# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Template texray.inf' _shelx_refln_list_code 4 _shelx_F_calc_maximum 657.88 _exptl_crystal_F_000 2704.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 19.1964 _cell_length_b 11.7855 _cell_length_c 26.0594 _cell_angle_alpha 90.000 _cell_angle_beta 107.328 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1175.83 -6.84 4.56 o 2 0 0 218594.59 218087.47 10363.88 o 3 0 0 238.51 242.01 47.14 o 4 0 0 253269.98 243567.34 12453.62 o 5 0 0 5519.36 5660.28 258.87 o 6 0 0 105.45 69.58 51.48 o 7 0 0 38471.07 40293.70 1411.42 o 8 0 0 41777.48 41354.42 1948.48 o 9 0 0 37085.89 39164.42 1283.27 o 10 0 0 122444.06 129990.30 3684.57 o 11 0 0 24.13 513.16 108.70 o 12 0 0 44489.67 43765.88 1322.48 o 13 0 0 26558.20 26759.61 865.49 o 14 0 0 25240.03 27417.05 898.38 o 15 0 0 69401.25 74415.47 2762.79 o 16 0 0 758.20 1525.59 255.73 o 17 0 0 41776.20 43014.44 2561.37 o 18 0 0 1087.67 1933.85 560.42 o 19 0 0 16395.54 18253.22 1452.36 o 20 0 0 195.24 797.22 517.01 o 21 0 0 496.91 311.78 528.85 o 22 0 0 2275.28 3125.74 824.85 o 23 0 0 2882.93 5260.87 1010.34 o 1 1 0 29235.61 22137.14 4063.07 o 2 1 0 155.22 136.01 23.56 o 3 1 0 81197.51 81699.13 1782.85 o 4 1 0 1716.59 1709.88 59.25 o 5 1 0 105370.18 110655.12 2198.05 o 6 1 0 217.57 173.42 37.95 o 7 1 0 39443.45 39756.10 817.10 o 8 1 0 34342.57 35834.64 750.56 o 9 1 0 8069.00 8398.81 220.38 o 10 1 0 37557.43 39037.14 827.26 o 11 1 0 37.29 162.35 68.00 o 12 1 0 69118.88 72826.14 1662.95 o 13 1 0 21095.61 22863.51 602.86 o 14 1 0 42202.66 43006.46 1162.27 o 15 1 0 4398.23 5065.70 342.19 o 16 1 0 274.27 123.14 141.21 o 17 1 0 3532.56 3264.39 507.14 o 18 1 0 6007.97 6556.81 598.60 o 19 1 0 743.24 1088.22 518.98 o 20 1 0 6698.93 8738.26 1148.47 o 21 1 0 330.58 715.60 446.41 o 22 1 0 13898.92 16029.91 1082.62 o 23 1 0 858.27 1757.42 1253.06 o 0 2 0 87762.71 92648.03 2586.60 o 1 2 0 606.25 641.82 77.99 o 2 2 0 7854.70 7871.21 191.92 o 3 2 0 219.32 228.87 79.17 o 4 2 0 169.29 177.59 34.73 o 5 2 0 5366.45 5587.91 160.21 o 6 2 0 0.03 56.84 60.94 o 7 2 0 4420.56 5070.95 299.90 o 8 2 0 5672.72 5399.64 178.57 o 9 2 0 1787.29 1969.23 106.00 o 10 2 0 34441.52 36013.98 852.79 o 11 2 0 363.22 462.24 86.91 o 12 2 0 11050.23 11037.38 337.30 o 13 2 0 19364.22 19321.36 708.68 o 14 2 0 1700.58 1780.75 194.57 o 15 2 0 10475.54 10453.68 584.75 o 16 2 0 2898.63 3017.37 246.96 o 17 2 0 4676.40 4917.64 309.88 o 18 2 0 2.78 -164.38 186.25 o 19 2 0 3234.40 