Acta Cryst. (2010). E66, o1102  [ doi:10.1107/S1600536810013589 ]

N-[Bis(dimethylamino)phosphinoyl]-2,2,2-trichloroacetamide

O. V. Amirkhanov, O. V. Moroz, K. O. Znovjyak, E. A. Trush and T. Y. Sliva

Online 17 April 2010

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.001 Å
• R factor = 0.030
• wR factor = 0.072
• Data-to-parameter ratio = 39.1

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT431_ALERT_2_B Short Inter HL..A Contact  Cl2    ..  O2      ..       2.96 Ang. 

Alert level C
ABSTY02_ALERT_1_C  An _exptl_absorpt_correction_type has been given without
            a literature citation. This should be contained in the
            _exptl_absorpt_process_details field.
            Absorption correction given as gaussian
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          5      
PLAT158_ALERT_4_C The Input Unitcell is NOT Standard/Reduced .....          ?
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600        128      

Alert level G
PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety         C6     

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster