -12 1 369.68 332.54 63.31 o -2 -12 1 70.41 -13.31 66.68 o -1 -12 1 51.81 37.50 45.33 o 0 -12 1 362.20 543.86 66.90 o 1 -12 1 81.82 56.81 49.17 o 2 -12 1 0.48 9.86 41.79 o 3 -12 1 90.09 108.79 41.52 o 4 -12 1 223.27 244.24 50.72 o 5 -12 1 427.12 414.87 59.69 o 6 -12 1 114.24 104.96 43.27 o 7 -12 1 298.47 245.71 54.70 o 8 -12 1 10.30 -36.14 36.14 o 9 -12 1 13.40 11.03 40.94 o 10 -12 1 217.04 208.47 60.21 o -6 -11 1 20.58 -32.12 50.19 o -5 -11 1 0.31 -42.96 45.42 o -4 -11 1 24.01 -42.07 42.07 o -3 -11 1 282.33 340.92 60.10 o -2 -11 1 545.54 563.33 67.25 o -1 -11 1 842.01 641.11 69.62 o 0 -11 1 538.14 588.62 76.63 o 1 -11 1 204.44 261.20 58.70 o 2 -11 1 32.92 -3.94 33.79 o 3 -11 1 16.58 -24.06 34.61 o 4 -11 1 14.27 -11.11 29.99 o 5 -11 1 1.63 7.43 32.93 o 6 -11 1 277.62 239.97 49.60 o 7 -11 1 85.83 111.80 129.04 o 8 -11 1 315.43 407.68 61.75 o 9 -11 1 723.03 792.90 80.25 o 10 -11 1 23.58 14.69 56.32 o 11 -11 1 5.10 3.26 45.68 o -7 -10 1 432.83 505.41 102.72 o -6 -10 1 138.06 119.48 54.32 o -5 -10 1 0.92 -29.36 44.04 o -4 -10 1 190.46 124.12 74.97 o -3 -10 1 240.93 252.52 53.28 o -2 -10 1 1207.33 1096.70 53.91 o -1 -10 1 1439.86 1363.87 57.93 o 0 -10 1 0.98 9.35 18.79 o 1 -10 1 941.79 969.26 50.81 o 2 -10 1 249.06 280.54 30.35 o 3 -10 1 213.55 207.05 31.54 o 4 -10 1 106.79 138.48 28.65 o 5 -10 1 412.72 439.51 41.76 o 6 -10 1 162.77 150.46 34.59 o 7 -10 1 1438.49 1413.38 72.04 o 8 -10 1 22.74 31.14 31.35 o 9 -10 1 25.24 10.02 50.95 o 10 -10 1 7.04 25.45 44.07 o 11 -10 1 493.55 482.41 77.82 o -8 -9 1 53.13 42.96 78.16 o -7 -9 1 1.53 -43.84 45.59 o -6 -9 1 8.63 -39.56 41.06 o -5 -9 1 121.29 76.34 31.26 o -4 -9 1 221.86 187.64 55.36 o -3 -9 1 250.48 255.93 35.35 o -2 -9 1 56.41 53.44 23.12 o -1 -9 1 319.64 309.73 33.33 o 0 -9 1 1030.19 933.03 38.34 o 1 -9 1 215.82 241.29 26.18 o 2 -9 1 119.16 100.96 19.65 o 3 -9 1 597.16 532.23 41.49 o 4 -9 1 1142.37 1227.22 56.18 o 5 -9 1 23.24 57.46 26.25 o 6 -9 1 8.98 -0.24 30.73 o 7 -9 1 105.24 56.40 30.66 o 8 -9 1 26.12 70.99 31.70 o 9 -9 1 710.21 771.89 59.35 o 10 -9 1 1012.84 1147.88 79.02 o 11 -9 1 88.48 123.87 50.42 o 12 -9 1 229.76 249.47 83.90 o -9 -8 1 6.70 67.31 80.07 o -8 -8 1 93.58 172.17 67.63 o -7 -8 1 262.04 255.66 42.21 o -6 -8 1 58.00 50.77 39.84 o -5 -8 1 91.36 68.07 31.32 o -4 -8 1 79.62 92.67 29.72 o -3 -8 1 191.24 186.14 31.64 o -2 -8 1 826.21 833.83 34.37 o -1 -8 1 1371.97 1423.57 36.18 o 0 -8 1 434.57 467.73 25.27 o 1 -8 1 1751.86 1761.19 37.88 o 2 -8 1 2468.71 2337.99 47.79 o 3 -8 1 936.07 903.54 38.80 o 4 -8 1 1713.68 1656.83 52.27 o 5 -8 1 391.63 400.68 40.43 o 6 -8 1 9.39 -49.32 49.32 o 7 -8 1 81.47 110.28 42.69 o 8 -8 1 16.34 25.74 30.05 o 9 -8 1 185.20 196.64 38.34 o 10 -8 1 345.54 382.75 49.13 o 11 -8 1 94.51 134.17 47.77 o 12 -8 1 67.64 93.29 68.11 o -9 -7 1 31.19 82.04 61.41 o -8 -7 1 124.83 141.60 38.30 o -7 -7 1 26.71 4.32 28.83 o -6 -7 1 17.51 50.21 30.72 o -5 -7 1 1817.28 1879.99 111.06 o -4 -7 1 187.74 162.04 30.28 o -3 -7 1 516.40 590.94 29.92 o -2 -7 1 8.73 2.98 13.41 o -1 -7 1 10.87 6.32 10.18 o 0 -7 1 4820.20 4383.08 47.80 o 1 -7 1 1312.96 1369.15 30.05 o 2 -7 1 102.81 67.35 11.34 o 3 -7 1 4914.97 4930.37 55.35 o 4 -7 1 197.92 169.92 18.17 o 5 -7 1 238.60 281.29 28.90 o 6 -7 1 24.13 -8.16 22.70 o 7 -7 1 4.50 15.60 25.56 o 8 -7 1 131.52 193.30 60.91 o 9 -7 1 1192.35 1328.19 89.71 o 10 -7 1 55.90 45.82 33.29 o 11 -7 1 140.31 189.31 49.74 o 12 -7 1 221.53 301.65 93.31 o -10 -6 1 4.39 -56.15 68.91 o -9 -6 1 39.46 42.58 34.64 o -8 -6 1 537.91 565.63 61.89 o -7 -6 1 635.93 715.63 54.29 o -6 -6 1 269.06 271.53 37.60 o -5 -6 1 1652.27 1648.27 62.44 o -4 -6 1 33.20 23.52 16.53 o -3 -6 1 1832.29 1658.51 43.44 o -2 -6 1 1590.08 1503.52 28.76 o -1 -6 1 47.92 48.42 10.68 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