# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' uop030 in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 626.36 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.8062 _cell_length_b 16.3418 _cell_length_c 17.1000 _cell_angle_alpha 106.593 _cell_angle_beta 99.932 _cell_angle_gamma 105.572 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 44192.88 47080.68 673.71 o 3 0 0 7761.03 8627.09 109.18 o 4 0 0 109.04 266.33 72.85 o 5 0 0 93296.34 90014.71 1358.63 o 6 0 0 1781.98 2018.43 203.13 o 7 0 0 103621.85 103239.19 1045.74 o 8 0 0 711.78 1129.58 233.43 o 9 0 0 35.04 193.52 313.07 o 10 0 0 6695.30 6756.92 488.97 o -11 1 0 3765.42 4579.86 570.91 o -10 1 0 34219.28 36584.12 656.50 o -9 1 0 3590.46 4079.35 261.23 o -8 1 0 44186.03 45742.45 556.12 o -7 1 0 52031.44 52288.24 876.91 o -6 1 0 2353.22 2580.67 128.80 o -5 1 0 38232.16 38394.77 264.04 o -4 1 0 16331.03 17535.87 417.08 o -3 1 0 54640.52 58415.34 312.45 o -2 1 0 2777.91 3222.76 182.88 o 1 1 0 111.57 297.82 101.03 o 2 1 0 2.93 466.66 149.28 o 3 1 0 361.22 566.46 69.15 o 4 1 0 29901.53 27269.61 685.42 o 5 1 0 6644.99 7399.67 275.95 o 6 1 0 14099.25 14053.09 545.15 o 7 1 0 4966.49 4592.42 291.27 o 8 1 0 1671.53 2006.93 277.72 o 9 1 0 12814.72 12608.52 534.18 o 10 1 0 2059.24 2576.12 371.23 o -11 2 0 5195.89 6110.41 691.46 o -10 2 0 14488.97 15754.13 637.08 o -9 2 0 175.54 26.79 225.22 o -8 2 0 2667.41 2797.12 255.99 o -7 2 0 1600.06 1466.15 142.99 o -6 2 0 12470.63 12955.56 281.49 o -5 2 0 6952.17 6855.17 170.79 o -4 2 0 11219.99 11015.95 526.25 o -3 2 0 183335.03 172096.22 5909.78 o -2 2 0 9780.07 12553.43 1051.61 o 1 2 0 264.40 660.76 185.23 o 2 2 0 4992.82 6713.65 351.70 o 3 2 0 77073.99 77331.62 702.58 o 4 2 0 185632.33 160303.95 2233.45 o 5 2 0 11046.02 10182.27 280.53 o 6 2 0 4104.42 3838.14 274.45 o 7 2 0 14348.80 13655.74 393.61 o 8 2 0 30450.67 31312.93 580.32 o 9 2 0 380.19 420.67 299.35 o 10 2 0 10739.78 11072.10 550.26 o -11 3 0 7755.82 9790.05 443.83 o -10 3 0 62920.33 68931.12 1194.16 o -9 3 0 18709.90 19995.78 387.80 o -8 3 0 95249.80 100753.44 1444.19 o -7 3 0 110.70 238.15 223.27 o -6 3 0 35315.12 37706.03 613.91 o -5 3 0 5773.37 6250.76 169.53 o -4 3 0 52001.95 54226.59 2951.25 o -3 3 0 267551.75 208457.30 14975.69 o -2 3 0 4948.85 5298.90 158.15 o -1 3 0 68153.06 72493.18 2087.35 o 0 3 0 14050.82 14813.44 576.85 o 1 3 0 1165.95 1935.72 323.79 o 2 3 0 37300.10 41460.53 1004.32 o 3 3 0 8829.38 9663.04 354.95 o 4 3 0 8350.35 8634.65 463.37 o 5 3 0 259.87 337.09 88.14 o 6 3 0 12842.24 12830.34 388.49 o 7 3 0 399.98 555.53 268.21 o 8 3 0 13547.29 13609.23 475.65 o 9 3 0 4106.81 4692.80 1702.68 o 10 3 0 14883.91 14297.33 777.65 o -11 4 0 3091.99 3012.98 284.91 o -10 4 0 26.71 -13.62 254.67 o -9 4 0 378.41 483.08 217.64 o -8 4 0 5703.10 6061.68 359.91 o -7 4 0 20248.57 22080.30 772.31 o -6 4 0 10348.18 9813.81 542.11 o -5 4 0 4407.80 4982.52 317.36 o -4 4 0 445.29 473.53 95.47 o -3 4 0 606.76 688.36 180.63 o -2 4 0 32664.38 34412.92 1010.22 o -1 4 0 31138.93 33521.57 369.00 o 0 4 0 43997.32 44655.86 469.04 o 1 4 0 8281.00 8681.45 553.59 o 2 4 0 21799.37 25776.54 3006.99 o 3 4 0 6913.95 8444.29 1874.85 o 4 4 0 65284.01 62235.39 979.66 o 5 4 0 5647.58 5910.94 341.23 o 6 4 0 156.27 2310.47 1016.73 o 7 4 0 113677.34 111511.67 2988.20 o 8 4 0 422.40 783.44 378.80 o 9 4 0 5024.23 5002.94 444.88 o -11 5 0 38052.45 38218.72 809.79 o -10 5 0 7282.63 7823.69 295.00 o -9 5 0 55939.47 57995.36 854.68 o -8 5 0 446.07 628.93 167.11 o -7 5 0 17719.12 18360.71 585.33 o -6 5 0 57423.34 58263.14 661.15 o -5 5 0 6405.16 6404.12 240.92 o -4 5 0 136762.73 124054.46 944.39 o -3 5 0 6564.30 6880.35 212.78 o -2 5 0 12.87 258.89 180.53 o -1 5 0 571.49 756.22 289.66 o 0 5 0 57509.11 56887.12 2181.21 o 1 5 0 21349.37 23447.80 444.65 o 2 5 0 38715.98 42299.74 1565.47 o 3 5 0 1244.68 1898.40 357.72 o 4 5 0 307.78 537.90 289.98 o 5 5 0 860.28 711.16 382.07 o 6 5 0 799.38 509.32 332.13 o 7 5 0 10833.96 11061.00 936.76 o 8 5 0 741.52 1295.58 392.89 o 9 5 0 473.91 853.64 425.56 o -11 6 0 5588.92 6053.14 305.37 o -10 6 0 329.79 271.07 282.67 o -9 6 0 5958.44 5855.24 297.87 o -8 6 0 13.00 179.67 168.89 o -7 6 0 5784.26 5866.63 298.94 o -6 6 0 907.59 1194.71 187.33 o -5 6 0 25097.75 21404.11 2526.65 o -4 6 0 416.21 706.73 235.89 o -3 6 0 24340.99 25154.93 383.29 o -2 6 0 23973.83 25685.17 374.82 o -1 6 0 1979.66 2424.52 259.41 o 0 6 0 15274.90 15487.51 369.82 o 1 6 0 3150.67 3135.69 238.97 o 2 6 0 24774.27 26184.70 655.91 o 3 6 0 14.97 -224.01 371.64 o 4 6 0 35512.23 34776.61 1124.17 o 5 6 0 928.30 818.60 427.09 o 6 6 0 28831.31 27148.48 2007.61 o 7 6 0 83819.80 74875.66 4942.33 o 8 6 0 420.30 167.71 502.61 o -11 7 0 13.67 308.96 339.36 o -10 7 0 1587.48 1935.18 532.32 o -9 7 0 13427.48 14540.63 360.92 o -8 7 0 45919.21 47800.59 1228.10 o -7 7 0 148.57 315.88 272.89 o -6 7 0 1253.00 1469.13 280.71 o -5 7 0 45941.71 44461.52 710.07 o -4 7 0 7073.35 6940.48 324.24 o -3 7 0 103900.69 99013.80 1262.75 o -2 7 0 5264.94 5536.89 263.93 o -1 7 0 262426.63 237353.33 2528.63 o 0 7 0 6966.83 7119.18 708.92 o 1 7 0 443.23 1258.33 526.26 o 2 7 0 14230.85 12197.92 6313.55 o 3 7 0 2068.50 2387.29 486.90 o 4 7 0 84162.00 82476.09 2916.55 o 5 7 0 95.51 505.51 498.08 o 6 7 0 74342.22 65479.47 1353.55 o 7 7 0 8267.68 7390.20 677.33 o 8 7 0 693.33 776.98 456.90 o -11 8 0 12177.91 12235.42 685.02 o -10 8 0 12.41 377.09 327.21 o -9 8 0 7.32 216.62 219.46 o -8 8 0 20997.19 21758.63 578.05 o -7 8 0 1255.48 1370.88 334.70 o -6 8 0 4904.95 3695.32 268.16 o -5 8 0 884.10 977.10 293.92 