supplementary materials


lh5037 scheme

Acta Cryst. (2010). E66, m839    [ doi:10.1107/S160053681002310X ]

12-Tungstophosphoric acid-1,1'-methylenebis(imidazolidine-2,4-dione)-imidazolidine-2,4-dione-water (2/1/4/21.5)

M. H. Alizadeh and I. Mohammadi Zonoz

Abstract top

In the asymmetric unit of the title organic-inorganic hybrid material, 2{H3[PW12O40]}·4C3H4N2O2·C7H8N4O4·21.5H2O, there are four crystallographically independent hydantoin molecules, one dimerized hydantoin molecule, viz. 1,1'-methylenebis(imidazolidine-2,4-dione, two independent H3PW12O40 molecules and 21.5 solvent water molecules. Nine of the solvent water molecules were refined as 0.5 occupancy. The tungstophosphoric acid moieties show characteristic features with respect to the bond lengths and angles.

Comment top

Hydantions, are biologically active compounds. The profound interest in different hydantoin derivatives stems from the well established medical applications of some Hydantoin derivatives as antiepileptic drugs (Micali et al., 1999). Polyoxometalates (POMs) have been attracting extensive interest in solid-state materials chemistry due to their potential applications in medicine, as well as the richness of their structures (Yanagie et al., 2006). Recently, an important advance in polyoxometalate chemistry is the modification of polyoxometalates with various organic ligands and transition metal complexes to obtain organic–inorganic hybrid materials (Guangzhe et al., 2008). Here we report the crystal structure the title hybrid containing hydantoin.

The title compound consists of hydantoin and a dimerized species of hydantoin which crystallize with H3[PW12O40] and 21.5 solvent water molecules. The asymmetric unit contains two independent H3[PW12O40] molecules (labeled with A and B in Figs. 1 & 2). The [PW12O40]-3 anion (Keggin structure) consists of a central PO4 tetrahedron that surrounded by twelve WO6 octahedrons (Keggin, 1933). In molecule A of H3PW12O40, all W–Ot(terminal) bonds are essentially equal, ranging from 1.697 (13)–1.724 (12) Å (mean 1.709 Å). In molecule B these values are 1.684 (11)–1.736 (13) A° mean (1.710 Å). The P–O distances in the two independendent molecules of H3PW12O40 are equal within experimental error ranging from 1.519 (11)-1.556 (12) A° (mean 1.538 A°) for molecule A and in the range 1.526 (12)–1.537 (12) A° (mean 1.530 A°) for molecule B. These quantities are similar to the W–Ot and P–O distances of a related Keggin structure which are 1.7041 (11) and 1.5305 (11) A° (Lebeden et al., 1969). In the two independent molecules of H3PW12O40 the O—P—O angles are close to the ideal 109.5° based sp3 hybridization principles. The four independent molecules of hydantoin are shown in (Fig. 3). The pseudo-dimerized species of hydantoin is shown in (Fig. 4).

Related literature top

For the medical applications of some hydantoin derivatives as antiepileptic drugs, see: Micali et al. (1999. For the applications of polyoxometalates, see: Yanagie et al. (2006). For background to organic–inorganic hybrid materials, see: Guangzhe et al. (2008). The [PW12O40]-3 anion (Keggin structure) consists of a central PO4 tetrahedron surrounded by twelve WO6 octahedrons, see: Keggin (1933). For a related Keggin structure, see: Lebeden et al. (1969).

Experimental top

A solution of Hydantoin (0.06 g, 0.60 mmol) in 5 ml of 1.00 M HCl was added to a stirred solution of H3[PW12O40] (0.28 g, 0.10 mmol) in 10 ml H2O and stirred at room temperature for 2 h. After stirring, it was filtered. The filtrate was allowed to evaporate slowly at room temperature. Good-quality white prism crystals were obtained after 4 days which were filtered off and washed with water, then dried at ambient temperature.

Refinement top

Neither the hydrogen atoms of the water molecules not the hydrogen atoms in the two crystallographically independent H3W12PO40 molecules could be located and were not included in the refinement. These H atoms are included in the molecular formula. The hydrogen atoms in the organic molecules (four independent hydantoin molecules and the dimerized molecule) were placed geometrically [C-H = 0.99 & N-H = 0.88 Å] and refined in a riding-model approximation with the Uiso(H) parameters equal to 1.2Ueq(C,N). The crystals used was an inversion twin with the ratio of twin components being 0.492 (11):0.508 (11).

Computing details top

Data collection: APEX2 (Bruker, 2005); cell refinement: SAINT (Bruker, 2005); data reduction: SAINT (Bruker, 2005); program(s) used to solve structure: SHELXTL (Sheldrick, 2008); program(s) used to refine structure: SHELXTL (Sheldrick, 2008); molecular graphics: SHELXTL (Sheldrick, 2008); software used to prepare material for publication: SHELXTL (Sheldrick, 2008).

Figures top
[Figure 1] Fig. 1. The molecular structure of one independent molecule [A] of H3[PW12O40] with 50% displacement ellipsoids. H atoms were not located.
[Figure 2] Fig. 2. The molecular structure of the other independent molecule [B] of H3[PW12O40] with 50% displacement ellipsoids. H atoms were not located.
[Figure 3] Fig. 3. Four crystallographically independent molecules of Hydantoin. Thermal ellipsoids are drawn at the 50% probability level.
[Figure 4] Fig. 4. The dimerized molecule of hydantoin. Thermal ellipsoids are given at the 50% probability level.
12-Tungstophosphoric acid–1,1'-methylenebis(imidazolidine-2,4-dione–imidazolidine-2,4-dione)–water (2/1/4/21.5) top
Crystal data top
2{H3[PW12O40]}·4C3H4N2O2·C7H8N4O4·21.5H2OZ = 1
Mr = 6760.23F(000) = 2985
Triclinic, P1Dx = 4.083 Mg m3
Hall symbol: P 1Mo Kα radiation, λ = 0.71073 Å
a = 12.7271 (6) ÅCell parameters from 5550 reflections
b = 13.3286 (7) Åθ = 2.3–27.8°
c = 18.9177 (9) ŵ = 25.15 mm1
α = 71.328 (1)°T = 100 K
β = 81.316 (1)°Prism, colourless
γ = 64.751 (1)°0.31 × 0.17 × 0.08 mm
V = 2749.3 (2) Å3
Data collection top
Bruker SMART APEXII CCD
diffractometer
25728 independent reflections
Radiation source: fine-focus sealed tube22772 reflections with I > 2σ(I)
graphiteRint = 0.048
φ and ω scansθmax = 27.9°, θmin = 1.8°
Absorption correction: integration
(SADABS; Bruker, 2005)
h = 1616
Tmin = 0.031, Tmax = 0.215k = 1717
51543 measured reflectionsl = 2424
Refinement top
Refinement on F2Secondary atom site location: difference Fourier map
Least-squares matrix: fullHydrogen site location: inferred from neighbouring sites
R[F2 > 2σ(F2)] = 0.043H-atom parameters constrained
wR(F2) = 0.102 w = 1/[σ2(Fo2) + (0.0474P)2]
where P = (Fo2 + 2Fc2)/3
S = 1.00(Δ/σ)max = 0.002
25728 reflectionsΔρmax = 2.44 e Å3
1577 parametersΔρmin = 1.32 e Å3
45 restraintsAbsolute structure: Flack (1983), 12649 Friedel pairs
Primary atom site location: structure-invariant direct methodsFlack parameter: 0.492 (11)
Crystal data top
2{H3[PW12O40]}·4C3H4N2O2·C7H8N4O4·21.5H2Oγ = 64.751 (1)°
Mr = 6760.23V = 2749.3 (2) Å3
Triclinic, P1Z = 1
a = 12.7271 (6) ÅMo Kα radiation
b = 13.3286 (7) ŵ = 25.15 mm1
c = 18.9177 (9) ÅT = 100 K
α = 71.328 (1)°0.31 × 0.17 × 0.08 mm
β = 81.316 (1)°
Data collection top
Bruker SMART APEXII CCD
diffractometer
25728 independent reflections
Absorption correction: integration
(SADABS; Bruker, 2005)
22772 reflections with I > 2σ(I)
Tmin = 0.031, Tmax = 0.215Rint = 0.048
51543 measured reflectionsθmax = 27.9°
Refinement top
R[F2 > 2σ(F2)] = 0.043H-atom parameters constrained
wR(F2) = 0.102Δρmax = 2.44 e Å3
S = 1.00Δρmin = 1.32 e Å3
25728 reflectionsAbsolute structure: Flack (1983), 12649 Friedel pairs
1577 parametersFlack parameter: 0.492 (11)
45 restraints
Special details top

Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
W1A0.53978 (5)0.04182 (6)0.09204 (4)0.02518 (14)
W2A0.49583 (6)0.05828 (6)0.29651 (4)0.02500 (13)
W3A0.79195 (5)0.15553 (6)0.21328 (4)0.02515 (14)
W4A0.66181 (5)0.23803 (6)0.02094 (4)0.02508 (14)
W5A0.39098 (5)0.31883 (6)0.10253 (4)0.02576 (14)
W6A0.35353 (5)0.21981 (6)0.30717 (4)0.02537 (14)
W7A0.59046 (5)0.03417 (6)0.41337 (4)0.02468 (13)
W8A0.88463 (5)0.05713 (6)0.32745 (4)0.02459 (13)
W9A0.91794 (5)0.03733 (6)0.13866 (4)0.02505 (14)
W10A0.76520 (5)0.33957 (6)0.14672 (4)0.02490 (13)
W11A0.49291 (5)0.42650 (6)0.22420 (4)0.02525 (14)
W12A0.72596 (5)0.24394 (6)0.33558 (4)0.02421 (13)
P1A0.6346 (4)0.1357 (4)0.2185 (3)0.0210 (7)
O1A0.5043 (10)0.0312 (11)0.0463 (6)0.027 (2)
O2A0.4792 (9)0.0003 (12)0.1913 (6)0.028 (3)
O3A0.6879 (10)0.0700 (11)0.1320 (7)0.030 (3)
O4A0.6155 (10)0.1218 (10)0.0163 (7)0.028 (2)
O5A0.4081 (9)0.1879 (11)0.0764 (6)0.028 (2)
O6A0.5818 (9)0.1684 (10)0.1433 (5)0.023 (2)
O7A0.4484 (11)0.1673 (11)0.3169 (7)0.033 (3)
O8A0.6589 (9)0.1396 (10)0.2741 (6)0.024 (2)
O9A0.3615 (9)0.0727 (11)0.3080 (7)0.028 (3)
O10A0.5461 (11)0.0725 (11)0.3930 (6)0.028 (2)
O11A0.5539 (9)0.0982 (9)0.2811 (6)0.022 (2)
O12A0.8423 (11)0.2951 (11)0.2089 (8)0.036 (3)
O13A0.8779 (9)0.1804 (10)0.2968 (6)0.025 (2)
O14A0.9038 (10)0.1018 (11)0.1500 (6)0.028 (3)
O15A0.7551 (9)0.0322 (10)0.2227 (6)0.025 (2)
O16A0.7020 (10)0.2876 (11)0.0693 (6)0.031 (3)
O17A0.5005 (10)0.3366 (12)0.0200 (6)0.030 (3)
O18A0.8050 (10)0.1118 (11)0.0641 (6)0.028 (2)
O19A0.6965 (10)0.3232 (11)0.0701 (7)0.027 (2)
O20A0.2635 (11)0.4191 (11)0.0612 (7)0.033 (3)
O21A0.3442 (10)0.2571 (11)0.2004 (6)0.029 (3)
O22A0.4415 (10)0.4046 (11)0.1427 (7)0.030 (3)
O23A0.2126 (10)0.2850 (11)0.3334 (7)0.027 (2)
O24A0.4353 (10)0.1437 (10)0.3981 (7)0.028 (2)
O25A0.4121 (10)0.3361 (11)0.2861 (7)0.028 (3)
O26A0.5979 (11)0.0109 (12)0.5079 (7)0.034 (3)
O27A0.7438 (9)0.0517 (10)0.3842 (6)0.024 (2)
O28A0.6340 (9)0.1624 (9)0.3880 (6)0.021 (2)
O29A0.9876 (10)0.1355 (11)0.3949 (7)0.031 (3)
O30A0.9759 (9)0.0293 (10)0.2398 (6)0.025 (2)
O31A0.8386 (9)0.0975 (9)0.3287 (6)0.024 (2)
O32A1.0446 (10)0.0166 (11)0.0883 (7)0.030 (3)
O33A0.8745 (9)0.1850 (9)0.1510 (6)0.023 (2)
O34A0.8409 (10)0.4202 (11)0.0987 (6)0.030 (3)
O35A0.6180 (9)0.4525 (11)0.1615 (6)0.027 (2)
O36A0.7991 (10)0.3118 (10)0.2481 (6)0.026 (2)
O37A0.6478 (10)0.2407 (10)0.2261 (7)0.028 (2)
O38A0.3997 (10)0.5648 (11)0.2237 (7)0.030 (3)
O39A0.5886 (9)0.3808 (10)0.3087 (7)0.027 (2)
O40A0.7763 (9)0.2702 (11)0.4045 (7)0.030 (3)
W1B0.28500 (6)0.89573 (6)0.78057 (4)0.02576 (14)
W2B0.00805 (6)1.06170 (6)0.67960 (4)0.02648 (14)
W3B0.28826 (6)1.00323 (6)0.57489 (4)0.02721 (14)
W4B0.45052 (6)0.61863 (6)0.77374 (4)0.02643 (14)
W5B0.18881 (6)0.68177 (6)0.86603 (4)0.02589 (14)
W6B0.08422 (6)0.84404 (6)0.76072 (4)0.02613 (14)
W7B0.07457 (5)0.94697 (6)0.57102 (4)0.02616 (14)
W8B0.20857 (5)0.88111 (6)0.47052 (4)0.02518 (14)
W9B0.46105 (5)0.72830 (6)0.56726 (4)0.02652 (14)
W10B0.36317 (6)0.49175 (6)0.65709 (4)0.02731 (14)
W11B0.10511 (6)0.54496 (6)0.75489 (4)0.02588 (14)
W12B0.10685 (6)0.64792 (6)0.56430 (4)0.02617 (14)
P1B0.1922 (4)0.7782 (5)0.6687 (3)0.0219 (8)
O1B0.3175 (10)0.9766 (11)0.8217 (7)0.029 (3)
O2B0.1302 (8)0.9866 (10)0.7499 (6)0.025 (2)
O3B0.3239 (10)0.9437 (11)0.6800 (6)0.027 (2)
O4B0.4279 (10)0.7579 (10)0.7941 (7)0.028 (2)
O5B0.2251 (9)0.8038 (10)0.8653 (6)0.023 (2)
O6B0.2535 (9)0.7532 (10)0.7399 (6)0.025 (2)
O7B0.0521 (10)1.2020 (11)0.6817 (7)0.031 (3)
O8B0.1325 (10)1.0612 (9)0.6062 (6)0.024 (2)
O9B0.0850 (10)0.9948 (11)0.7468 (7)0.030 (3)
O10B0.0791 (11)1.0705 (11)0.6024 (7)0.033 (3)
O11B0.0666 (10)0.8656 (10)0.6694 (6)0.025 (2)
O12B0.3202 (13)1.1247 (13)0.5464 (7)0.039 (3)
O13B0.2408 (10)1.0022 (10)0.4833 (6)0.024 (2)
O14B0.4367 (10)0.8791 (11)0.5611 (6)0.030 (3)
O15B0.2586 (10)0.8244 (11)0.6015 (6)0.027 (2)
O16B0.5857 (10)0.5264 (11)0.8097 (7)0.031 (3)
O17B0.3547 (10)0.5888 (10)0.8594 (7)0.028 (2)
O18B0.4851 (9)0.6866 (11)0.6707 (6)0.026 (2)
O19B0.4135 (11)0.5202 (11)0.7363 (6)0.029 (3)
O20B0.1599 (10)0.6306 (11)0.9581 (6)0.029 (3)
O21B0.0380 (10)0.7849 (10)0.8299 (7)0.028 (2)
O22B0.1703 (9)0.5737 (10)0.8247 (6)0.023 (2)
O23B0.1999 (10)0.8450 (12)0.8189 (7)0.031 (3)
O24B0.1492 (9)0.9040 (10)0.6667 (7)0.027 (2)
O25B0.0219 (9)0.6901 (11)0.7526 (7)0.028 (2)
O26B0.1882 (11)1.0139 (12)0.5104 (7)0.035 (3)
O27B0.0542 (9)0.9521 (11)0.5083 (6)0.026 (2)
O28B0.0162 (9)0.7889 (9)0.5745 (6)0.023 (2)
O29B0.1888 (10)0.9244 (11)0.3778 (6)0.029 (3)
O30B0.3732 (10)0.7856 (12)0.4814 (7)0.032 (3)
O31B0.1829 (9)0.7413 (11)0.5027 (6)0.027 (2)
O32B0.6004 (9)0.6773 (11)0.5336 (7)0.029 (3)
O33B0.4198 (10)0.5990 (11)0.5911 (7)0.029 (3)
O34B0.4721 (11)0.3607 (12)0.6525 (7)0.034 (3)
O35B0.2565 (10)0.4442 (10)0.7303 (7)0.028 (2)
O36B0.2576 (11)0.5220 (11)0.5830 (7)0.031 (3)
O37B0.1927 (10)0.6648 (9)0.6643 (7)0.027 (2)
O38B0.0547 (11)0.4455 (11)0.8109 (7)0.033 (3)
O39B0.0583 (9)0.5645 (10)0.6580 (6)0.027 (2)
O40B0.0542 (12)0.6090 (12)0.5041 (7)0.035 (3)
O11S0.5640 (12)0.9099 (13)0.7449 (8)0.041 (3)
O12S0.8214 (12)0.5389 (14)0.7586 (9)0.053 (4)
N11S0.6885 (14)0.7143 (15)0.7709 (9)0.038 (4)
H11A0.68070.69480.81980.045*
C12S0.6292 (15)0.8277 (19)0.7240 (12)0.039 (4)
N13S0.6611 (13)0.8208 (15)0.6528 (8)0.034 (3)
H13A0.63400.87910.61260.041*
C14S0.7414 (18)0.711 (2)0.6518 (12)0.048 (5)
H14A0.81590.71310.62880.057*
H14B0.71170.67770.62350.057*
C15S0.7572 (14)0.6404 (18)0.7329 (10)0.035 (4)
O21S0.2573 (10)0.0468 (12)0.1061 (7)0.037 (3)
O22S0.0405 (11)0.3550 (12)0.1969 (7)0.037 (3)
N21S0.1446 (14)0.2227 (15)0.1342 (9)0.038 (4)
H21A0.14770.26980.08980.045*
C22S0.1957 (12)0.1059 (17)0.1513 (10)0.030 (4)
N23S0.1727 (13)0.0582 (13)0.2205 (8)0.029 (3)
H23A0.19700.01660.24260.035*
C24S0.1022 (14)0.1475 (18)0.2538 (10)0.034 (4)
H24A0.14040.14170.29760.041*
H24B0.02560.14430.26950.041*
C25S0.0897 (13)0.2568 (18)0.1922 (11)0.033 (4)
O31S0.6244 (12)0.6492 (13)0.9293 (7)0.042 (3)
O32S0.2598 (12)0.8610 (13)1.0077 (7)0.041 (3)
N31S0.4519 (13)0.7778 (15)0.9624 (9)0.039 (4)
H31A0.46510.84090.94330.047*
C32S0.5303 (13)0.6685 (14)0.9602 (9)0.026 (3)
N33S0.4787 (15)0.5935 (17)0.9991 (9)0.043 (4)
H33A0.51090.51791.00730.052*
C34S0.3622 (15)0.6594 (17)1.0244 (11)0.037 (4)
H34A0.30230.64961.00280.044*
H34B0.35530.63461.07950.044*
C35S0.3507 (15)0.7751 (16)0.9983 (9)0.032 (4)
O41S0.7423 (11)0.8810 (12)0.9700 (7)0.037 (3)
O42S0.9170 (14)1.1328 (14)0.8526 (9)0.051 (4)
N41S0.8051 (14)1.0245 (14)0.8993 (9)0.037 (4)
H41A0.74331.07090.87180.045*
C42S0.8178 (19)0.9196 (19)0.9534 (10)0.040 (4)
N43S0.9293 (16)0.8672 (18)0.9850 (10)0.050 (5)
H43A0.95900.80111.01990.061*
C44S0.9844 (15)0.948 (2)0.9466 (13)0.044 (5)
H44A1.00630.97430.98320.053*
H44B1.05550.90920.91940.053*
C45S0.9028 (18)1.044 (2)0.8957 (14)0.050 (6)
O51S0.2438 (10)0.8084 (12)0.2496 (7)0.035 (3)
O52S0.1195 (13)0.6632 (15)0.1058 (8)0.047 (4)
N51S0.1783 (11)0.7587 (13)0.1615 (8)0.028 (3)
H51A0.18880.80900.12090.034*
C52S0.1986 (15)0.7530 (16)0.2332 (11)0.034 (4)
N53S0.1671 (12)0.6717 (14)0.2797 (8)0.030 (3)
C54S0.1341 (15)0.6151 (17)0.2409 (8)0.032 (4)
H54A0.05410.62050.25500.038*
H54B0.18810.53250.25080.038*
C55S0.1413 (14)0.6801 (15)0.1614 (9)0.029 (4)
O61S0.262 (2)0.3989 (18)0.4493 (10)0.072 (6)
O62S0.5802 (15)0.4843 (18)0.4446 (9)0.064 (5)
N61S0.4395 (18)0.4107 (17)0.4572 (11)0.052 (5)
H61A0.47730.34060.48630.062*
C62S0.322 (3)0.453 (3)0.4312 (15)0.063 (7)
N63S0.3002 (13)0.5580 (14)0.3869 (8)0.034 (3)
C64S0.3925 (17)0.5963 (16)0.3839 (10)0.035 (4)
H64A0.36640.66240.40500.042*
H64B0.42180.61820.33220.042*
C65S0.4819 (16)0.4899 (19)0.4316 (10)0.038 (4)
