Acta Cryst. (2010). E66, m368  [ doi:10.1107/S1600536810007749 ]

Poly[(dimethylformamide)(₄-2,2'-sulfanediyldibenzoato)nickel(II)]

J.-B. Xie

Online 6 March 2010

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.005 Å
• R factor = 0.036
• wR factor = 0.079
• Data-to-parameter ratio = 14.7

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ni1    --  O5      ..       6.03 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ni1    --  O2_d    ..       6.52 su   
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        Ni1     
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         15      
PLAT041_ALERT_1_C Calc. and Reported SumFormula    Strings  Differ          ?
PLAT042_ALERT_1_C Calc. and Reported MoietyFormula Strings  Differ          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       2.00 Ratio
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         14      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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