o -4 8 0 5356.23 5524.89 268.42 o -3 8 0 2231.38 2459.34 243.85 o -2 8 0 7331.88 7356.37 367.49 o -1 8 0 24306.18 25206.38 499.06 o 0 8 0 576.38 417.90 271.27 o 1 8 0 46237.68 48207.69 1807.84 o 2 8 0 1291.77 2476.08 508.05 o 3 8 0 329.65 1235.07 784.83 o 4 8 0 18680.40 18589.21 938.42 o 5 8 0 958.16 1078.71 501.28 o 6 8 0 22260.42 19438.03 896.37 o 7 8 0 5656.99 6282.36 673.59 o 8 8 0 11733.01 8714.34 731.78 o -11 9 0 7580.75 7628.43 512.72 o -10 9 0 77.35 451.53 384.91 o -9 9 0 1614.18 1505.65 249.39 o -8 9 0 210.35 482.20 346.42 o -7 9 0 21.49 -23.36 1057.29 o -6 9 0 22081.99 21048.39 688.12 o -5 9 0 31585.88 30364.36 635.72 o -4 9 0 120099.04 113880.91 1733.64 o -3 9 0 58736.34 55798.92 1010.46 o -2 9 0 61840.98 60677.89 1062.43 o -1 9 0 82763.77 83394.13 866.40 o 0 9 0 1576.70 1308.58 294.18 o 1 9 0 64877.34 64936.60 3097.54 o 2 9 0 64.65 550.17 499.27 o 3 9 0 142544.02 139251.02 5653.97 o 4 9 0 52707.30 34644.84 20090.79 o 5 9 0 657.39 1641.96 601.76 o 6 9 0 32589.54 28371.76 1100.29 o 7 9 0 746.44 603.00 583.62 o -11 10 0 61711.09 62069.91 5220.90 o -10 10 0 2475.08 2441.52 300.81 o -9 10 0 13595.60 13259.48 553.63 o -8 10 0 572.97 361.43 471.61 o -7 10 0 20384.18 20096.44 597.25 o -6 10 0 19120.93 18857.87 582.02 o -5 10 0 8915.17 8694.01 470.12 o -4 10 0 110439.20 103621.73 1254.09 o -3 10 0 5013.09 5411.46 334.44 o -2 10 0 18593.38 19414.82 514.84 o -1 10 0 9326.60 10102.18 415.70 o 0 10 0 37.46 319.67 370.23 o 1 10 0 12075.29 12489.27 611.32 o 2 10 0 272.58 323.53 517.50 o 3 10 0 27760.40 29890.01 845.56 o 4 10 0 4276.13 3167.26 886.20 o 5 10 0 3350.11 3853.74 748.40 o 6 10 0 5011.70 3280.47 712.31 o 7 10 0 2556.74 2363.42 731.59 o -11 11 0 4290.51 4680.69 537.96 o -10 11 0 1976.34 1995.67 322.04 o -9 11 0 983.21 690.47 574.76 o -8 11 0 4791.77 4676.24 485.85 o -7 11 0 9907.52 10592.44 961.99 o -6 11 0 1636.41 2233.49 419.80 o -5 11 0 498.54 523.68 398.72 o -4 11 0 25504.29 25590.66 658.21 o -3 11 0 8155.10 8712.49 444.60 o -2 11 0 79323.19 76105.12 1917.18 o -1 11 0 20771.29 20229.44 555.43 o 0 11 0 18194.91 20664.43 535.03 o 1 11 0 23243.19 25286.05 568.07 o 2 11 0 2794.50 3558.92 1252.38 o 3 11 0 64011.77 70538.99 4625.69 o 4 11 0 278.55 470.82 637.40 o 5 11 0 6433.78 6141.41 845.85 o 6 11 0 7422.21 4652.63 801.21 o -10 12 0 12628.63 12372.22 599.88 o -9 12 0 861.67 1292.85 436.57 o -8 12 0 10229.09 9959.88 542.64 o -7 12 0 113590.31 107338.70 1291.04 o -6 12 0 19948.71 18748.47 643.42 o -5 12 0 71027.09 68586.88 1313.91 o -4 12 0 19981.97 18568.88 499.76 o -3 12 0 3485.44 3787.38 396.73 o -2 12 0 13479.74 13320.97 501.78 o -1 12 0 4198.35 4524.76 937.27 o 0 12 0 43321.71 46576.91 1101.61 o 1 12 0 1.37 466.25 467.02 o 2 12 0 2949.59 3963.28 539.48 o 3 12 0 21372.88 24221.57 1146.75 o 4 