C71S0.1830 (16)0.6370 (18)0.3608 (11)0.039 (4)
H71A0.16010.70770.37640.047*
H71B0.12920.59990.38610.047*
O1W0.5503 (12)0.9421 (12)0.8854 (8)0.043 (3)
O2W0.4125 (12)0.8069 (12)0.1466 (8)0.041 (3)
O3W0.3800 (17)0.3375 (14)0.8981 (11)0.070 (6)
O4W0.9874 (11)0.5576 (11)0.0836 (7)0.039 (3)
O5W0.2477 (15)0.0725 (19)0.9631 (11)0.065 (5)
O6W0.9302 (13)0.4123 (13)0.3241 (8)0.046 (3)
O7W0.7473 (16)0.6829 (15)0.0709 (10)0.059 (4)
O8W0.6186 (14)0.7045 (18)0.1852 (10)0.066 (5)
O9W0.7353 (16)0.3242 (14)0.7712 (8)0.055 (4)
O10W0.6992 (16)0.5738 (18)0.3186 (10)0.073 (5)
O11W0.3862 (17)0.1428 (16)0.8723 (11)0.070 (5)
O12W0.1626 (15)0.3317 (18)0.9750 (9)0.064 (5)
O13W0.0175 (17)0.5272 (15)0.9526 (11)0.071 (5)
O14W0.6103 (16)0.161 (2)0.8070 (11)0.073 (5)
O15W0.9674 (18)0.531 (2)0.3885 (9)0.071 (5)
O16W0.7427 (18)0.332 (2)0.5480 (11)0.096 (8)
O17W0.8394 (18)0.473 (2)0.9142 (11)0.113 (10)
O18W0.992 (3)0.238 (3)0.4653 (15)0.047 (8)0.50
O19W0.774 (2)0.677 (2)0.4218 (15)0.037 (6)0.50
O20W0.001 (3)0.260 (3)0.9504 (16)0.047 (7)0.50
O21W0.759 (2)0.434 (2)0.6399 (13)0.033 (5)0.50
O22W0.082 (2)0.366 (3)0.503 (2)0.053 (9)0.50
O23W0.024 (3)0.423 (3)0.6304 (19)0.058 (10)0.50
O24W0.603 (3)0.200 (3)0.5587 (17)0.053 (7)0.50
O25W0.436 (3)0.141 (3)0.685 (2)0.066 (9)0.50
O26W0.086 (3)0.191 (3)0.840 (3)0.092 (16)0.50
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
W1A0.0258 (3)0.0264 (3)0.0236 (3)0.0100 (3)0.0008 (2)0.0081 (3)
W2A0.0263 (3)0.0256 (3)0.0238 (3)0.0113 (3)0.0002 (2)0.0070 (3)
W3A0.0253 (3)0.0229 (3)0.0265 (3)0.0081 (3)0.0014 (2)0.0079 (3)
W4A0.0264 (3)0.0255 (3)0.0217 (3)0.0093 (3)0.0003 (2)0.0064 (3)
W5A0.0249 (3)0.0255 (3)0.0230 (3)0.0061 (3)0.0027 (2)0.0065 (3)
W6A0.0230 (3)0.0275 (3)0.0239 (3)0.0086 (3)0.0004 (2)0.0073 (3)
W7A0.0255 (3)0.0261 (3)0.0220 (3)0.0104 (3)0.0014 (2)0.0059 (3)
W8A0.0235 (3)0.0239 (3)0.0250 (3)0.0079 (3)0.0028 (2)0.0066 (3)
W9A0.0231 (3)0.0246 (3)0.0255 (3)0.0081 (3)0.0011 (2)0.0075 (3)
W10A0.0246 (3)0.0244 (3)0.0246 (3)0.0092 (3)0.0005 (2)0.0072 (3)
W11A0.0245 (3)0.0229 (3)0.0253 (3)0.0061 (3)0.0006 (2)0.0077 (3)
W12A0.0250 (3)0.0243 (3)0.0233 (3)0.0090 (3)0.0015 (2)0.0076 (3)
P1A0.0201 (16)0.0196 (18)0.0218 (18)0.0061 (14)0.0013 (13)0.0064 (15)
O1A0.037 (6)0.032 (7)0.018 (5)0.019 (5)0.007 (4)0.004 (5)
O2A0.023 (5)0.044 (7)0.021 (5)0.018 (5)0.003 (4)0.008 (5)
O3A0.029 (6)0.031 (7)0.026 (6)0.010 (5)0.004 (5)0.006 (5)
O4A0.034 (6)0.019 (6)0.026 (6)0.006 (5)0.003 (5)0.004 (5)
O5A0.022 (5)0.029 (6)0.029 (6)0.012 (5)0.003 (4)0.001 (5)
O6A0.025 (5)0.031 (6)0.010 (5)0.008 (5)0.001 (4)0.007 (4)
O7A0.039 (6)0.024 (6)0.044 (7)0.016 (5)0.004 (5)0.014 (5)
O8A0.020 (5)0.024 (6)0.027 (6)0.009 (5)0.005 (4)0.007 (5)
O9A0.021 (5)0.031 (6)0.033 (6)0.011 (5)0.006 (4)0.006 (5)
O10A0.038 (6)0.036 (7)0.018 (5)0.023 (5)0.002 (4)0.006 (5)
O11A0.024 (5)0.018 (5)0.025 (6)0.011 (4)0.001 (4)0.005 (4)
O12A0.036 (7)0.020 (6)0.047 (8)0.009 (5)0.006 (6)0.003 (6)
O13A0.019 (5)0.030 (6)0.023 (5)0.005 (5)0.003 (4)0.010 (5)
O14A0.027 (5)0.038 (7)0.017 (5)0.012 (5)0.003 (4)0.010 (5)
O15A0.016 (5)0.024 (6)0.029 (6)0.005 (4)0.001 (4)0.003 (5)
O16A0.033 (6)0.035 (7)0.020 (6)0.017 (5)0.000 (4)0.004 (5)
O17A0.025 (5)0.041 (7)0.023 (6)0.015 (5)0.009 (4)0.010 (5)
O18A0.028 (5)0.029 (6)0.021 (6)0.009 (5)0.005 (4)0.003 (5)
O19A0.030 (5)0.028 (6)0.023 (6)0.012 (5)0.000 (4)0.007 (5)
O20A0.039 (7)0.023 (6)0.027 (6)0.004 (5)0.011 (5)0.003 (5)
O21A0.030 (6)0.036 (7)0.018 (5)0.012 (5)0.004 (4)0.005 (5)
O22A0.022 (5)0.028 (6)0.031 (6)0.002 (5)0.005 (4)0.007 (5)
O23A0.026 (5)0.028 (6)0.031 (6)0.008 (5)0.002 (5)0.017 (5)
O24A0.035 (6)0.016 (5)0.029 (6)0.006 (5)0.003 (5)0.008 (5)
O25A0.030 (6)0.031 (7)0.028 (6)0.018 (5)0.010 (5)0.009 (5)
O26A0.034 (6)0.038 (7)0.039 (7)0.018 (6)0.002 (5)0.017 (6)
O27A0.021 (5)0.023 (6)0.019 (5)0.005 (4)0.005 (4)0.003 (4)
O28A0.022 (5)0.018 (5)0.026 (6)0.011 (4)0.001 (4)0.006 (4)
O29A0.032 (6)0.025 (6)0.028 (6)0.006 (5)0.009 (5)0.001 (5)
O30A0.016 (5)0.028 (6)0.028 (6)0.005 (4)0.005 (4)0.009 (5)
O31A0.025 (4)0.014 (4)0.026 (4)0.002 (3)0.001 (3)0.006 (3)
O32A0.025 (6)0.023 (6)0.043 (7)0.008 (5)0.011 (5)0.017 (6)
O33A0.020 (5)0.017 (5)0.026 (6)0.005 (4)0.003 (4)0.003 (4)
O34A0.030 (6)0.035 (7)0.023 (6)0.012 (5)0.005 (4)0.010 (5)
O35A0.023 (5)0.033 (7)0.019 (5)0.010 (5)0.005 (4)0.004 (5)
O36A0.037 (6)0.031 (6)0.011 (5)0.012 (5)0.004 (4)0.012 (5)
O37A0.032 (6)0.017 (5)0.036 (7)0.008 (5)0.002 (5)0.013 (5)
O38A0.026 (5)0.029 (6)0.025 (6)0.005 (5)0.009 (4)0.011 (5)
O39A0.023 (5)0.027 (6)0.033 (6)0.012 (5)0.001 (4)0.010 (5)
O40A0.020 (5)0.032 (7)0.038 (7)0.005 (5)0.000 (4)0.020 (6)
W1B0.0282 (3)0.0258 (3)0.0244 (3)0.0108 (3)0.0012 (2)0.0084 (3)
W2B0.0285 (3)0.0228 (3)0.0257 (3)0.0072 (3)0.0015 (2)0.0078 (3)
W3B0.0317 (3)0.0270 (3)0.0244 (3)0.0136 (3)0.0010 (2)0.0075 (3)
W4B0.0258 (3)0.0261 (3)0.0255 (3)0.0084 (3)0.0016 (2)0.0073 (3)
W5B0.0289 (3)0.0263 (3)0.0221 (3)0.0110 (3)0.0002 (2)0.0068 (3)
W6B0.0258 (3)0.0277 (4)0.0237 (3)0.0093 (3)0.0018 (2)0.0090 (3)
W7B0.0254 (3)0.0272 (3)0.0243 (3)0.0084 (3)0.0015 (2)0.0080 (3)
W8B0.0268 (3)0.0257 (3)0.0219 (3)0.0098 (3)0.0001 (2)0.0066 (3)
W9B0.0247 (3)0.0282 (4)0.0251 (3)0.0094 (3)0.0009 (2)0.0079 (3)
W10B0.0293 (3)0.0238 (3)0.0273 (3)0.0083 (3)0.0013 (3)0.0095 (3)
W11B0.0301 (3)0.0254 (3)0.0234 (3)0.0120 (3)0.0007 (2)0.0078 (3)
W12B0.0301 (3)0.0268 (3)0.0229 (3)0.0123 (3)0.0007 (2)0.0083 (3)
P1B0.0255 (17)0.0232 (19)0.0173 (18)0.0098 (15)0.0009 (14)0.0059 (15)
O1B0.035 (6)0.030 (7)0.025 (6)0.016 (5)0.001 (5)0.007 (5)
O2B0.014 (5)0.029 (6)0.023 (6)0.004 (4)0.001 (4)0.012 (5)
O3B0.038 (6)0.034 (7)0.015 (5)0.022 (6)0.001 (4)0.004 (5)
O4B0.029 (6)0.022 (6)0.034 (6)0.005 (5)0.001 (5)0.016 (5)
O5B0.029 (5)0.027 (6)0.020 (5)0.014 (5)0.003 (4)0.014 (5)
O6B0.019 (5)0.025 (6)0.028 (6)0.004 (4)0.007 (4)0.007 (5)
O7B0.034 (6)0.023 (6)0.029 (6)0.003 (5)0.001 (5)0.014 (5)
O8B0.032 (6)0.014 (5)0.018 (5)0.003 (5)0.001 (4)0.002 (4)
O9B0.030 (6)0.034 (7)0.026 (6)0.019 (5)0.003 (5)0.004 (5)
O10B0.039 (7)0.030 (7)0.029 (6)0.008 (5)0.011 (5)0.011 (5)
O11B0.035 (6)0.024 (6)0.021 (5)0.016 (5)0.003 (4)0.010 (5)
O12B0.060 (8)0.047 (8)0.019 (6)0.032 (7)0.000 (6)0.005 (6)
O13B0.032 (5)0.018 (5)0.020 (5)0.010 (4)0.000 (4)0.004 (4)
O14B0.027 (5)0.038 (7)0.026 (6)0.013 (5)0.003 (4)0.013 (5)
O15B0.032 (6)0.028 (6)0.021 (6)0.012 (5)0.002 (4)0.010 (5)
O16B0.028 (6)0.025 (6)0.038 (7)0.013 (5)0.011 (5)0.001 (5)
O17B0.032 (6)0.021 (6)0.029 (6)0.009 (5)0.001 (5)0.008 (5)
O18B0.019 (5)0.030 (6)0.023 (6)0.004 (5)0.001 (4)0.010 (5)
O19B0.039 (6)0.032 (7)0.021 (6)0.018 (6)0.003 (5)0.009 (5)
O20B0.035 (6)0.031 (7)0.023 (6)0.013 (5)0.001 (5)0.010 (5)
O21B0.028 (5)0.016 (5)0.036 (7)0.002 (5)0.002 (5)0.013 (5)
O22B0.027 (5)0.025 (6)0.021 (5)0.009 (5)0.006 (4)0.010 (5)
O23B0.032 (6)0.036 (7)0.033 (6)0.017 (6)0.010 (5)0.018 (6)
O24B0.022 (5)0.017 (5)0.036 (6)0.007 (4)0.001 (4)0.001 (5)
O25B0.024 (5)0.030 (6)0.033 (6)0.013 (5)0.001 (4)0.010 (5)
O26B0.030 (6)0.036 (7)0.033 (7)0.010 (6)0.007 (5)0.005 (6)
O27B0.027 (5)0.034 (7)0.013 (5)0.013 (5)0.005 (4)0.004 (5)
O28B0.022 (5)0.009 (5)0.032 (6)0.005 (4)0.001 (4)0.002 (4)
O29B0.036 (6)0.040 (7)0.016 (5)0.019 (6)0.001 (4)0.006 (5)
O30B0.030 (6)0.038 (7)0.024 (6)0.007 (5)0.001 (5)0.016 (5)
O31B0.021 (5)0.029 (6)0.024 (6)0.007 (5)0.000 (4)0.005 (5)
O32B0.013 (4)0.035 (6)0.031 (5)0.001 (4)0.007 (4)0.017 (5)
O33B0.029 (6)0.034 (7)0.025 (6)0.013 (5)0.006 (5)0.011 (5)
O34B0.038 (7)0.030 (7)0.026 (6)0.010 (6)0.001 (5)0.004 (5)
O35B0.029 (6)0.017 (6)0.033 (6)0.004 (5)0.002 (5)0.010 (5)
O36B0.036 (6)0.025 (6)0.028 (6)0.007 (5)0.002 (5)0.010 (5)
O37B0.037 (6)0.013 (5)0.031 (6)0.008 (5)0.006 (5)0.007 (5)
