(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2010). E66, o958 [ doi:10.1107/S1600536810011013 ]

N-(4-Chlorophenyl)ethanimidamide

N. Boechat, W. B. Kover, S. B. Ferreira, S. M. S. V. Wardell, J. L. Wardell and E. R. T. Tiekink

Online 27 March 2010

Key indicators

Single-crystal X-ray study
T = 120 K
Mean (C-C) = 0.004 Å
R factor = 0.047
wR factor = 0.150
Data-to-parameter ratio = 18.0

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT919_ALERT_3_B Reflection(s) # Likely Affected by the Beamstop           1      

Alert level C
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          1      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600          3      

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   2 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check


checkCIF publication errors

Alert level A
PUBL024_ALERT_1_A The number of authors is greater than 5.
              Please specify the role of each of the co-authors
              for your paper.

Author Response: The contribution of the authors to this submission is as follows:

 Boechat      - co-supervisor of student
 Kover        - co-supervisor of student
 Ferreira     - Ph.D. student
 Wardell, S.  - preliminary crystallographic analysis
 Wardell, J.  - spectroscopy and write-up
 Tiekink      - final crystallography and write-up


   1 ALERT level A = Data missing that is essential or data in wrong format
   0 ALERT level G = General alerts. Data that may be required is missing