12 0 289.61 410.29 683.72 o 5 12 0 4437.39 4319.83 808.74 o -10 13 0 9652.06 10154.41 641.85 o -9 13 0 31.01 274.63 459.76 o -8 13 0 378.45 526.69 452.52 o -7 13 0 463.20 548.77 436.80 o -6 13 0 2069.79 1943.36 487.35 o -5 13 0 1007.38 1091.55 312.73 o -4 13 0 4712.93 4245.26 438.03 o -3 13 0 14251.17 14052.47 554.21 o -2 13 0 17694.96 17888.97 583.14 o -1 13 0 6719.55 7153.30 455.87 o 0 13 0 3338.00 4735.93 390.31 o 1 13 0 2044.98 2354.96 485.53 o 2 13 0 18914.23 21423.47 1320.68 o 3 13 0 3403.56 2903.47 911.57 o 4 13 0 2193.93 3359.53 906.03 o 5 13 0 422.16 1486.72 840.52 o -10 14 0 11926.74 12712.87 1424.39 o -9 14 0 3962.13 4686.63 524.62 o -8 14 0 9811.26 10875.56 621.83 o -7 14 0 27526.11 28509.66 833.17 o -6 14 0 20997.78 20187.02 712.19 o -5 14 0 17815.16 16536.26 520.23 o -4 14 0 47602.66 44813.24 1747.39 o -3 14 0 10695.20 11474.90 526.59 o -2 14 0 1936.15 2133.32 391.61 o -1 14 0 860.94 1073.75 382.75 o 0 14 0 12915.08 13511.59 499.16 o 1 14 0 249.50 447.07 508.39 o 2 14 0 1625.92 2528.39 513.88 o 3 14 0 16198.71 18021.43 1423.29 o 4 14 0 105.15 1216.20 844.14 o -9 15 0 37.65 225.06 475.34 o -8 15 0 1268.66 1246.78 534.94 o -7 15 0 4715.27 4897.73 584.51 o -6 15 0 10227.77 9264.01 619.89 o -5 15 0 1065.21 957.47 416.78 o -4 15 0 2425.90 2218.11 417.96 o -3 15 0 1190.54 1639.38 398.60 o -2 15 0 191.98 412.95 369.43 o -1 15 0 1879.81 2118.91 351.31 o 0 15 0 14410.43 17372.04 1085.19 o 1 15 0 1296.82 1654.05 477.91 o 2 15 0 7315.12 9695.90 1304.38 o 3 15 0 11391.54 10674.81 1318.68 o -8 16 0 14429.38 14813.20 764.54 o -7 16 0 5023.10 5028.21 608.89 o -6 16 0 14121.52 13084.36 932.53 o -5 16 0 22117.75 20547.83 684.40 o -4 16 0 27822.80 27923.96 733.68 o -3 16 0 14.13 54.09 388.73 o -2 16 0 1635.40 1543.91 448.68 o -1 16 0 9027.05 10409.32 644.69 o 0 16 0 47151.27 55037.89 4738.57 o 1 16 0 1033.57 2195.83 1121.67 o 2 16 0 16659.88 21514.68 1534.52 o -7 17 0 8165.63 8806.96 938.81 o -6 17 0 581.99 637.43 573.14 o -5 17 0 17567.57 17519.09 666.81 o -4 17 0 8041.39 8313.74 563.55 o -3 17 0 99.53 408.82 400.86 o -2 17 0 2122.80 2089.24 371.29 o -1 17 0 21.47 748.60 496.22 o 0 17 0 533.18 1360.35 530.59 o -6 18 0 912.34 1523.15 649.41 o -5 18 0 15486.41 15577.46 673.64 o -4 18 0 480.54 413.54 427.70 o -3 18 0 24153.22 24182.17 738.58 o -2 18 0 1862.12 2248.62 536.32 o -1 18 0 4354.81 5707.18 625.98 o 1 -18 1 6237.62 6206.76 627.82 o 2 -18 1 6469.49 5584.93 779.19 o 3 -18 1 1212.53 608.48 426.86 o 4 -18 1 97.05 352.77 397.27 o 5 -18 1 7748.45 8184.47 556.88 o 6 -18 1 527.08 1097.82 659.58 o -1 -17 1 2644.60 4011.93 562.33 o 0 -17 1 3614.82 4583.90 556.19 o 1 -17 1 4455.86 5257.99 566.68 o 2 -17 1 19286.79 18746.27 1069.69 o 3 -17 1 18782.51 18240.43 648.07 o 4 -17 1 67189.41 62735.37 1127.17 o 5 -17 1 