O38B0.034 (6)0.031 (7)0.033 (7)0.014 (5)0.007 (5)0.009 (5)
O39B0.022 (5)0.027 (6)0.024 (6)0.007 (5)0.003 (4)0.002 (5)
O40B0.048 (7)0.030 (7)0.025 (6)0.012 (6)0.012 (5)0.007 (5)
O11S0.047 (8)0.041 (8)0.037 (7)0.023 (7)0.002 (6)0.003 (6)
O12S0.027 (7)0.049 (10)0.069 (10)0.011 (7)0.003 (6)0.008 (8)
N11S0.040 (8)0.037 (9)0.024 (7)0.013 (7)0.005 (6)0.007 (7)
C12S0.025 (8)0.047 (12)0.059 (13)0.026 (8)0.003 (8)0.021 (10)
N13S0.039 (8)0.050 (10)0.015 (6)0.018 (8)0.002 (5)0.011 (7)
C14S0.039 (10)0.076 (17)0.047 (12)0.031 (11)0.005 (9)0.029 (12)
C15S0.022 (8)0.054 (12)0.038 (10)0.027 (9)0.002 (7)0.010 (9)
O21S0.027 (6)0.040 (8)0.038 (7)0.011 (6)0.000 (5)0.008 (6)
O22S0.034 (6)0.038 (8)0.037 (7)0.013 (6)0.007 (5)0.006 (6)
N21S0.041 (8)0.035 (9)0.031 (8)0.016 (7)0.004 (6)0.003 (7)
C22S0.013 (6)0.044 (10)0.040 (10)0.015 (7)0.012 (6)0.023 (8)
N23S0.047 (8)0.021 (7)0.020 (7)0.014 (6)0.007 (6)0.003 (6)
C24S0.024 (8)0.056 (12)0.026 (8)0.021 (8)0.003 (6)0.011 (8)
C25S0.016 (7)0.044 (11)0.047 (11)0.013 (7)0.002 (7)0.023 (9)
O31S0.048 (8)0.049 (9)0.028 (7)0.017 (7)0.010 (6)0.009 (6)
O32S0.042 (7)0.046 (8)0.025 (6)0.009 (6)0.004 (5)0.010 (6)
N31S0.039 (8)0.044 (10)0.034 (8)0.028 (8)0.015 (6)0.009 (7)
C32S0.020 (7)0.021 (8)0.028 (8)0.003 (6)0.011 (6)0.002 (6)
N33S0.043 (9)0.051 (11)0.032 (8)0.004 (8)0.000 (7)0.027 (8)
C34S0.029 (8)0.038 (10)0.043 (11)0.004 (8)0.008 (7)0.027 (9)
C35S0.038 (9)0.027 (9)0.027 (8)0.010 (7)0.020 (7)0.001 (7)
O41S0.041 (7)0.042 (8)0.030 (7)0.020 (6)0.012 (5)0.015 (6)
O42S0.063 (10)0.048 (9)0.048 (9)0.023 (8)0.021 (7)0.028 (8)
N41S0.041 (8)0.027 (8)0.033 (8)0.010 (7)0.006 (6)0.002 (7)
C42S0.055 (12)0.048 (12)0.020 (8)0.020 (10)0.009 (8)0.018 (8)
N43S0.046 (10)0.050 (12)0.033 (9)0.006 (9)0.000 (7)0.002 (8)
C44S0.023 (8)0.051 (13)0.067 (14)0.007 (8)0.007 (8)0.044 (12)
C45S0.037 (10)0.062 (15)0.065 (15)0.023 (11)0.023 (10)0.042 (13)
O51S0.030 (6)0.032 (7)0.042 (7)0.005 (5)0.002 (5)0.020 (6)
O52S0.057 (9)0.068 (11)0.042 (8)0.037 (8)0.001 (6)0.033 (8)
N51S0.027 (6)0.040 (8)0.022 (7)0.012 (6)0.002 (5)0.016 (6)
C52S0.030 (8)0.029 (9)0.042 (10)0.006 (7)0.003 (7)0.019 (8)
N53S0.032 (7)0.038 (8)0.025 (7)0.015 (6)0.001 (5)0.013 (6)
C54S0.038 (9)0.045 (11)0.014 (7)0.023 (8)0.005 (6)0.007 (7)
C55S0.024 (7)0.025 (8)0.022 (8)0.000 (6)0.003 (6)0.002 (7)
O61S0.121 (17)0.074 (13)0.048 (10)0.066 (13)0.042 (10)0.035 (10)
O62S0.061 (10)0.077 (13)0.036 (9)0.003 (9)0.017 (7)0.020 (9)
N61S0.067 (12)0.041 (11)0.044 (10)0.011 (10)0.007 (9)0.027 (9)
C62S0.087 (19)0.058 (17)0.046 (14)0.030 (15)0.019 (13)0.027 (13)
N63S0.040 (8)0.041 (9)0.020 (7)0.012 (7)0.005 (6)0.010 (7)
C64S0.051 (10)0.027 (9)0.020 (8)0.013 (8)0.001 (7)0.003 (7)
C65S0.034 (7)0.048 (9)0.023 (7)0.003 (6)0.015 (6)0.010 (6)
C71S0.038 (10)0.037 (11)0.036 (10)0.010 (9)0.004 (8)0.008 (8)
O1W0.037 (7)0.036 (8)0.054 (9)0.011 (6)0.009 (6)0.020 (7)
O2W0.045 (7)0.035 (7)0.043 (8)0.015 (6)0.008 (6)0.009 (6)
O3W0.096 (14)0.035 (9)0.085 (13)0.025 (9)0.053 (11)0.007 (9)
O4W0.044 (7)0.027 (7)0.044 (8)0.009 (6)0.014 (6)0.020 (6)
O5W0.052 (9)0.088 (14)0.073 (12)0.028 (10)0.006 (8)0.048 (11)
O6W0.047 (8)0.038 (8)0.045 (8)0.012 (7)0.003 (6)0.006 (7)
O7W0.067 (10)0.047 (10)0.059 (10)0.027 (9)0.017 (8)0.002 (8)
O8W0.047 (9)0.076 (13)0.072 (12)0.018 (9)0.018 (8)0.019 (10)
O9W0.086 (12)0.041 (9)0.039 (8)0.029 (9)0.006 (8)0.013 (7)
O10W0.064 (11)0.080 (14)0.061 (11)0.036 (11)0.002 (9)0.008 (10)
O11W0.074 (12)0.045 (10)0.075 (12)0.011 (9)0.008 (9)0.017 (9)
O12W0.059 (10)0.080 (13)0.043 (9)0.023 (10)0.022 (8)0.003 (9)
O13W0.085 (13)0.041 (10)0.078 (13)0.023 (10)0.004 (10)0.012 (9)
O14W0.055 (10)0.093 (16)0.065 (12)0.034 (11)0.003 (8)0.011 (11)
O15W0.090 (13)0.103 (16)0.046 (10)0.067 (13)0.000 (9)0.017 (10)
O16W0.077 (13)0.12 (2)0.059 (12)0.013 (13)0.039 (10)0.035 (13)
O17W0.068 (12)0.107 (19)0.056 (12)0.008 (12)0.003 (9)0.051 (12)
O18W0.062 (18)0.043 (17)0.041 (15)0.038 (15)0.041 (14)0.021 (13)
O19W0.034 (7)0.035 (7)0.034 (7)0.010 (5)0.008 (5)0.006 (5)
O20W0.049 (16)0.054 (19)0.044 (16)0.032 (15)0.001 (12)0.005 (14)
O21W0.040 (7)0.030 (7)0.028 (7)0.010 (5)0.003 (4)0.010 (5)
O22W0.022 (12)0.060 (19)0.10 (3)0.024 (13)0.032 (14)0.056 (19)
O23W0.07 (2)0.08 (2)0.07 (2)0.07 (2)0.056 (18)0.07 (2)
O24W0.059 (9)0.050 (9)0.047 (8)0.013 (5)0.000 (5)0.022 (5)
O25W0.070 (10)0.063 (10)0.062 (10)0.026 (6)0.001 (5)0.018 (5)
O26W0.030 (16)0.05 (2)0.18 (5)0.012 (15)0.01 (2)0.04 (3)
Geometric parameters (Å, °) top
W1A—O1A1.712 (11)W6B—O9B1.937 (13)
W1A—O4A1.897 (12)W6B—O11B2.430 (11)
W1A—O3A1.913 (12)W7B—O26B1.716 (12)
W1A—O5A1.919 (12)W7B—O27B1.886 (10)
W1A—O2A1.921 (11)W7B—O28B1.894 (10)
W1A—O6A2.460 (11)W7B—O10B1.898 (12)
W2A—O7A1.716 (11)W7B—O24B1.945 (11)
W2A—O9A1.898 (12)W7B—O11B2.434 (11)
W2A—O2A1.900 (11)W8B—O29B1.684 (11)
W2A—O8A1.941 (11)W8B—O13B1.918 (11)
W2A—O10A1.951 (11)W8B—O31B1.919 (12)
W2A—O11A2.417 (10)W8B—O27B1.920 (11)
W3A—O12A1.716 (13)W8B—O30B1.934 (12)
W3A—O8A1.870 (10)W8B—O15B2.446 (11)
W3A—O3A1.903 (11)W9B—O32B1.709 (10)
W3A—O13A1.919 (10)W9B—O14B1.865 (13)
W3A—O14A1.943 (11)W9B—O30B1.870 (12)
W3A—O15A2.403 (12)W9B—O18B1.890 (11)
W4A—O16A1.708 (11)W9B—O33B1.911 (12)
W4A—O19A1.891 (12)W9B—O15B2.432 (12)
W4A—O17A1.907 (12)W10B—O34B1.725 (13)
W4A—O4A1.908 (12)W10B—O33B1.893 (12)
W4A—O18A1.942 (11)W10B—O19B1.914 (11)
W4A—O6A2.445 (10)W10B—O36B1.917 (12)
W5A—O20A1.701 (12)W10B—O35B1.941 (12)
W5A—O5A1.880 (13)W10B—O37B2.426 (12)
W5A—O21A1.889 (11)W11B—O38B1.706 (12)
W5A—O22A1.905 (12)W11B—O22B1.872 (10)
W5A—O17A1.955 (11)W11B—O35B1.912 (11)
W5A—O6A2.436 (11)W11B—O25B1.912 (12)
W6A—O23A1.702 (11)W11B—O39B1.917 (11)
W6A—O24A1.895 (12)W11B—O37B2.433 (12)
W6A—O25A1.902 (11)W12B—O40B1.709 (12)
W6A—O9A1.915 (13)W12B—O31B1.898 (11)
W6A—O21A1.929 (11)W12B—O28B1.911 (11)
W6A—O11A2.445 (11)W12B—O36B1.924 (12)
W7A—O26A1.697 (13)W12B—O39B1.938 (11)
W7A—O24A1.886 (12)W12B—O37B2.435 (11)
W7A—O10A1.894 (12)P1B—O15B1.525 (12)
W7A—O27A1.897 (11)P1B—O11B1.526 (13)
W7A—O28A1.913 (10)P1B—O6B1.531 (11)
W7A—O11A2.418 (11)P1B—O37B1.537 (12)
W8A—O29A1.709 (11)O11S—C12S1.20 (3)
W8A—O31A1.895 (11)O12S—C15S1.22 (2)
W8A—O30A1.905 (11)N11S—C15S1.33 (3)
W8A—O27A1.930 (10)N11S—C12S1.42 (3)
W8A—O13A1.946 (12)N11S—H11A0.8800
W8A—O15A2.421 (11)C12S—N13S1.37 (3)
W9A—O32A1.705 (11)N13S—C14S1.39 (3)
W9A—O14A1.881 (13)N13S—H13A0.8800
W9A—O18A1.881 (11)C14S—C15S1.51 (3)
W9A—O33A1.887 (11)C14S—H14A0.9900
W9A—O30A1.942 (11)C14S—H14B0.9900
W9A—O15A2.426 (11)O21S—C22S1.29 (2)
W10A—O34A1.704 (12)O22S—C25S1.21 (2)
W10A—O35A1.887 (11)N21S—C25S1.31 (2)
W10A—O36A1.913 (10)N21S—C22S1.35 (2)
W10A—O19A1.914 (12)N21S—H21A0.8800
W10A—O33A1.916 (11)C22S—N23S1.31 (2)
W10A—O37A2.442 (12)N23S—C24S1.42 (2)
W11A—O38A1.713 (12)N23S—H23A0.8800
W11A—O22A1.909 (12)C24S—C25S1.51 (3)
W11A—O25A1.916 (11)C24S—H24A0.9900
W11A—O35A1.923 (10)C24S—H24B0.9900
W11A—O39A1.933 (11)O31S—C32S1.21 (2)
W11A—O37A2.412 (12)O32S—C35S1.27 (2)
W12A—O40A1.724 (12)N31S—C35S1.37 (2)
W12A—O28A1.892 (10)N31S—C32S1.38 (2)
W12A—O39A1.896 (12)N31S—H31A0.8800
W12A—O31A1.897 (11)C32S—N33S1.38 (3)
W12A—O36A1.928 (11)N33S—C34S1.46 (2)
W12A—O37A2.449 (12)N33S—H33A0.8800
P1A—O6A1.519 (11)C34S—C35S1.41 (3)
P1A—O37A1.529 (12)C34S—H34A0.9900
P1A—O11A1.549 (11)C34S—H34B0.9900
P1A—O15A1.556 (12)O41S—C42S1.23 (2)
W1B—O1B1.718 (12)O42S—C45S1.28 (3)
W1B—O3B1.865 (11)N41S—C45S1.36 (3)
W1B—O2B1.882 (10)N41S—C42S1.40 (3)
W1B—O4B1.933 (12)N41S—H41A0.8800
W1B—O5B1.954 (11)C42S—N43S1.42 (3)
W1B—O6B2.458 (12)N43S—C44S1.47 (3)
W2B—O7B1.703 (12)N43S—H43A0.8800
W2B—O9B1.880 (11)C44S—C45S1.42 (3)
W2B—O2B1.907 (10)C44S—H44A0.9900
W2B—O10B1.909 (11)C44S—H44B0.9900