2939.40 490.85 o 20 2 0 8.51 299.62 334.33 o 21 2 0 57.32 145.06 380.85 o 22 2 0 11.02 -225.63 387.43 o 23 2 0 711.95 1123.23 498.41 o 1 3 0 13.61 -16.01 34.20 o 2 3 0 127.37 159.65 35.99 o 3 3 0 7476.56 7540.36 179.60 o 4 3 0 2043.61 2220.07 110.96 o 5 3 0 5155.77 5505.73 188.27 o 6 3 0 4303.23 4763.65 189.95 o 7 3 0 96.03 118.98 72.86 o 8 3 0 2177.61 2360.26 144.69 o 9 3 0 764.38 876.60 116.28 o 10 3 0 8312.68 8032.38 253.38 o 11 3 0 3467.07 3434.42 157.19 o 12 3 0 4976.23 5329.01 359.15 o 13 3 0 718.13 730.58 159.01 o 14 3 0 1094.66 839.16 174.00 o 15 3 0 4623.23 5225.54 302.44 o 16 3 0 35.11 9.16 156.38 o 17 3 0 989.46 1177.99 213.47 o 18 3 0 77.51 7.94 210.22 o 19 3 0 18.29 -192.83 205.93 o 20 3 0 1285.38 980.26 381.10 o 21 3 0 1101.33 990.66 424.26 o 22 3 0 93.56 464.88 432.13 o 23 3 0 254.20 18.28 426.41 o 0 4 0 77990.80 82784.03 2339.46 o 1 4 0 3875.92 3893.02 119.42 o 2 4 0 93081.45 99150.55 2794.38 o 3 4 0 2271.73 2092.65 82.56 o 4 4 0 2690.46 3247.21 127.43 o 5 4 0 1652.31 1671.31 119.63 o 6 4 0 32702.55 34882.97 810.86 o 7 4 0 24340.46 24684.89 676.99 o 8 4 0 19721.06 20448.51 586.08 o 9 4 0 7785.70 8224.72 308.59 o 10 4 0 11474.87 11731.34 405.43 o 11 4 0 8353.75 8232.27 344.64 o 12 4 0 16070.50 14955.47 503.54 o 13 4 0 7837.32 7893.17 354.83 o 14 4 0 161.06 103.40 166.39 o 15 4 0 12831.75 12475.46 491.33 o 16 4 0 1752.90 2079.43 241.72 o 17 4 0 13934.22 13202.46 786.39 o 18 4 0 1740.98 1836.99 254.74 o 19 4 0 3689.01 3969.95 400.79 o 20 4 0 509.61 523.34 264.47 o 21 4 0 17.11 149.37 398.67 o 22 4 0 80.54 -394.83 501.22 o 1 5 0 21341.47 22228.54 482.27 o 2 5 0 3750.74 3619.22 136.61 o 3 5 0 160338.14 170326.47 3382.91 o 4 5 0 4073.93 4663.10 144.67 o 5 5 0 136214.63 143660.13 3059.13 o 6 5 0 41.53 36.40 72.24 o 7 5 0 54967.61 53689.82 1229.78 o 8 5 0 10159.24 9936.20 353.89 o 9 5 0 12101.16 12388.60 425.18 o 10 5 0 57919.50 58929.17 1534.25 o 11 5 0 212.64 208.56 137.11 o 12 5 0 63255.64 59312.51 1571.80 o 13 5 0 9507.79 8829.70 522.94 o 14 5 0 13638.13 12618.96 490.90 o 15 5 0 9320.88 9320.88 425.41 o 16 5 0 1016.01 777.68 206.44 o 17 5 0 2830.68 3392.03 306.88 o 18 5 0 7874.63 8756.63 461.68 o 19 5 0 203.79 489.82 270.34 o 20 5 0 12340.77 12914.21 752.75 o 21 5 0 690.26 544.17 441.97 o 22 5 0 10335.60 9674.50 888.94 o 0 6 0 149951.34 154093.73 4343.71 o 1 6 0 1123.61 1281.75 89.45 o 2 6 0 54653.54 53937.32 1113.00 o 3 6 0 4099.61 4233.07 214.11 o 4 6 0 10114.82 10495.94 296.55 o 5 6 0 28750.01 29349.54 