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Acta Cryst. (2010). E66, m351 [ doi:10.1107/S1600536810007014 ]
Bis(acetato-![[kappa]](/logos/entities/kappa_rmgif.gif)
2O,O')diphenyl(pyridine-N)tin(IV)
Online 3 March 2010
Key indicators
- Single-crystal X-ray study
- T = 296 K
- Mean
![[sigma]](http://journals.iucr.org/logos/entities/sigma_rmgif.gif)
(C-C) = 0.007 Å
- R factor = 0.033
- wR factor = 0.067
- Data-to-parameter ratio = 14.8
checkCIF/PLATON results
No syntax errors found
Alert level B
PLAT922_ALERT_1_B wR2 * 100.0 in the CIF and FCF Differ by ....... -1.27
PLAT923_ALERT_1_B S values in the CIF and FCF Differ by ....... 0.03
PLAT927_ALERT_1_B Reported and Calculated wR2 * 100.0 Differ by . -1.28
Alert level C
PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd. # 1
C21 H21 N O4 Sn
Alert level G
PLAT128_ALERT_4_G Non-standard setting of Space-group P21/c .... P21/n
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 45
C7 -SN1 -C1 -C6 -58.10 1.90 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 53
C7 -SN1 -C1 -C2 120.10 1.70 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 69
C1 -SN1 -C7 -C8 -32.00 2.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 77
C1 -SN1 -C7 -C12 151.20 1.70 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 119
C1 -SN1 -C18 -C19 -150.00 10.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 120
C7 -SN1 -C18 -C19 34.00 10.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 121
O3 -SN1 -C18 -C19 -58.00 10.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 122
O1 -SN1 -C18 -C19 -58.00 9.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 123
O2 -SN1 -C18 -C19 124.00 10.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 124
O4 -SN1 -C18 -C19 -52.00 10.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 125
N1 -SN1 -C18 -C19 122.00 10.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 126
C20 -SN1 -C18 -C19 -58.00 10.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 145
C1 -SN1 -C20 -C21 32.00 5.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 146
C7 -SN1 -C20 -C21 -152.00 5.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 147
O3 -SN1 -C20 -C21 -61.00 5.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 148
O1 -SN1 -C20 -C21 -61.00 5.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 149
O2 -SN1 -C20 -C21 -56.00 5.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 150
O4 -SN1 -C20 -C21 121.00 5.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 151
N1 -SN1 -C20 -C21 118.00 5.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 152
C18 -SN1 -C20 -C21 -61.00 5.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 193
C28 -SN2 -C22 -C27 -20.50 1.80 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 200
C28 -SN2 -C22 -C23 155.20 1.50 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 215
C22 -SN2 -C28 -C33 -96.90 1.60 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 222
C22 -SN2 -C28 -C29 81.90 1.60 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 265
C22 -SN2 -C41 -C42 68.00 16.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 266
C28 -SN2 -C41 -C42 -114.00 16.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 267
O6 -SN2 -C41 -C42 -22.00 16.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 268
O8 -SN2 -C41 -C42 -21.00 16.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 269
O7 -SN2 -C41 -C42 159.00 16.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 270
O5 -SN2 -C41 -C42 -25.00 17.00 1.555 1.555 1.555 1.555
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 271
N2 -SN2 -C41 -C42 158.00 16.00 1.555 1.555 1.555 1.555
0 ALERT level A = In general: serious problem
3 ALERT level B = Potentially serious problem
1 ALERT level C = Check and explain
32 ALERT level G = General alerts; check
3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
0 ALERT type 2 Indicator that the structure model may be wrong or deficient
0 ALERT type 3 Indicator that the structure quality may be low
33 ALERT type 4 Improvement, methodology, query or suggestion
0 ALERT type 5 Informative message, check
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