W2B—O8B1.942 (11)O51S—C52S1.24 (2)
W2B—O11B2.458 (11)O52S—C55S1.24 (2)
W3B—O12B1.736 (13)N51S—C55S1.32 (2)
W3B—O8B1.873 (11)N51S—C52S1.39 (2)
W3B—O13B1.925 (11)N51S—H51A0.8800
W3B—O3B1.936 (10)C52S—N53S1.33 (2)
W3B—O14B1.958 (12)N53S—C54S1.42 (2)
W3B—O15B2.454 (12)N53S—C71S1.47 (2)
W4B—O16B1.717 (11)C54S—C55S1.49 (2)
W4B—O4B1.909 (11)C54S—H54A0.9900
W4B—O19B1.914 (12)C54S—H54B0.9900
W4B—O17B1.917 (12)O61S—C62S1.21 (3)
W4B—O18B1.940 (11)O62S—C65S1.28 (3)
W4B—O6B2.414 (10)N61S—C65S1.31 (3)
W5B—O20B1.701 (12)N61S—C62S1.46 (4)
W5B—O5B1.867 (11)N61S—H61A0.8800
W5B—O21B1.894 (11)C62S—N63S1.31 (3)
W5B—O17B1.948 (12)N63S—C64S1.45 (2)
W5B—O22B1.951 (11)N63S—C71S1.46 (2)
W5B—O6B2.429 (12)C64S—C65S1.49 (3)
W6B—O23B1.698 (11)C64S—H64A0.9900
W6B—O24B1.859 (12)C64S—H64B0.9900
W6B—O25B1.908 (12)C71S—H71A0.9900
W6B—O21B1.913 (12)C71S—H71B0.9900
O1A—W1A—O4A102.7 (5)O19B—W4B—O6B83.8 (5)
O1A—W1A—O3A101.8 (6)O17B—W4B—O6B73.5 (4)
O4A—W1A—O3A89.5 (5)O18B—W4B—O6B83.5 (4)
O1A—W1A—O5A103.5 (5)O20B—W5B—O5B102.0 (5)
O4A—W1A—O5A86.1 (5)O20B—W5B—O21B101.3 (6)
O3A—W1A—O5A154.6 (5)O5B—W5B—O21B91.8 (5)
O1A—W1A—O2A103.4 (5)O20B—W5B—O17B101.7 (5)
O4A—W1A—O2A154.0 (5)O5B—W5B—O17B88.3 (5)
O3A—W1A—O2A86.0 (5)O21B—W5B—O17B156.5 (5)
O5A—W1A—O2A87.1 (5)O20B—W5B—O22B101.3 (5)
O1A—W1A—O6A172.5 (5)O5B—W5B—O22B156.6 (5)
O4A—W1A—O6A72.0 (4)O21B—W5B—O22B85.8 (5)
O3A—W1A—O6A83.6 (5)O17B—W5B—O22B84.9 (5)
O5A—W1A—O6A71.3 (4)O20B—W5B—O6B172.5 (5)
O2A—W1A—O6A82.0 (4)O5B—W5B—O6B73.3 (4)
O7A—W2A—O9A104.5 (5)O21B—W5B—O6B84.9 (4)
O7A—W2A—O2A101.4 (6)O17B—W5B—O6B72.6 (4)
O9A—W2A—O2A89.9 (5)O22B—W5B—O6B83.3 (4)
O7A—W2A—O8A100.9 (5)O23B—W6B—O24B102.9 (6)
O9A—W2A—O8A154.7 (5)O23B—W6B—O25B101.2 (6)
O2A—W2A—O8A84.9 (5)O24B—W6B—O25B91.5 (5)
O7A—W2A—O10A103.1 (6)O23B—W6B—O21B101.7 (6)
O9A—W2A—O10A87.8 (5)O24B—W6B—O21B155.3 (5)
O2A—W2A—O10A155.3 (5)O25B—W6B—O21B84.9 (5)
O8A—W2A—O10A86.7 (5)O23B—W6B—O9B103.1 (6)
O7A—W2A—O11A173.6 (5)O24B—W6B—O9B86.9 (5)
O9A—W2A—O11A71.9 (4)O25B—W6B—O9B155.4 (5)
O2A—W2A—O11A84.1 (5)O21B—W6B—O9B86.4 (5)
O8A—W2A—O11A82.9 (4)O23B—W6B—O11B173.2 (5)
O10A—W2A—O11A71.8 (4)O24B—W6B—O11B72.4 (4)
O12A—W3A—O8A103.2 (6)O25B—W6B—O11B84.0 (4)
O12A—W3A—O3A102.8 (6)O21B—W6B—O11B82.9 (5)
O8A—W3A—O3A86.0 (5)O9B—W6B—O11B72.1 (4)
O12A—W3A—O13A99.9 (6)O26B—W7B—O27B103.5 (5)
O8A—W3A—O13A89.9 (5)O26B—W7B—O28B104.2 (6)
O3A—W3A—O13A157.2 (5)O27B—W7B—O28B86.3 (5)
O12A—W3A—O14A102.0 (6)O26B—W7B—O10B102.8 (6)
O8A—W3A—O14A154.8 (5)O27B—W7B—O10B89.9 (5)
O3A—W3A—O14A87.2 (5)O28B—W7B—O10B152.9 (5)
O13A—W3A—O14A87.1 (5)O26B—W7B—O24B102.5 (5)
O12A—W3A—O15A170.3 (5)O27B—W7B—O24B153.9 (5)
O8A—W3A—O15A83.7 (4)O28B—W7B—O24B86.1 (5)
O3A—W3A—O15A84.1 (5)O10B—W7B—O24B85.7 (5)
O13A—W3A—O15A73.1 (4)O26B—W7B—O11B171.8 (5)
O14A—W3A—O15A71.4 (5)O27B—W7B—O11B83.1 (4)
O16A—W4A—O19A102.6 (6)O28B—W7B—O11B80.9 (4)
O16A—W4A—O17A101.3 (5)O10B—W7B—O11B72.0 (4)
O19A—W4A—O17A91.3 (5)O24B—W7B—O11B71.0 (4)
O16A—W4A—O4A102.5 (6)O29B—W8B—O13B101.6 (5)
O19A—W4A—O4A154.7 (5)O29B—W8B—O31B102.9 (5)
O17A—W4A—O4A86.8 (5)O13B—W8B—O31B155.5 (5)
O16A—W4A—O18A102.9 (5)O29B—W8B—O27B102.6 (5)
O19A—W4A—O18A84.9 (5)O13B—W8B—O27B88.1 (5)
O17A—W4A—O18A155.7 (5)O31B—W8B—O27B85.5 (5)
O4A—W4A—O18A86.5 (5)O29B—W8B—O30B103.9 (6)
O16A—W4A—O6A172.4 (5)O13B—W8B—O30B87.3 (5)
O19A—W4A—O6A83.1 (4)O31B—W8B—O30B87.9 (5)
O17A—W4A—O6A73.3 (4)O27B—W8B—O30B153.5 (5)
O4A—W4A—O6A72.2 (4)O29B—W8B—O15B172.8 (5)
O18A—W4A—O6A82.4 (4)O13B—W8B—O15B73.3 (4)
O20A—W5A—O5A101.7 (5)O31B—W8B—O15B82.4 (4)
O20A—W5A—O21A103.2 (6)O27B—W8B—O15B82.6 (4)
O5A—W5A—O21A90.7 (5)O30B—W8B—O15B71.1 (4)
O20A—W5A—O22A103.5 (5)O32B—W9B—O14B101.2 (6)
O5A—W5A—O22A154.5 (5)O32B—W9B—O30B102.6 (5)
O21A—W5A—O22A87.5 (5)O14B—W9B—O30B89.5 (5)
O20A—W5A—O17A100.5 (6)O32B—W9B—O18B101.7 (5)
O5A—W5A—O17A85.0 (5)O14B—W9B—O18B88.7 (5)
O21A—W5A—O17A156.3 (5)O30B—W9B—O18B155.6 (5)
O22A—W5A—O17A86.6 (5)O32B—W9B—O33B103.7 (6)
O20A—W5A—O6A171.2 (5)O14B—W9B—O33B155.1 (5)
O5A—W5A—O6A72.4 (4)O30B—W9B—O33B86.0 (5)
O21A—W5A—O6A83.7 (4)O18B—W9B—O33B85.5 (5)
O22A—W5A—O6A82.1 (4)O32B—W9B—O15B172.3 (5)
O17A—W5A—O6A72.8 (4)O14B—W9B—O15B73.3 (4)
O23A—W6A—O24A104.4 (5)O30B—W9B—O15B72.4 (4)
O23A—W6A—O25A104.3 (5)O18B—W9B—O15B83.7 (4)
O24A—W6A—O25A90.0 (5)O33B—W9B—O15B82.0 (5)
O23A—W6A—O9A101.4 (5)O34B—W10B—O33B102.2 (6)
O24A—W6A—O9A87.6 (5)O34B—W10B—O19B102.3 (6)
O25A—W6A—O9A154.0 (5)O33B—W10B—O19B86.6 (5)
O23A—W6A—O21A102.8 (5)O34B—W10B—O36B102.4 (6)
O24A—W6A—O21A152.7 (5)O33B—W10B—O36B90.6 (5)
O25A—W6A—O21A85.6 (5)O19B—W10B—O36B155.2 (5)
O9A—W6A—O21A84.7 (5)O34B—W10B—O35B102.2 (5)
O23A—W6A—O11A171.1 (5)O33B—W10B—O35B155.4 (5)
O24A—W6A—O11A71.4 (4)O19B—W10B—O35B85.9 (5)
O25A—W6A—O11A83.7 (4)O36B—W10B—O35B86.5 (5)
O9A—W6A—O11A71.0 (4)O34B—W10B—O37B172.6 (5)
O21A—W6A—O11A81.4 (4)O33B—W10B—O37B83.6 (5)
O26A—W7A—O24A101.9 (6)O19B—W10B—O37B82.4 (5)
O26A—W7A—O10A102.6 (5)O36B—W10B—O37B72.8 (5)
O24A—W7A—O10A88.6 (5)O35B—W10B—O37B72.2 (4)
O26A—W7A—O27A102.4 (5)O38B—W11B—O22B101.6 (5)
O24A—W7A—O27A155.6 (5)O38B—W11B—O35B100.1 (6)
O10A—W7A—O27A87.5 (5)O22B—W11B—O35B89.8 (5)
O26A—W7A—O28A102.3 (5)O38B—W11B—O25B103.6 (5)
O24A—W7A—O28A87.1 (5)O22B—W11B—O25B86.0 (5)
O10A—W7A—O28A155.1 (5)O35B—W11B—O25B156.2 (5)
O27A—W7A—O28A86.4 (5)O38B—W11B—O39B102.2 (6)
O26A—W7A—O11A172.2 (5)O22B—W11B—O39B156.2 (5)
O24A—W7A—O11A72.1 (4)O35B—W11B—O39B87.4 (5)
O10A—W7A—O11A72.7 (4)O25B—W11B—O39B87.1 (5)
O27A—W7A—O11A83.7 (4)O38B—W11B—O37B171.0 (5)
O28A—W7A—O11A82.7 (4)O22B—W11B—O37B83.8 (4)
O29A—W8A—O31A103.4 (5)O35B—W11B—O37B72.5 (5)
O29A—W8A—O30A102.3 (5)O25B—W11B—O37B83.8 (4)
O31A—W8A—O30A89.5 (5)O39B—W11B—O37B72.8 (4)
O29A—W8A—O27A101.9 (5)O40B—W12B—O31B105.1 (6)
O31A—W8A—O27A86.3 (5)O40B—W12B—O28B104.2 (6)
O30A—W8A—O27A155.8 (4)O31B—W12B—O28B86.5 (5)
O29A—W8A—O13A100.8 (5)O40B—W12B—O36B100.1 (6)
O31A—W8A—O13A155.7 (5)O31B—W12B—O36B87.5 (5)
O30A—W8A—O13A87.7 (5)O28B—W12B—O36B155.7 (5)
O27A—W8A—O13A86.5 (5)O40B—W12B—O39B99.3 (6)
O29A—W8A—O15A171.6 (5)O31B—W12B—O39B155.5 (5)
O31A—W8A—O15A83.8 (4)O28B—W12B—O39B89.6 (5)
O30A—W8A—O15A73.1 (4)O36B—W12B—O39B86.3 (5)
O27A—W8A—O15A82.8 (4)O40B—W12B—O37B169.0 (5)
O13A—W8A—O15A72.3 (4)O31B—W12B—O37B83.0 (4)
O32A—W9A—O14A101.0 (5)O28B—W12B—O37B83.4 (4)
O32A—W9A—O18A102.8 (6)O36B—W12B—O37B72.5 (5)
O14A—W9A—O18A88.8 (5)O39B—W12B—O37B72.5 (4)
O32A—W9A—O33A103.0 (5)O15B—P1B—O11B110.4 (7)
O14A—W9A—O33A156.0 (5)O15B—P1B—O6B108.7 (7)
O18A—W9A—O33A86.3 (5)O11B—P1B—O6B110.7 (7)
O32A—W9A—O30A100.9 (5)O15B—P1B—O37B109.4 (7)
O14A—W9A—O30A87.1 (5)O11B—P1B—O37B108.8 (7)
O18A—W9A—O30A156.3 (5)O6B—P1B—O37B108.8 (7)
O33A—W9A—O30A88.1 (5)W1B—O2B—W2B154.2 (6)
O32A—W9A—O15A170.1 (5)W1B—O3B—W3B152.4 (6)
O14A—W9A—O15A71.8 (4)W4B—O4B—W1B125.6 (6)
O18A—W9A—O15A84.1 (4)W5B—O5B—W1B126.8 (6)
O33A—W9A—O15A84.3 (4)P1B—O6B—W4B126.7 (7)
O30A—W9A—O15A72.4 (4)P1B—O6B—W5B125.1 (6)
O34A—W10A—O35A103.1 (5)W4B—O6B—W5B89.6 (4)
O34A—W10A—O36A102.3 (5)P1B—O6B—W1B125.8 (7)
O35A—W10A—O36A88.3 (5)W4B—O6B—W1B89.1 (3)
O34A—W10A—O19A103.7 (5)W5B—O6B—W1B88.7 (4)
O35A—W10A—O19A87.2 (5)W3B—O8B—W2B152.5 (6)
O36A—W10A—O19A153.9 (5)W2B—O9B—W6B126.9 (7)
O34A—W10A—O33A102.5 (5)W7B—O10B—W2B127.9 (7)
O35A—W10A—O33A154.2 (5)P1B—O11B—W6B126.8 (6)
O36A—W10A—O33A89.2 (5)P1B—O11B—W7B127.0 (6)
O19A—W10A—O33A83.9 (5)W6B—O11B—W7B89.1 (4)
O34A—W10A—O37A172.5 (5)P1B—O11B—W2B124.5 (6)
O35A—W10A—O37A71.7 (4)W6B—O11B—W2B88.6 (4)
O36A—W10A—O37A72.6 (4)W7B—O11B—W2B88.7 (4)
O19A—W10A—O37A81.6 (4)W8B—O13B—W3B125.3 (6)
O33A—W10A—O37A83.1 (4)W9B—O14B—W3B126.5 (6)
O38A—W11A—O22A103.2 (5)P1B—O15B—W9B127.2 (7)
O38A—W11A—O25A102.7 (5)P1B—O15B—W8B126.0 (6)
O22A—W11A—O25A85.4 (5)W9B—O15B—W8B88.7 (4)
O38A—W11A—O35A101.5 (5)P1B—O15B—W3B125.6 (7)