5115.76 5198.00 750.79 o 6 -17 1 2424.18 2910.60 717.20 o 7 -17 1 22957.59 23238.65 833.83 o 8 -17 1 571.28 1286.26 551.10 o -2 -16 1 2406.84 3352.89 1099.70 o -1 -16 1 36264.36 43784.62 1375.52 o 0 -16 1 5414.73 6662.71 741.91 o 1 -16 1 656.01 1697.45 495.44 o 2 -16 1 22643.97 21494.00 645.88 o 3 -16 1 4019.79 4109.98 434.76 o 4 -16 1 34262.09 32328.77 1586.81 o 5 -16 1 509.66 664.88 428.89 o 6 -16 1 1734.56 1839.21 468.68 o 7 -16 1 1590.18 1879.32 551.23 o 8 -16 1 7180.17 7888.72 640.64 o -3 -15 1 1719.47 170.59 931.43 o -2 -15 1 621.64 612.64 530.32 o -1 -15 1 23.01 865.37 498.08 o 0 -15 1 105.89 914.95 487.20 o 1 -15 1 5414.53 5559.91 439.81 o 2 -15 1 10687.07 10650.42 734.28 o 3 -15 1 24486.22 21875.85 658.37 o 4 -15 1 44852.21 43341.54 878.51 o 5 -15 1 3415.67 3415.24 369.47 o 6 -15 1 580.00 819.10 478.61 o 7 -15 1 1997.20 2401.99 536.35 o 8 -15 1 22050.76 22538.61 812.13 o 9 -15 1 14701.76 14347.22 835.26 o -4 -14 1 42598.55 48973.95 1732.47 o -3 -14 1 1854.76 2037.35 1019.32 o -2 -14 1 569.70 1252.14 543.60 o -1 -14 1 37139.43 43570.95 2576.58 o 0 -14 1 4713.99 5138.71 695.47 o 1 -14 1 77750.51 79069.59 1563.79 o 2 -14 1 214.67 628.32 346.14 o 3 -14 1 40164.72 39770.02 1511.92 o 4 -14 1 11709.18 11540.87 552.97 o 5 -14 1 11779.41 10455.13 464.29 o 6 -14 1 5200.25 5100.16 552.35 o 7 -14 1 3501.04 3291.42 522.58 o 8 -14 1 12468.04 12385.46 630.40 o 9 -14 1 2404.14 2645.30 603.78 o 10 -14 1 2052.63 1713.89 488.20 o -5 -13 1 414.91 1053.03 789.32 o -4 -13 1 32467.90 34162.17 1422.27 o -3 -13 1 2057.06 1816.47 562.24 o -2 -13 1 1427.86 1387.21 787.73 o -1 -13 1 3799.11 4143.23 1042.54 o 0 -13 1 674.90 1381.71 341.85 o 1 -13 1 382.28 494.09 364.60 o 2 -13 1 4843.01 4907.61 437.67 o 3 -13 1 69.88 120.72 402.38 o 4 -13 1 1054.82 1173.46 379.79 o 5 -13 1 40.20 91.44 348.05 o 6 -13 1 2546.11 3145.98 569.85 o 7 -13 1 218.15 310.49 454.15 o 8 -13 1 20423.92 20117.45 720.91 o 9 -13 1 4167.85 4693.96 775.76 o 10 -13 1 2686.44 2463.18 506.95 o -6 -12 1 18194.57 15892.65 1060.20 o -5 -12 1 964.04 2389.41 715.95 o -4 -12 1 1040.57 1567.17 925.95 o -3 -12 1 8129.03 9599.03 769.49 o -2 -12 1 27676.90 32201.89 1434.33 o -1 -12 1 1727.92 2484.22 391.02 o 0 -12 1 73814.02 78815.34 922.89 o 1 -12 1 29486.52 31366.96 642.39 o 2 -12 1 26799.57 25825.48 643.06 o 3 -12 1 14156.21 13499.81 549.63 o 4 -12 1 22541.90 21182.79 526.55 o 5 -12 1 5566.48 5358.28 389.22 o 6 -12 1 12648.99 12571.54 573.67 o 7 -12 1 668.97 622.57 471.63 o 8 -12 1 23740.30 22231.85 729.09 o 9 -12 1 20376.65 19965.11 711.59 o 10 -12 1 58.41 -1.39 397.38 o -6 -11 1 1051.86 1532.25 729.67 o -5 -11 1 4775.91 5247.02 793.33 o -4 -11 1 3918.92 2780.91 546.51 o -3 -11 1 2679.06 3986.45 1723.83 o -2 -11 1 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