693.45 o 6 6 0 57.37 81.97 87.27 o 7 6 0 18818.84 19000.74 494.11 o 8 6 0 19678.94 20852.71 492.12 o 9 6 0 7778.96 7962.45 333.62 o 10 6 0 23152.30 22236.92 1205.38 o 11 6 0 155.31 417.77 155.05 o 12 6 0 17176.95 16701.84 576.04 o 13 6 0 15169.35 15099.20 552.89 o 14 6 0 1463.96 1457.89 221.94 o 15 6 0 33489.71 33386.16 1014.45 o 16 6 0 28.32 17.23 194.65 o 17 6 0 22229.94 21497.42 1053.85 o 18 6 0 163.92 305.86 231.63 o 19 6 0 7554.87 6709.30 528.70 o 20 6 0 25.42 -173.71 301.41 o 21 6 0 803.70 698.35 334.19 o 1 7 0 11041.45 11196.58 291.59 o 2 7 0 232.16 336.30 84.01 o 3 7 0 19291.85 18600.90 621.18 o 4 7 0 6900.59 6964.97 280.65 o 5 7 0 40673.75 44286.71 1165.53 o 6 7 0 7568.63 8202.99 305.28 o 7 7 0 34382.16 34316.88 826.83 o 8 7 0 14055.83 12800.67 396.83 o 9 7 0 35191.35 34515.93 1080.33 o 10 7 0 6445.13 6617.77 288.81 o 11 7 0 9815.21 9740.18 415.72 o 12 7 0 7506.84 7191.45 523.51 o 13 7 0 599.45 968.18 204.61 o 14 7 0 240.58 401.24 196.28 o 15 7 0 351.35 129.72 196.39 o 16 7 0 708.28 827.40 245.86 o 17 7 0 34.54 92.64 219.21 o 18 7 0 3348.36 3804.31 470.53 o 19 7 0 499.60 31.91 298.49 o 20 7 0 4803.04 4741.15 623.55 o 21 7 0 1344.27 967.23 375.62 o 0 8 0 200.36 24.12 121.26 o 1 8 0 25189.63 25403.57 581.11 o 2 8 0 61.95 123.24 89.64 o 3 8 0 30774.77 29774.27 921.30 o 4 8 0 715.58 562.26 134.03 o 5 8 0 8963.49 8932.24 350.54 o 6 8 0 1911.10 1782.78 185.83 o 7 8 0 196.08 380.18 143.30 o 8 8 0 411.87 506.04 138.14 o 9 8 0 5289.53 4818.64 248.54 o 10 8 0 1809.19 1912.62 223.53 o 11 8 0 4340.19 4188.81 255.25 o 12 8 0 1546.41 1350.74 185.11 o 13 8 0 3018.43 3298.15 259.26 o 14 8 0 777.88 517.81 196.38 o 15 8 0 1189.87 1418.95 264.89 o 16 8 0 2482.23 2649.92 316.74 o 17 8 0 21.44 170.68 239.75 o 18 8 0 6298.03 6366.92 466.30 o 19 8 0 818.35 785.74 342.56 o 20 8 0 322.89 181.15 314.34 o 1 9 0 4332.00 4415.00 193.06 o 2 9 0 711.13 761.15 121.77 o 3 9 0 14654.85 13489.58 461.10 o 4 9 0 24050.60 23973.58 762.19 o 5 9 0 13497.07 13248.16 474.86 o 6 9 0 14354.77 14457.86 548.57 o 7 9 0 775.71 745.56 177.50 o 8 9 0 1781.35 2010.19 218.33 o 9 9 0 2147.95 2432.42 238.01 o 10 9 0 1950.10 1866.32 198.11 o 11 9 0 6040.52 5955.02 307.49 o 12 9 0 6319.92 5979.64 314.57 o 13 9 0 3654.07 3501.14 270.54 o 14 9 0 6284.73 5916.29 341.88 o 15 9 0 5138.06 4881.25 329.75 o 16 9 0 916.87 966.69 228.67 o 17 9 0 960.33 1225.41 264.89 o 18 9 0 173.69 340.51 257.59 o 19 9 0 2850.07 3959.51 435.86 o 0 10 0 16701.89 17394.66 650.53 o 1 10 