O22A—W11A—O35A88.8 (5)W9B—O15B—W3B88.7 (4)
O25A—W11A—O35A155.8 (5)W8B—O15B—W3B88.3 (4)
O38A—W11A—O39A101.5 (5)W4B—O17B—W5B124.0 (6)
O22A—W11A—O39A155.3 (5)W9B—O18B—W4B151.3 (6)
O25A—W11A—O39A88.2 (5)W10B—O19B—W4B150.4 (7)
O35A—W11A—O39A87.3 (5)W5B—O21B—W6B152.0 (7)
O38A—W11A—O37A171.1 (5)W11B—O22B—W5B150.5 (6)
O22A—W11A—O37A82.8 (5)W6B—O24B—W7B127.4 (6)
O25A—W11A—O37A84.1 (5)W6B—O25B—W11B151.6 (6)
O35A—W11A—O37A71.8 (5)W7B—O27B—W8B152.6 (7)
O39A—W11A—O37A72.8 (5)W7B—O28B—W12B151.9 (6)
O40A—W12A—O28A103.9 (5)W9B—O30B—W8B127.4 (6)
O40A—W12A—O39A100.6 (5)W12B—O31B—W8B151.6 (7)
O28A—W12A—O39A89.3 (5)W10B—O33B—W9B152.6 (7)
O40A—W12A—O31A104.4 (5)W11B—O35B—W10B125.5 (6)
O28A—W12A—O31A85.4 (5)W10B—O36B—W12B125.4 (7)
O39A—W12A—O31A155.1 (5)P1B—O37B—W10B126.2 (7)
O40A—W12A—O36A101.2 (5)P1B—O37B—W11B126.2 (7)
O28A—W12A—O36A154.8 (5)W10B—O37B—W11B89.6 (4)
O39A—W12A—O36A87.4 (5)P1B—O37B—W12B124.6 (6)
O31A—W12A—O36A87.2 (5)W10B—O37B—W12B89.2 (4)
O40A—W12A—O37A170.4 (5)W11B—O37B—W12B89.4 (4)
O28A—W12A—O37A83.0 (4)W11B—O39B—W12B125.3 (6)
O39A—W12A—O37A72.5 (4)C15S—N11S—C12S112.8 (16)
O31A—W12A—O37A82.6 (4)C15S—N11S—H11A123.6
O36A—W12A—O37A72.2 (4)C12S—N11S—H11A123.6
O6A—P1A—O37A108.7 (7)O11S—C12S—N13S129 (2)
O6A—P1A—O11A109.0 (6)O11S—C12S—N11S125 (2)
O37A—P1A—O11A110.7 (7)N13S—C12S—N11S105.4 (18)
O6A—P1A—O15A108.8 (7)C12S—N13S—C14S111.8 (17)
O37A—P1A—O15A110.7 (7)C12S—N13S—H13A124.1
O11A—P1A—O15A109.1 (6)C14S—N13S—H13A124.1
W2A—O2A—W1A151.9 (6)N13S—C14S—C15S104.9 (17)
W3A—O3A—W1A150.8 (7)N13S—C14S—H14A110.8
W1A—O4A—W4A127.5 (7)C15S—C14S—H14A110.8
W5A—O5A—W1A127.9 (6)N13S—C14S—H14B110.8
P1A—O6A—W5A125.7 (6)C15S—C14S—H14B110.8
P1A—O6A—W4A126.5 (6)H14A—C14S—H14B108.8
W5A—O6A—W4A89.0 (3)O12S—C15S—N11S127.1 (19)
P1A—O6A—W1A126.7 (7)O12S—C15S—C14S128 (2)
W5A—O6A—W1A88.4 (3)N11S—C15S—C14S105.0 (18)
W4A—O6A—W1A88.2 (3)C25S—N21S—C22S111.3 (16)
W3A—O8A—W2A152.5 (7)C25S—N21S—H21A124.3
W2A—O9A—W6A127.6 (6)C22S—N21S—H21A124.3
W7A—O10A—W2A125.4 (6)O21S—C22S—N23S123.2 (18)
P1A—O11A—W2A126.1 (6)O21S—C22S—N21S125.8 (17)
P1A—O11A—W7A125.1 (6)N23S—C22S—N21S111.1 (15)
W2A—O11A—W7A89.9 (4)C22S—N23S—C24S108.6 (15)
P1A—O11A—W6A126.1 (6)C22S—N23S—H23A125.7
W2A—O11A—W6A89.4 (3)C24S—N23S—H23A125.7
W7A—O11A—W6A88.6 (4)N23S—C24S—C25S103.4 (14)
W3A—O13A—W8A124.3 (6)N23S—C24S—H24A111.1
W9A—O14A—W3A126.7 (6)C25S—C24S—H24A111.1
P1A—O15A—W3A126.5 (6)N23S—C24S—H24B111.1
P1A—O15A—W8A124.8 (7)C25S—C24S—H24B111.1
W3A—O15A—W8A90.2 (4)H24A—C24S—H24B109.1
P1A—O15A—W9A124.6 (6)O22S—C25S—N21S128 (2)
W3A—O15A—W9A90.1 (4)O22S—C25S—C24S126.3 (17)
W8A—O15A—W9A89.5 (3)N21S—C25S—C24S105.6 (17)
W4A—O17A—W5A124.8 (6)C35S—N31S—C32S111.1 (15)
W9A—O18A—W4A150.6 (7)C35S—N31S—H31A124.4
W4A—O19A—W10A154.2 (7)C32S—N31S—H31A124.4
W5A—O21A—W6A151.0 (7)O31S—C32S—N31S123.5 (16)
W5A—O22A—W11A151.1 (7)O31S—C32S—N33S130.1 (17)
W7A—O24A—W6A127.8 (7)N31S—C32S—N33S106.3 (14)
W6A—O25A—W11A152.6 (7)C32S—N33S—C34S109.5 (17)
W7A—O27A—W8A150.2 (7)C32S—N33S—H33A125.3
W12A—O28A—W7A152.7 (7)C34S—N33S—H33A125.3
W8A—O30A—W9A125.0 (5)C35S—C34S—N33S104.1 (17)
W8A—O31A—W12A153.0 (6)C35S—C34S—H34A110.9
W9A—O33A—W10A152.7 (6)N33S—C34S—H34A110.9
W10A—O35A—W11A127.0 (7)C35S—C34S—H34B110.9
W10A—O36A—W12A126.1 (6)N33S—C34S—H34B110.9
P1A—O37A—W11A126.3 (6)H34A—C34S—H34B109.0
P1A—O37A—W10A127.0 (7)O32S—C35S—N31S127.0 (17)
W11A—O37A—W10A89.3 (4)O32S—C35S—C34S124.1 (17)
P1A—O37A—W12A124.5 (7)N31S—C35S—C34S108.9 (16)
W11A—O37A—W12A89.0 (4)C45S—N41S—C42S109.8 (19)
W10A—O37A—W12A88.9 (4)C45S—N41S—H41A125.1
W12A—O39A—W11A125.6 (7)C42S—N41S—H41A125.1
O1B—W1B—O3B104.5 (5)O41S—C42S—N41S124 (2)
O1B—W1B—O2B104.7 (6)O41S—C42S—N43S126 (2)
O3B—W1B—O2B85.3 (5)N41S—C42S—N43S109.4 (18)
O1B—W1B—O4B101.4 (5)C42S—N43S—C44S104.6 (17)
O3B—W1B—O4B89.8 (5)C42S—N43S—H43A127.7
O2B—W1B—O4B153.9 (5)C44S—N43S—H43A127.7
O1B—W1B—O5B102.0 (5)C45S—C44S—N43S107.7 (16)
O3B—W1B—O5B153.5 (5)C45S—C44S—H44A110.2
O2B—W1B—O5B87.5 (5)N43S—C44S—H44A110.2
O4B—W1B—O5B85.6 (5)C45S—C44S—H44B110.2
O1B—W1B—O6B170.5 (5)N43S—C44S—H44B110.2
O3B—W1B—O6B82.5 (4)H44A—C44S—H44B108.5
O2B—W1B—O6B82.0 (4)O42S—C45S—N41S125 (2)
O4B—W1B—O6B71.9 (4)O42S—C45S—C44S127 (2)
O5B—W1B—O6B71.2 (4)N41S—C45S—C44S108 (2)
O7B—W2B—O9B103.9 (6)C55S—N51S—C52S112.3 (15)
O7B—W2B—O2B104.3 (5)C55S—N51S—H51A123.8
O9B—W2B—O2B91.1 (5)C52S—N51S—H51A123.8
O7B—W2B—O10B101.0 (6)O51S—C52S—N53S127.1 (18)
O9B—W2B—O10B86.3 (6)O51S—C52S—N51S126.2 (18)
O2B—W2B—O10B154.4 (5)N53S—C52S—N51S106.5 (15)
O7B—W2B—O8B101.8 (5)C52S—N53S—C54S111.7 (14)
O9B—W2B—O8B154.3 (5)C52S—N53S—C71S121.7 (15)
O2B—W2B—O8B84.2 (5)C54S—N53S—C71S126.1 (15)
O10B—W2B—O8B87.1 (5)N53S—C54S—C55S102.9 (14)
O7B—W2B—O11B171.4 (5)N53S—C54S—H54A111.2
O9B—W2B—O11B72.3 (5)C55S—C54S—H54A111.2
O2B—W2B—O11B83.6 (4)N53S—C54S—H54B111.2
O10B—W2B—O11B71.3 (5)C55S—C54S—H54B111.2
O8B—W2B—O11B82.1 (4)H54A—C54S—H54B109.1
O12B—W3B—O8B103.1 (6)O52S—C55S—N51S126.4 (16)
O12B—W3B—O13B102.2 (5)O52S—C55S—C54S127.3 (17)
O8B—W3B—O13B89.9 (5)N51S—C55S—C54S106.3 (14)
O12B—W3B—O3B102.8 (5)C65S—N61S—C62S111 (2)
O8B—W3B—O3B85.7 (5)C65S—N61S—H61A124.3
O13B—W3B—O3B155.0 (5)C62S—N61S—H61A124.3
O12B—W3B—O14B103.1 (6)O61S—C62S—N63S131 (3)
O8B—W3B—O14B153.7 (5)O61S—C62S—N61S124 (3)
O13B—W3B—O14B87.0 (5)N63S—C62S—N61S105 (2)
O3B—W3B—O14B86.1 (5)C62S—N63S—C64S113.7 (18)
O12B—W3B—O15B172.6 (5)C62S—N63S—C71S121 (2)
O8B—W3B—O15B82.7 (4)C64S—N63S—C71S123.1 (16)
O13B—W3B—O15B73.0 (4)N63S—C64S—C65S101.2 (15)
O3B—W3B—O15B82.0 (4)N63S—C64S—H64A111.5
O14B—W3B—O15B71.4 (4)C65S—C64S—H64A111.5
O16B—W4B—O4B102.0 (5)N63S—C64S—H64B111.5
O16B—W4B—O19B101.1 (6)C65S—C64S—H64B111.5
O4B—W4B—O19B156.9 (5)H64A—C64S—H64B109.4
O16B—W4B—O17B100.3 (5)O62S—C65S—N61S129 (2)
O4B—W4B—O17B88.5 (5)O62S—C65S—C64S123 (2)
O19B—W4B—O17B87.9 (5)N61S—C65S—C64S108.4 (17)
O16B—W4B—O18B103.0 (5)N63S—C71S—N53S115.7 (15)
O4B—W4B—O18B88.4 (5)N63S—C71S—H71A108.3
O19B—W4B—O18B86.0 (5)N53S—C71S—H71A108.4
O17B—W4B—O18B156.7 (5)N63S—C71S—H71B108.4
O16B—W4B—O6B172.0 (5)N53S—C71S—H71B108.3
O4B—W4B—O6B73.3 (4)H71A—C71S—H71B107.4
O7A—W2A—O2A—W1A126.1 (16)O17B—W5B—O5B—W1B71.1 (8)
O9A—W2A—O2A—W1A129.1 (16)O22B—W5B—O5B—W1B1.9 (17)
O8A—W2A—O2A—W1A26.0 (16)O6B—W5B—O5B—W1B1.2 (6)
O10A—W2A—O2A—W1A45 (3)O1B—W1B—O5B—W5B171.9 (7)
O11A—W2A—O2A—W1A57.3 (16)O3B—W1B—O5B—W5B9.4 (16)
O1A—W1A—O2A—W2A127.7 (16)O2B—W1B—O5B—W5B83.7 (8)
O4A—W1A—O2A—W2A54 (2)O4B—W1B—O5B—W5B71.2 (8)
O3A—W1A—O2A—W2A26.5 (16)O6B—W1B—O5B—W5B1.2 (6)
O5A—W1A—O2A—W2A129.0 (16)O15B—P1B—O6B—W4B60.5 (10)
O6A—W1A—O2A—W2A57.5 (16)O11B—P1B—O6B—W4B178.0 (7)
O12A—W3A—O3A—W1A130.6 (14)O37B—P1B—O6B—W4B58.5 (10)
O8A—W3A—O3A—W1A28.0 (14)O15B—P1B—O6B—W5B178.6 (7)
O13A—W3A—O3A—W1A52 (2)O11B—P1B—O6B—W5B57.1 (10)
O14A—W3A—O3A—W1A127.7 (15)O37B—P1B—O6B—W5B62.4 (9)
O15A—W3A—O3A—W1A56.2 (14)O15B—P1B—O6B—W1B60.3 (9)
O1A—W1A—O3A—W3A130.3 (14)O11B—P1B—O6B—W1B61.2 (9)
O4A—W1A—O3A—W3A126.8 (15)O37B—P1B—O6B—W1B179.3 (7)
O5A—W1A—O3A—W3A47 (2)O16B—W4B—O6B—P1B171 (3)
O2A—W1A—O3A—W3A27.5 (14)O4B—W4B—O6B—P1B134.8 (9)
O6A—W1A—O3A—W3A54.9 (14)O19B—W4B—O6B—P1B42.1 (9)
O1A—W1A—O4A—W4A170.9 (8)O17B—W4B—O6B—P1B131.7 (9)
O3A—W1A—O4A—W4A87.1 (8)O18B—W4B—O6B—P1B44.5 (8)
O5A—W1A—O4A—W4A67.9 (8)O16B—W4B—O6B—W5B35 (3)
O2A—W1A—O4A—W4A7.4 (17)O4B—W4B—O6B—W5B89.8 (5)
O6A—W1A—O4A—W4A3.7 (7)O19B—W4B—O6B—W5B93.3 (4)
O16A—W4A—O4A—W1A170.7 (8)O17B—W4B—O6B—W5B3.7 (4)
O19A—W4A—O4A—W1A16.5 (17)O18B—W4B—O6B—W5B179.9 (5)
O17A—W4A—O4A—W1A69.8 (8)O16B—W4B—O6B—W1B54 (3)
O18A—W4A—O4A—W1A86.9 (8)O4B—W4B—O6B—W1B1.1 (4)
O6A—W4A—O4A—W1A3.7 (7)O19B—W4B—O6B—W1B178.0 (4)
O20A—W5A—O5A—W1A172.2 (8)O17B—W4B—O6B—W1B92.4 (5)
O21A—W5A—O5A—W1A84.1 (8)O18B—W4B—O6B—W1B91.3 (5)
O22A—W5A—O5A—W1A1.4 (16)O20B—W5B—O6B—P1B174 (4)
