Acta Cryst. (2010). E66, m354  [ doi:10.1107/S1600536810007415 ]

Bis(N-isopropyl-N-methyldithiocarbamato-²S,S')diphenyltin(IV)

A. F. Muthalib, I. Baba, Y. Farina and S. W. Ng

Online 3 March 2010

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• R factor = 0.026
• wR factor = 0.089
• Data-to-parameter ratio = 20.6

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low .......       0.96      
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Sn1    --  S2      ..      13.37 su   
PLAT919_ALERT_3_B Reflection(s) # Likely Affected by the Beamstop           1      

Alert level C
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Sn1    --  S1      ..       6.46 su   
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C9     
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         59      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         31      
PLAT950_ALERT_1_C Reported and Calculated Hmax Values Differ by ..          2      

Alert level G
REFLT03_ALERT_1_G ALERT: Expected hkl max differ from CIF values
           From the CIF: _diffrn_reflns_theta_max           27.50
           From the CIF: _reflns_number_total               2785
           From the CIF: _diffrn_reflns_limit_ max hkl   22.   11.   18.
           From the CIF: _diffrn_reflns_limit_ min hkl  -22.  -11.  -13.
           TEST1: Expected hkl limits for theta max
           Calculated maximum hkl   24.   11.   18.
           Calculated minimum hkl  -24.  -11.  -18.
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported   _diffrn_ambient_temperature        293 K    

   0 ALERT level A = In general: serious problem
   3 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   3 ALERT level G = General alerts; check

   4 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check


checkCIF publication errors

Alert level G
PUBL013_ALERT_1_G The _publ_section_comment (discussion of study) is
            missing. This is required for a full paper submission (but is
            optional for an electronic paper).

   0 ALERT level A = Data missing that is essential or data in wrong format
   1 ALERT level G = General alerts. Data that may be required is missing

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