0 2654.73 2835.25 176.45 o 2 10 0 19682.50 19898.45 628.76 o 3 10 0 4677.26 4859.95 277.29 o 4 10 0 2055.74 2039.18 210.51 o 5 10 0 3742.37 3577.57 257.74 o 6 10 0 5253.02 5387.48 307.87 o 7 10 0 12858.01 12778.85 488.56 o 8 10 0 14097.14 14896.27 548.64 o 9 10 0 14023.57 12617.24 503.64 o 10 10 0 7029.75 6109.78 361.73 o 11 10 0 2777.46 2991.82 288.47 o 12 10 0 2542.09 2687.92 256.92 o 13 10 0 549.25 435.82 190.39 o 14 10 0 72.82 337.18 193.60 o 15 10 0 5859.66 6214.60 379.11 o 16 10 0 1866.81 2069.55 284.87 o 17 10 0 6041.71 6646.24 476.28 o 18 10 0 2722.95 2571.10 366.37 o 1 11 0 2247.66 2036.24 226.15 o 2 11 0 1136.09 1151.32 222.16 o 3 11 0 13775.94 13231.75 494.12 o 4 11 0 494.40 314.97 184.00 o 5 11 0 28812.54 30666.29 1078.34 o 6 11 0 7.49 108.16 170.72 o 7 11 0 17594.13 17516.15 624.10 o 8 11 0 2905.24 2876.16 278.95 o 9 11 0 2424.90 2691.38 398.75 o 10 11 0 6646.08 5859.43 372.57 o 11 11 0 146.04 104.10 201.40 o 12 11 0 4239.32 4230.04 351.20 o 13 11 0 609.32 579.75 244.16 o 14 11 0 2168.74 2579.31 650.54 o 15 11 0 771.45 586.51 244.00 o 16 11 0 30.18 58.31 244.24 o 0 12 0 10508.29 9456.15 820.90 o 1 12 0 4961.35 5065.54 366.00 o 2 12 0 3826.44 4943.51 314.05 o 3 12 0 4071.52 3923.77 291.23 o 4 12 0 2580.08 2660.11 268.24 o 5 12 0 5142.38 5635.65 346.38 o 6 12 0 54.76 291.28 190.59 o 7 12 0 1349.05 1351.25 241.26 o 8 12 0 1506.11 1733.80 252.69 o 9 12 0 28.30 -4.51 195.92 o 10 12 0 1920.50 1965.85 302.48 o 11 12 0 1994.80 1840.33 278.25 o 12 12 0 2220.38 2545.52 312.92 o 13 12 0 1399.66 1567.96 290.79 o 14 12 0 1529.57 1282.96 325.31 o 1 13 0 63.14 -55.21 242.74 o 2 13 0 1809.92 1937.52 295.49 o 3 13 0 133.33 279.51 304.35 o 4 13 0 4878.22 4407.87 384.55 o 5 13 0 2581.54 2792.38 352.99 o 6 13 0 14711.75 14537.41 589.80 o 7 13 0 7439.53 8018.88 444.09 o 8 13 0 8680.93 8862.80 545.72 o 9 13 0 4163.92 4163.93 409.78 o 10 13 0 1684.82 1677.67 329.94 o 11 13 0 1815.12 1280.38 326.03 o 12 13 0 95.96 205.87 269.88 o 0 14 0 12.69 367.04 402.56 o 1 14 0 6797.30 6834.81 554.59 o 2 14 0 109.89 203.20 315.73 o 3 14 0 2866.25 3257.97 435.62 o 4 14 0 1195.41 1540.04 308.89 o 5 14 0 266.09 304.19 250.93 o 6 14 0 3000.41 3298.39 386.97 o 7 14 0 1121.78 726.55 286.18 o 8 14 0 2546.60 2240.97 437.04 o 9 14 0 5633.20 6622.24 520.81 o 1 15 0 222.32 795.21 330.69 o 2 15 0 1348.78 1453.43 365.19 o 3 15 0 750.69 1234.91 702.50 o 4 15 0 5890.90 6983.87 612.74 o -23 1 1 3683.18 4395.19 648.06 o -22 1 1 207.12 552.29 445.11 o -21 1 1 3957.75 4378.56 787.35 o -20 1 1 83.57 289.91 463.73 o -19 1 1 7125.51 7239.46 666.98 o -18 1 1 2538.14 2838.95 431.16 o -17 1 1 1906.06 1400.66 213.34 o -16 1 1 5038.34 5425.83 359.99 o -15 1 1 2941.69 2663.86 283.69 o -14 1 1 8173.27 8749.13 342.23 o -13 1 1 22029.73 21998.69 561.60 o -12 1 1 7012.48 6367.35 214.15 o -11 1 1 28277.75 28542.51 627.76 o -10 1 1 1.39 77.92 68.54 o -9 1 1 10938.92 10454.48 258.68 o -8 1 1 15618.21 15972.18 359.22 o -7 1 1 449.95 495.50 60.33 o -6 1 1 91521.35 96650.27 1925.26 o -5 1 1 3131.54 3492.86 114.42 o -4 1 1 82862.38 84921.71 1685.85 o -3 1 1 128.81 101.59 29.64 o -2 1 1 68787.12 72279.49 1741.60 o -1 1 1 1630.84 1479.99 98.67 o 0 1 1 6365.47 3.95 7.89 o 1 1 1 162.20 83.20 33.97 o 2 1 1 18634.52 20100.76 450.65 o 3 1 1 550.87 511.75 36.23 o 4 1 1 43312.41 43677.79 971.73 o 5 1 1 3913.57 4032.36 131.05 o 6 1 1 19716.10 19941.38 511.98 o 7 1 1 83.78 184.43 51.23 o 8 1 1 10607.42 10104.20 279.01 o 9 1 1 26026.32 26595.91 642.13 o 10 1 1 84.46 124.82 79.18 o 11 1 1 47881.95 50759.39 1182.87 o 12 1 1 3514.96 3784.98 178.01 o 13 1 1 38322.15 38684.08 1242.89 o 14 1 1 2711.09 3111.39 215.17 o 15 1 1 1668.75 1414.28 311.02 o 16 1 1 2491.60 2187.05 731.95 o 17 1 1 6.58 234.10 134.59 o 18 1 1 26.72 -378.40 252.27 o 19 1 1 2773.24 3188.91 708.42 o 20 1 1 827.83 725.55 415.11 o 21 1 1 5161.47 6768.40 937.33 o 22 1 1 1765.74 2032.77 551.03 o 23 1 1 5148.98 7073.69 812.08 o -23 2 1 2584.52 3177.72 616.57 o -22 2 1 1285.55 1341.14 469.94 o -21 2 1 169.39 209.79 375.15 o -20 2 1 1599.07 1298.12 416.64 o -19 2 1 580.66 900.99 436.10 o -18 2 1 24561.66 23440.80 763.20 o -17 2 1 613.75 915.02 192.08 o -16 2 1 48324.92 49808.30 1363.22 o -15 2 1 390.59 468.66 157.50 o -14 2 1 51583.27 52080.41 1391.60 o -13 2 1 11700.51 12370.52 370.78 o -12 2 1 10481.44 10983.35 329.10 o -11 2 1 45613.54 47264.10 995.16 o -10 2 1 5921.09 6164.84 178.02 o -9 2 1 48800.65 51238.29 1054.01 o -8 2 1 397.31 480.80 44.16 o -7 2 1 26499.83 26381.04 555.69 o -6 2 1 34507.44 35885.85 912.16 o -5 2 1 780.61 933.01 124.07 o -4 2 1 24984.58 26010.96 661.36 o -3 2 1 153932.97 159782.59 3468.65 o -2 2 1 33101.28 36260.15 719.05 o -1 2 1 363011.53 331003.78 7139.95 o 0 2 1 2950.00 2989.19 80.14 o 1 2 1 308224.22 291715.81 5582.67 o 2 2 1 52962.46 57903.06 1252.92 o 3 2 1 44853.87 49540.03 1079.67 o 4 2 1 9580.37 9529.45 243.09 o 5 2 1 964.79 859.91 56.72 o 6 2 1 15998.24 15207.66 376.34 o 7 2 1 19978.05 19893.67 484.73 