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Acta Cryst. (2010). E66, m498  [ doi:10.1107/S160053681001189X ]

[O-Ethyl (Z)-N-(2-chlorophenyl)thiocarbamato-[kappa]S](tricyclohexylphosphine-[kappa]P)gold(I)

P. P. Tadbuppa and E. R. T. Tiekink

Online 10 April 2010


Key indicators

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Alert level B PLAT919_ALERT_3_B Reflection(s) # Likely Affected by the Beamstop 2
Alert level C PLAT215_ALERT_3_C Disordered C8A has ADP max/min Ratio ..... 3.30 PLAT215_ALERT_3_C Disordered C8B has ADP max/min Ratio ..... 3.30 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C19 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C3 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C11 PLAT313_ALERT_2_C Oxygen with three covalent bonds (rare) ........ O1A PLAT313_ALERT_2_C Oxygen with three covalent bonds (rare) ........ O1B PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang .. 11 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 7 PLAT234_ALERT_4_C Large Hirshfeld Difference C25 -- C26 .. 0.17 Ang. PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 6
Alert level G PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 8.00 Perc. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 4 PLAT128_ALERT_4_G Non-standard setting of Space-group P21/c .... P21/n PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 1 P1 -AU -S1 -C1 95.00 1.20 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 2 S1 -AU -P1 -C16 40.80 1.20 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 3 S1 -AU -P1 -C10 -77.60 1.20 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 4 S1 -AU -P1 -C22 164.60 1.20 1.555 1.555 1.555 1.555 PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 10 PLAT779_ALERT_4_G Suspect or Irrelevant (Bond) Angle in CIF ...... 0.00 Deg. O1B -C1 -O1A 1.555 1.555 1.555
0 ALERT level A = In general: serious problem 1 ALERT level B = Potentially serious problem 11 ALERT level C = Check and explain 9 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 7 ALERT type 3 Indicator that the structure quality may be low 9 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

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