O17A—W5A—O5A—W1A72.6 (8)O5B—W5B—O6B—P1B133.6 (9)
O6A—W5A—O5A—W1A1.0 (6)O21B—W5B—O6B—P1B40.2 (8)
O1A—W1A—O5A—W5A173.5 (7)O17B—W5B—O6B—P1B132.9 (9)
O4A—W1A—O5A—W5A71.3 (8)O22B—W5B—O6B—P1B46.1 (8)
O3A—W1A—O5A—W5A9.2 (16)O20B—W5B—O6B—W4B38 (4)
O2A—W1A—O5A—W5A83.5 (8)O5B—W5B—O6B—W4B89.9 (5)
O6A—W1A—O5A—W5A1.0 (6)O21B—W5B—O6B—W4B176.7 (5)
O37A—P1A—O6A—W5A61.9 (9)O17B—W5B—O6B—W4B3.6 (4)
O11A—P1A—O6A—W5A58.8 (9)O22B—W5B—O6B—W4B90.4 (4)
O15A—P1A—O6A—W5A177.6 (7)O20B—W5B—O6B—W1B51 (4)
O37A—P1A—O6A—W4A58.5 (10)O5B—W5B—O6B—W1B0.8 (4)
O11A—P1A—O6A—W4A179.1 (7)O21B—W5B—O6B—W1B94.2 (4)
O15A—P1A—O6A—W4A62.1 (9)O17B—W5B—O6B—W1B92.7 (4)
O37A—P1A—O6A—W1A178.6 (7)O22B—W5B—O6B—W1B179.5 (4)
O11A—P1A—O6A—W1A60.8 (9)O1B—W1B—O6B—P1B179 (3)
O15A—P1A—O6A—W1A58.0 (9)O3B—W1B—O6B—P1B43.2 (8)
O20A—W5A—O6A—P1A176 (3)O2B—W1B—O6B—P1B43.1 (8)
O5A—W5A—O6A—P1A135.2 (9)O4B—W1B—O6B—P1B135.4 (9)
O21A—W5A—O6A—P1A42.5 (8)O5B—W1B—O6B—P1B133.1 (9)
O22A—W5A—O6A—P1A45.9 (8)O1B—W1B—O6B—W4B45 (3)
O17A—W5A—O6A—P1A134.7 (9)O3B—W1B—O6B—W4B93.3 (5)
O20A—W5A—O6A—W4A40 (3)O2B—W1B—O6B—W4B179.6 (5)
O5A—W5A—O6A—W4A88.8 (4)O4B—W1B—O6B—W4B1.1 (4)
O21A—W5A—O6A—W4A178.5 (5)O5B—W1B—O6B—W4B90.4 (4)
O22A—W5A—O6A—W4A90.2 (5)O1B—W1B—O6B—W5B45 (3)
O17A—W5A—O6A—W4A1.3 (4)O3B—W1B—O6B—W5B177.1 (5)
O20A—W5A—O6A—W1A48 (3)O2B—W1B—O6B—W5B90.8 (4)
O5A—W5A—O6A—W1A0.6 (4)O4B—W1B—O6B—W5B90.7 (5)
O21A—W5A—O6A—W1A93.3 (4)O5B—W1B—O6B—W5B0.8 (4)
O22A—W5A—O6A—W1A178.3 (5)O12B—W3B—O8B—W2B124.8 (14)
O17A—W5A—O6A—W1A89.5 (5)O13B—W3B—O8B—W2B132.7 (15)
O16A—W4A—O6A—P1A180 (88)O3B—W3B—O8B—W2B22.6 (14)
O19A—W4A—O6A—P1A40.7 (8)O14B—W3B—O8B—W2B50 (2)
O17A—W4A—O6A—P1A134.2 (9)O15B—W3B—O8B—W2B59.8 (14)
O4A—W4A—O6A—P1A133.8 (9)O7B—W2B—O8B—W3B126.6 (14)
O18A—W4A—O6A—P1A45.1 (9)O9B—W2B—O8B—W3B57 (2)
O16A—W4A—O6A—W5A44 (4)O2B—W2B—O8B—W3B23.1 (14)
O19A—W4A—O6A—W5A94.8 (5)O10B—W2B—O8B—W3B132.8 (15)
O17A—W4A—O6A—W5A1.3 (4)O11B—W2B—O8B—W3B61.2 (14)
O4A—W4A—O6A—W5A90.7 (5)O7B—W2B—O9B—W6B169.0 (8)
O18A—W4A—O6A—W5A179.5 (5)O2B—W2B—O9B—W6B86.0 (8)
O16A—W4A—O6A—W1A44 (4)O10B—W2B—O9B—W6B68.5 (8)
O19A—W4A—O6A—W1A176.8 (5)O8B—W2B—O9B—W6B7.1 (17)
O17A—W4A—O6A—W1A89.7 (5)O11B—W2B—O9B—W6B3.0 (7)
O4A—W4A—O6A—W1A2.3 (4)O23B—W6B—O9B—W2B172.0 (8)
O18A—W4A—O6A—W1A91.0 (4)O24B—W6B—O9B—W2B69.5 (8)
O1A—W1A—O6A—P1A179 (3)O25B—W6B—O9B—W2B17.4 (17)
O4A—W1A—O6A—P1A133.6 (9)O21B—W6B—O9B—W2B86.8 (8)
O3A—W1A—O6A—P1A42.1 (8)O11B—W6B—O9B—W2B3.0 (7)
O5A—W1A—O6A—P1A134.4 (8)O26B—W7B—O10B—W2B171.5 (8)
O2A—W1A—O6A—P1A44.8 (8)O27B—W7B—O10B—W2B84.7 (9)
O1A—W1A—O6A—W5A46 (4)O28B—W7B—O10B—W2B3.0 (17)
O4A—W1A—O6A—W5A91.4 (4)O24B—W7B—O10B—W2B69.6 (9)
O3A—W1A—O6A—W5A177.1 (4)O11B—W7B—O10B—W2B1.9 (7)
O5A—W1A—O6A—W5A0.6 (4)O7B—W2B—O10B—W7B174.1 (8)
O2A—W1A—O6A—W5A90.2 (4)O9B—W2B—O10B—W7B70.7 (9)
O1A—W1A—O6A—W4A43 (4)O2B—W2B—O10B—W7B14.3 (18)
O4A—W1A—O6A—W4A2.3 (4)O8B—W2B—O10B—W7B84.5 (9)
O3A—W1A—O6A—W4A93.8 (4)O11B—W2B—O10B—W7B1.8 (7)
O5A—W1A—O6A—W4A89.7 (4)O15B—P1B—O11B—W6B179.6 (7)
O2A—W1A—O6A—W4A179.3 (4)O6B—P1B—O11B—W6B60.0 (9)
O12A—W3A—O8A—W2A130.7 (14)O37B—P1B—O11B—W6B59.5 (9)
O3A—W3A—O8A—W2A28.4 (15)O15B—P1B—O11B—W7B57.0 (9)
O13A—W3A—O8A—W2A129.2 (15)O6B—P1B—O11B—W7B177.5 (7)
O14A—W3A—O8A—W2A46 (2)O37B—P1B—O11B—W7B63.0 (9)
O15A—W3A—O8A—W2A56.1 (14)O15B—P1B—O11B—W2B61.9 (9)
O7A—W2A—O8A—W3A128.4 (15)O6B—P1B—O11B—W2B58.6 (9)
O9A—W2A—O8A—W3A51 (2)O37B—P1B—O11B—W2B178.1 (7)
O2A—W2A—O8A—W3A27.8 (15)O23B—W6B—O11B—P1B177 (4)
O10A—W2A—O8A—W3A128.9 (15)O24B—W6B—O11B—P1B135.8 (9)
O11A—W2A—O8A—W3A56.8 (14)O25B—W6B—O11B—P1B42.3 (8)
O7A—W2A—O9A—W6A170.9 (8)O21B—W6B—O11B—P1B43.3 (8)
O2A—W2A—O9A—W6A87.4 (8)O9B—W6B—O11B—P1B131.8 (9)
O8A—W2A—O9A—W6A9.4 (17)O23B—W6B—O11B—W7B45 (4)
O10A—W2A—O9A—W6A68.0 (8)O24B—W6B—O11B—W7B1.8 (4)
O11A—W2A—O9A—W6A3.6 (7)O25B—W6B—O11B—W7B95.3 (4)
O23A—W6A—O9A—W2A171.8 (8)O21B—W6B—O11B—W7B179.1 (4)
O24A—W6A—O9A—W2A67.5 (8)O9B—W6B—O11B—W7B90.6 (5)
O25A—W6A—O9A—W2A17.6 (16)O23B—W6B—O11B—W2B43 (4)
O21A—W6A—O9A—W2A86.2 (8)O24B—W6B—O11B—W2B90.6 (5)
O11A—W6A—O9A—W2A3.6 (7)O25B—W6B—O11B—W2B175.9 (4)
O26A—W7A—O10A—W2A169.2 (8)O21B—W6B—O11B—W2B90.3 (4)
O24A—W7A—O10A—W2A67.3 (8)O9B—W6B—O11B—W2B1.9 (4)
O27A—W7A—O10A—W2A88.7 (8)O26B—W7B—O11B—P1B175 (3)
O28A—W7A—O10A—W2A12.8 (17)O27B—W7B—O11B—P1B40.5 (8)
O11A—W7A—O10A—W2A4.5 (7)O28B—W7B—O11B—P1B46.8 (8)
O7A—W2A—O10A—W7A171.5 (8)O10B—W7B—O11B—P1B132.6 (9)
O9A—W2A—O10A—W7A67.2 (8)O24B—W7B—O11B—P1B135.8 (9)
O2A—W2A—O10A—W7A17.8 (18)O26B—W7B—O11B—W6B38 (4)
O8A—W2A—O10A—W7A88.1 (8)O27B—W7B—O11B—W6B178.1 (5)
O11A—W2A—O10A—W7A4.5 (7)O28B—W7B—O11B—W6B90.7 (4)
O6A—P1A—O11A—W2A58.7 (9)O10B—W7B—O11B—W6B89.8 (5)
O37A—P1A—O11A—W2A178.1 (7)O24B—W7B—O11B—W6B1.8 (4)
O15A—P1A—O11A—W2A59.9 (9)O26B—W7B—O11B—W2B51 (4)
O6A—P1A—O11A—W7A179.4 (7)O27B—W7B—O11B—W2B93.3 (5)
O37A—P1A—O11A—W7A61.2 (9)O28B—W7B—O11B—W2B179.4 (4)
O15A—P1A—O11A—W7A60.7 (9)O10B—W7B—O11B—W2B1.1 (4)
O6A—P1A—O11A—W6A62.3 (9)O24B—W7B—O11B—W2B90.4 (5)
O37A—P1A—O11A—W6A57.1 (9)O7B—W2B—O11B—P1B162 (3)
O15A—P1A—O11A—W6A179.1 (7)O9B—W2B—O11B—P1B133.4 (9)
O7A—W2A—O11A—P1A170 (4)O2B—W2B—O11B—P1B40.2 (8)
O9A—W2A—O11A—P1A133.9 (8)O10B—W2B—O11B—P1B134.4 (9)
O2A—W2A—O11A—P1A42.0 (8)O8B—W2B—O11B—P1B44.8 (8)
O8A—W2A—O11A—P1A43.6 (8)O7B—W2B—O11B—W6B62 (3)
O10A—W2A—O11A—P1A132.4 (9)O9B—W2B—O11B—W6B1.9 (4)
O7A—W2A—O11A—W7A35 (5)O2B—W2B—O11B—W6B95.2 (4)
O9A—W2A—O11A—W7A90.8 (5)O10B—W2B—O11B—W6B90.2 (5)
O2A—W2A—O11A—W7A177.3 (4)O8B—W2B—O11B—W6B179.9 (4)
O8A—W2A—O11A—W7A91.7 (4)O7B—W2B—O11B—W7B27 (3)
O10A—W2A—O11A—W7A2.9 (4)O9B—W2B—O11B—W7B91.0 (5)
O7A—W2A—O11A—W6A54 (4)O2B—W2B—O11B—W7B175.7 (4)
O9A—W2A—O11A—W6A2.2 (4)O10B—W2B—O11B—W7B1.1 (4)
O2A—W2A—O11A—W6A94.1 (4)O8B—W2B—O11B—W7B90.8 (4)
O8A—W2A—O11A—W6A179.7 (4)O29B—W8B—O13B—W3B173.4 (7)
O10A—W2A—O11A—W6A91.4 (5)O31B—W8B—O13B—W3B9.2 (16)
O26A—W7A—O11A—P1A174 (4)O27B—W8B—O13B—W3B84.2 (7)
O24A—W7A—O11A—P1A132.8 (9)O30B—W8B—O13B—W3B69.8 (8)
O10A—W7A—O11A—P1A133.0 (9)O15B—W8B—O13B—W3B1.4 (6)
O27A—W7A—O11A—P1A43.7 (8)O12B—W3B—O13B—W8B172.8 (8)
O28A—W7A—O11A—P1A43.5 (8)O8B—W3B—O13B—W8B83.7 (8)
O26A—W7A—O11A—W2A50 (4)O3B—W3B—O13B—W8B4.1 (17)
O24A—W7A—O11A—W2A91.3 (4)O14B—W3B—O13B—W8B70.1 (8)
O10A—W7A—O11A—W2A2.9 (4)O15B—W3B—O13B—W8B1.3 (6)
O27A—W7A—O11A—W2A92.3 (4)O32B—W9B—O14B—W3B169.7 (7)
O28A—W7A—O11A—W2A179.4 (4)O30B—W9B—O14B—W3B67.0 (8)
O26A—W7A—O11A—W6A39 (4)O18B—W9B—O14B—W3B88.6 (8)
O24A—W7A—O11A—W6A1.8 (4)O33B—W9B—O14B—W3B12.3 (17)
O10A—W7A—O11A—W6A92.4 (5)O15B—W9B—O14B—W3B4.8 (6)
O27A—W7A—O11A—W6A178.3 (4)O12B—W3B—O14B—W9B170.2 (7)
O28A—W7A—O11A—W6A91.2 (4)O8B—W3B—O14B—W9B15.4 (16)
O23A—W6A—O11A—P1A165 (3)O13B—W3B—O14B—W9B68.3 (8)
O24A—W6A—O11A—P1A132.1 (8)O3B—W3B—O14B—W9B87.6 (8)
O25A—W6A—O11A—P1A39.9 (8)O15B—W3B—O14B—W9B4.8 (6)
O9A—W6A—O11A—P1A133.9 (9)O11B—P1B—O15B—W9B179.7 (7)
O21A—W6A—O11A—P1A46.6 (8)O6B—P1B—O15B—W9B58.7 (10)
O23A—W6A—O11A—W2A29 (3)O37B—P1B—O15B—W9B60.0 (9)
O24A—W6A—O11A—W2A91.8 (5)O11B—P1B—O15B—W8B58.6 (10)
O25A—W6A—O11A—W2A176.1 (5)O6B—P1B—O15B—W8B179.8 (7)
O9A—W6A—O11A—W2A2.2 (4)O37B—P1B—O15B—W8B61.1 (10)
O21A—W6A—O11A—W2A89.6 (5)O11B—P1B—O15B—W3B59.7 (9)
O23A—W6A—O11A—W7A61 (3)O6B—P1B—O15B—W3B61.9 (9)
O24A—W6A—O11A—W7A1.8 (4)O37B—P1B—O15B—W3B179.5 (7)
O25A—W6A—O11A—W7A94.0 (4)O32B—W9B—O15B—P1B177 (3)
O9A—W6A—O11A—W7A92.1 (5)O14B—W9B—O15B—P1B132.5 (9)
O21A—W6A—O11A—W7A179.5 (5)O30B—W9B—O15B—P1B132.7 (9)
O12A—W3A—O13A—W8A170.4 (7)O18B—W9B—O15B—P1B42.0 (9)
O8A—W3A—O13A—W8A86.2 (7)O33B—W9B—O15B—P1B44.3 (8)
O3A—W3A—O13A—W8A6.9 (16)O32B—W9B—O15B—W8B47 (4)
O14A—W3A—O13A—W8A68.7 (7)O14B—W9B—O15B—W8B91.4 (5)
O15A—W3A—O13A—W8A2.7 (6)O30B—W9B—O15B—W8B3.5 (5)
O29A—W8A—O13A—W3A172.3 (7)O18B—W9B—O15B—W8B178.1 (5)
O31A—W8A—O13A—W3A13.4 (15)O33B—W9B—O15B—W8B91.8 (5)