o 8 2 1 60905.94 64263.17 1448.13 o 9 2 1 57954.23 58876.09 1340.16 o 10 2 1 9751.21 10397.18 306.06 o 11 2 1 36469.55 36790.48 885.07 o 12 2 1 437.67 534.16 100.11 o 13 2 1 20735.46 21292.63 860.71 o 14 2 1 26352.05 27329.44 811.88 o 15 2 1 1034.40 851.56 180.13 o 16 2 1 45632.16 47095.54 1676.34 o 17 2 1 33.70 -148.60 180.06 o 18 2 1 13975.63 13991.12 1214.02 o 19 2 1 553.90 332.40 356.91 o 20 2 1 2654.39 2402.15 502.30 o 21 2 1 309.31 427.41 495.30 o 22 2 1 270.19 -53.49 408.83 o 23 2 1 2533.25 2355.44 608.20 o -23 3 1 7346.24 8407.48 834.36 o -22 3 1 224.30 511.01 422.78 o -21 3 1 12438.54 12898.89 953.11 o -20 3 1 284.80 52.16 343.75 o -19 3 1 16778.97 17063.67 635.02 o -18 3 1 2517.34 2832.08 271.01 o -17 3 1 4765.39 5320.08 329.81 o -16 3 1 10748.02 10803.76 448.72 o -15 3 1 6787.87 7280.20 351.17 o -14 3 1 17285.34 18003.75 591.25 o -13 3 1 42196.85 41367.85 1131.55 o -12 3 1 15660.18 16351.52 526.24 o -11 3 1 43864.23 44414.17 1176.12 o -10 3 1 4311.33 4288.00 211.66 o -9 3 1 23719.91 23791.59 664.77 o -8 3 1 24774.29 25614.83 721.50 o -7 3 1 17561.65 17870.49 501.54 o -6 3 1 188357.25 193848.53 4681.04 o -5 3 1 2381.98 2543.96 123.70 o -4 3 1 219376.22 220571.20 5298.31 o -3 3 1 333.84 248.68 45.01 o -2 3 1 197271.84 196063.92 3795.38 o -1 3 1 2385.66 2468.85 84.31 o 0 3 1 17847.57 18678.42 396.56 o 1 3 1 24117.86 25043.31 738.20 o 2 3 1 89499.98 94563.36 1830.38 o 3 3 1 10564.78 10383.90 257.24 o 4 3 1 148275.11 155131.03 3336.41 o 5 3 1 360.09 380.33 53.16 o 6 3 1 83822.59 88420.13 1957.27 o 7 3 1 5838.36 5487.12 178.65 o 8 3 1 55408.84 58459.54 1325.62 o 9 3 1 36406.29 35404.50 933.46 o 10 3 1 4848.03 4607.50 190.84 o 11 3 1 106960.92 109615.86 2452.06 o 12 3 1 2038.35 2087.70 191.32 o 13 3 1 85287.15 89457.98 2281.00 o 14 3 1 8423.23 7566.73 350.63 o 15 3 1 5977.03 6276.99 434.64 o 16 3 1 2516.71 3225.00 316.80 o 17 3 1 323.37 554.52 260.93 o 18 3 1 209.61 491.40 366.97 o 19 3 1 6405.34 7119.84 487.21 o 20 3 1 658.98 1043.89 421.40 o 21 3 1 19446.57 19870.83 1199.65 o 22 3 1 1533.50 1363.63 499.95 o 23 3 1 9789.44 11281.70 962.74 o -23 4 1 6.92 35.82 437.13 o -22 4 1 82.40 94.51 412.43 o -21 4 1 318.67 895.89 410.23 o -20 4 1 380.11 522.92 326.98 o -19 4 1 5.23 -302.13 208.46 o -18 4 1 11596.44 11740.74 511.22 o -17 4 1 1024.82 611.54 241.02 o -16 4 1 15440.82 16486.50 591.32 o -15 4 1 1274.78 1821.97 224.48 o -14 4 1 44554.19 44253.19 1798.95 o 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