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Acta Cryst. (2010). E66, m633  [ doi:10.1107/S1600536810016466 ]

Dichlorido{(E)-2,4,6-trimethyl-N-[phenyl(2-pyridyl)methylidene]aniline-[kappa]2N,N'}palladium(II)

C.-H. Yang, Y.-L. Peng, M.-H. Wang, K.-C. Shih and M.-L. Hsueh

Online 8 May 2010


Key indicators

checkCIF/PLATON results

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Alert level C PLAT432_ALERT_2_C Short Inter X...Y Contact Cl1 .. C5 .. 3.24 Ang. PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2 PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 4
Alert level G REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF. From the CIF: _diffrn_reflns_theta_max 26.08 From the CIF: _reflns_number_total 3956 Count of symmetry unique reflns 2286 Completeness (_total/calc) 173.05% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 1670 Fraction of Friedel pairs measured 0.731 Are heavy atom types Z>Si present yes
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 4 ALERT level C = Check and explain 1 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

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