O30A—W8A—O13A—W3A70.3 (7)O32B—W9B—O15B—W3B42 (4)
O27A—W8A—O13A—W3A86.2 (7)O14B—W9B—O15B—W3B3.1 (4)
O15A—W8A—O13A—W3A2.7 (6)O30B—W9B—O15B—W3B91.8 (5)
O32A—W9A—O14A—W3A170.8 (8)O18B—W9B—O15B—W3B93.6 (5)
O18A—W9A—O14A—W3A86.4 (8)O33B—W9B—O15B—W3B179.9 (5)
O33A—W9A—O14A—W3A8.3 (16)O29B—W8B—O15B—P1B179 (88)
O30A—W9A—O14A—W3A70.3 (7)O13B—W8B—O15B—P1B133.5 (9)
O15A—W9A—O14A—W3A2.2 (6)O31B—W8B—O15B—P1B43.3 (9)
O12A—W3A—O14A—W9A170.5 (8)O27B—W8B—O15B—P1B43.2 (9)
O8A—W3A—O14A—W9A12.6 (16)O30B—W8B—O15B—P1B133.6 (10)
O3A—W3A—O14A—W9A87.0 (8)O29B—W8B—O15B—W9B44 (4)
O13A—W3A—O14A—W9A71.0 (7)O13B—W8B—O15B—W9B89.6 (5)
O15A—W3A—O14A—W9A2.2 (6)O31B—W8B—O15B—W9B93.7 (4)
O6A—P1A—O15A—W3A60.1 (9)O27B—W8B—O15B—W9B179.8 (5)
O37A—P1A—O15A—W3A179.4 (7)O30B—W8B—O15B—W9B3.4 (5)
O11A—P1A—O15A—W3A58.7 (9)O29B—W8B—O15B—W3B45 (4)
O6A—P1A—O15A—W8A178.6 (7)O13B—W8B—O15B—W3B0.9 (4)
O37A—P1A—O15A—W8A59.2 (9)O31B—W8B—O15B—W3B177.6 (4)
O11A—P1A—O15A—W8A62.7 (9)O27B—W8B—O15B—W3B91.1 (5)
O6A—P1A—O15A—W9A60.8 (9)O30B—W8B—O15B—W3B92.1 (5)
O37A—P1A—O15A—W9A58.5 (10)O12B—W3B—O15B—P1B176 (4)
O11A—P1A—O15A—W9A179.6 (7)O8B—W3B—O15B—P1B41.6 (8)
O12A—W3A—O15A—P1A178 (3)O13B—W3B—O15B—P1B133.7 (9)
O8A—W3A—O15A—P1A41.9 (8)O3B—W3B—O15B—P1B45.1 (8)
O3A—W3A—O15A—P1A44.7 (8)O14B—W3B—O15B—P1B133.7 (9)
O13A—W3A—O15A—P1A133.7 (9)O12B—W3B—O15B—W9B39 (4)
O14A—W3A—O15A—P1A133.7 (9)O8B—W3B—O15B—W9B178.2 (4)
O12A—W3A—O15A—W8A43 (3)O13B—W3B—O15B—W9B89.6 (5)
O8A—W3A—O15A—W8A93.6 (4)O3B—W3B—O15B—W9B91.6 (4)
O3A—W3A—O15A—W8A179.8 (4)O14B—W3B—O15B—W9B3.0 (4)
O13A—W3A—O15A—W8A1.8 (4)O12B—W3B—O15B—W8B50 (4)
O14A—W3A—O15A—W8A90.8 (4)O8B—W3B—O15B—W8B93.0 (4)
O12A—W3A—O15A—W9A47 (3)O13B—W3B—O15B—W8B0.9 (4)
O8A—W3A—O15A—W9A176.9 (5)O3B—W3B—O15B—W8B179.7 (5)
O3A—W3A—O15A—W9A90.4 (4)O14B—W3B—O15B—W8B91.7 (5)
O13A—W3A—O15A—W9A91.2 (4)O16B—W4B—O17B—W5B169.4 (7)
O14A—W3A—O15A—W9A1.4 (4)O4B—W4B—O17B—W5B67.5 (7)
O29A—W8A—O15A—P1A170 (3)O19B—W4B—O17B—W5B89.7 (7)
O31A—W8A—O15A—P1A40.7 (8)O18B—W4B—O17B—W5B15.0 (17)
O30A—W8A—O15A—P1A132.1 (8)O6B—W4B—O17B—W5B5.6 (6)
O27A—W8A—O15A—P1A46.3 (8)O20B—W5B—O17B—W4B169.4 (7)
O13A—W8A—O15A—P1A134.9 (8)O5B—W5B—O17B—W4B67.4 (7)
O29A—W8A—O15A—W3A34 (3)O21B—W5B—O17B—W4B23.0 (16)
O31A—W8A—O15A—W3A177.3 (4)O22B—W5B—O17B—W4B90.1 (7)
O30A—W8A—O15A—W3A91.3 (5)O6B—W5B—O17B—W4B5.5 (6)
O27A—W8A—O15A—W3A90.3 (4)O32B—W9B—O18B—W4B132.3 (14)
O13A—W8A—O15A—W3A1.8 (4)O14B—W9B—O18B—W4B126.6 (14)
O29A—W8A—O15A—W9A56 (3)O30B—W9B—O18B—W4B41 (2)
O31A—W8A—O15A—W9A92.6 (4)O33B—W9B—O18B—W4B29.2 (14)
O30A—W8A—O15A—W9A1.2 (4)O15B—W9B—O18B—W4B53.3 (14)
O27A—W8A—O15A—W9A179.6 (5)O16B—W4B—O18B—W9B130.3 (14)
O13A—W8A—O15A—W9A91.9 (4)O4B—W4B—O18B—W9B127.8 (14)
O32A—W9A—O15A—P1A179 (54)O19B—W4B—O18B—W9B29.8 (14)
O14A—W9A—O15A—P1A135.0 (9)O17B—W4B—O18B—W9B45 (2)
O18A—W9A—O15A—P1A44.4 (8)O6B—W4B—O18B—W9B54.4 (14)
O33A—W9A—O15A—P1A42.5 (8)O34B—W10B—O19B—W4B126.8 (14)
O30A—W9A—O15A—P1A132.2 (9)O33B—W10B—O19B—W4B25.0 (14)
O32A—W9A—O15A—W3A43 (3)O36B—W10B—O19B—W4B59 (2)
O14A—W9A—O15A—W3A1.4 (4)O35B—W10B—O19B—W4B131.6 (15)
O18A—W9A—O15A—W3A92.1 (5)O37B—W10B—O19B—W4B59.0 (14)
O33A—W9A—O15A—W3A178.9 (4)O16B—W4B—O19B—W10B128.7 (14)
O30A—W9A—O15A—W3A91.3 (5)O4B—W4B—O19B—W10B50 (2)
O32A—W9A—O15A—W8A48 (3)O17B—W4B—O19B—W10B131.3 (15)
O14A—W9A—O15A—W8A91.6 (5)O18B—W4B—O19B—W10B26.2 (14)
O18A—W9A—O15A—W8A177.7 (5)O6B—W4B—O19B—W10B57.7 (14)
O33A—W9A—O15A—W8A90.9 (4)O20B—W5B—O21B—W6B130.0 (14)
O30A—W9A—O15A—W8A1.1 (4)O5B—W5B—O21B—W6B127.4 (14)
O16A—W4A—O17A—W5A172.5 (8)O17B—W5B—O21B—W6B38 (2)
O19A—W4A—O17A—W5A84.4 (8)O22B—W5B—O21B—W6B29.3 (14)
O4A—W4A—O17A—W5A70.4 (8)O6B—W5B—O21B—W6B54.4 (14)
O18A—W4A—O17A—W5A3.9 (18)O23B—W6B—O21B—W5B130.2 (14)
O6A—W4A—O17A—W5A2.0 (7)O24B—W6B—O21B—W5B53 (2)
O20A—W5A—O17A—W4A172.1 (8)O25B—W6B—O21B—W5B29.8 (14)
O5A—W5A—O17A—W4A71.1 (8)O9B—W6B—O21B—W5B127.2 (15)
O21A—W5A—O17A—W4A8.9 (18)O11B—W6B—O21B—W5B54.8 (14)
O22A—W5A—O17A—W4A84.8 (8)O38B—W11B—O22B—W5B131.2 (13)
O6A—W5A—O17A—W4A2.0 (7)O35B—W11B—O22B—W5B128.5 (13)
O32A—W9A—O18A—W4A128.7 (13)O25B—W11B—O22B—W5B28.1 (13)
O14A—W9A—O18A—W4A130.3 (14)O39B—W11B—O22B—W5B45 (2)
O33A—W9A—O18A—W4A26.2 (13)O37B—W11B—O22B—W5B56.0 (13)
O30A—W9A—O18A—W4A50 (2)O20B—W5B—O22B—W11B128.5 (13)
O15A—W9A—O18A—W4A58.5 (13)O5B—W5B—O22B—W11B57 (2)
O16A—W4A—O18A—W9A127.4 (14)O21B—W5B—O22B—W11B27.9 (13)
O19A—W4A—O18A—W9A25.6 (14)O17B—W5B—O22B—W11B130.5 (13)
O17A—W4A—O18A—W9A56 (2)O6B—W5B—O22B—W11B57.5 (13)
O4A—W4A—O18A—W9A130.5 (14)O23B—W6B—O24B—W7B172.1 (8)
O6A—W4A—O18A—W9A58.0 (13)O25B—W6B—O24B—W7B86.1 (8)
O16A—W4A—O19A—W10A129.0 (15)O21B—W6B—O24B—W7B5.0 (17)
O17A—W4A—O19A—W10A129.1 (15)O9B—W6B—O24B—W7B69.3 (8)
O4A—W4A—O19A—W10A44 (2)O11B—W6B—O24B—W7B2.9 (7)
O18A—W4A—O19A—W10A26.8 (15)O26B—W7B—O24B—W6B171.7 (8)
O6A—W4A—O19A—W10A56.1 (15)O27B—W7B—O24B—W6B11.3 (17)
O34A—W10A—O19A—W4A128.2 (15)O28B—W7B—O24B—W6B84.6 (8)
O35A—W10A—O19A—W4A129.0 (16)O10B—W7B—O24B—W6B69.6 (8)
O36A—W10A—O19A—W4A49 (2)O11B—W7B—O24B—W6B2.9 (7)
O33A—W10A—O19A—W4A26.8 (15)O23B—W6B—O25B—W11B131.5 (15)
O37A—W10A—O19A—W4A57.1 (15)O24B—W6B—O25B—W11B125.0 (15)
O20A—W5A—O21A—W6A125.0 (15)O21B—W6B—O25B—W11B30.5 (15)
O5A—W5A—O21A—W6A132.8 (15)O9B—W6B—O25B—W11B39 (2)
O22A—W5A—O21A—W6A21.7 (15)O11B—W6B—O25B—W11B52.8 (14)
O17A—W5A—O21A—W6A54 (2)O38B—W11B—O25B—W6B131.7 (14)
O6A—W5A—O21A—W6A60.6 (15)O22B—W11B—O25B—W6B30.7 (15)
O23A—W6A—O21A—W5A126.2 (15)O35B—W11B—O25B—W6B50 (2)
O24A—W6A—O21A—W5A59 (2)O39B—W11B—O25B—W6B126.5 (15)
O25A—W6A—O21A—W5A22.5 (15)O37B—W11B—O25B—W6B53.5 (14)
O9A—W6A—O21A—W5A133.3 (15)O26B—W7B—O27B—W8B127.2 (14)
O11A—W6A—O21A—W5A61.8 (15)O28B—W7B—O27B—W8B23.5 (14)
O20A—W5A—O22A—W11A126.6 (14)O10B—W7B—O27B—W8B129.7 (14)
O5A—W5A—O22A—W11A63 (2)O24B—W7B—O27B—W8B50 (2)
O21A—W5A—O22A—W11A23.6 (14)O11B—W7B—O27B—W8B57.8 (14)
O17A—W5A—O22A—W11A133.4 (14)O29B—W8B—O27B—W7B126.3 (14)
O6A—W5A—O22A—W11A60.4 (13)O13B—W8B—O27B—W7B132.3 (14)
O38A—W11A—O22A—W5A126.9 (14)O31B—W8B—O27B—W7B24.1 (14)
O25A—W11A—O22A—W5A24.9 (14)O30B—W8B—O27B—W7B52 (2)
O35A—W11A—O22A—W5A131.6 (14)O15B—W8B—O27B—W7B58.8 (14)
O39A—W11A—O22A—W5A51 (2)O26B—W7B—O28B—W12B124.5 (14)
O37A—W11A—O22A—W5A59.8 (14)O27B—W7B—O28B—W12B21.5 (14)
O26A—W7A—O24A—W6A171.8 (8)O10B—W7B—O28B—W12B61 (2)
O10A—W7A—O24A—W6A69.2 (8)O24B—W7B—O28B—W12B133.6 (14)
O27A—W7A—O24A—W6A11.5 (17)O11B—W7B—O28B—W12B62.1 (14)
O28A—W7A—O24A—W6A86.2 (8)O40B—W12B—O28B—W7B126.4 (14)
O11A—W7A—O24A—W6A3.0 (6)O31B—W12B—O28B—W7B21.7 (14)
O23A—W6A—O24A—W7A168.9 (7)O36B—W12B—O28B—W7B54 (2)
O25A—W6A—O24A—W7A86.4 (8)O39B—W12B—O28B—W7B134.0 (14)
O9A—W6A—O24A—W7A67.7 (8)O37B—W12B—O28B—W7B61.6 (14)
O21A—W6A—O24A—W7A5.8 (16)O32B—W9B—O30B—W8B168.4 (9)
O11A—W6A—O24A—W7A3.0 (6)O14B—W9B—O30B—W8B67.1 (9)
O23A—W6A—O25A—W11A130.6 (15)O18B—W9B—O30B—W8B18.6 (19)
O24A—W6A—O25A—W11A124.5 (15)O33B—W9B—O30B—W8B88.4 (9)
O9A—W6A—O25A—W11A40 (2)O15B—W9B—O30B—W8B5.5 (7)
O21A—W6A—O25A—W11A28.5 (15)O29B—W8B—O30B—W9B169.0 (9)
O11A—W6A—O25A—W11A53.2 (15)O13B—W8B—O30B—W9B67.8 (9)
O38A—W11A—O25A—W6A131.7 (15)O31B—W8B—O30B—W9B88.2 (9)
O22A—W11A—O25A—W6A29.1 (15)O27B—W8B—O30B—W9B12.6 (18)
O35A—W11A—O25A—W6A48 (2)O15B—W8B—O30B—W9B5.5 (7)
O39A—W11A—O25A—W6A127.0 (15)O40B—W12B—O31B—W8B127.5 (13)
O37A—W11A—O25A—W6A54.0 (15)O28B—W12B—O31B—W8B23.7 (13)
O26A—W7A—O27A—W8A125.5 (13)O36B—W12B—O31B—W8B132.8 (14)
O24A—W7A—O27A—W8A51 (2)O39B—W12B—O31B—W8B58 (2)
O10A—W7A—O27A—W8A132.2 (13)O37B—W12B—O31B—W8B60.1 (13)
O28A—W7A—O27A—W8A23.7 (13)O29B—W8B—O31B—W12B125.9 (13)
O11A—W7A—O27A—W8A59.3 (13)O13B—W8B—O31B—W12B51 (2)
O29A—W8A—O27A—W7A126.8 (13)O27B—W8B—O31B—W12B24.0 (13)
O31A—W8A—O27A—W7A23.9 (13)O30B—W8B—O31B—W12B130.3 (14)
O30A—W8A—O27A—W7A57 (2)O15B—W8B—O31B—W12B59.1 (13)
O13A—W8A—O27A—W7A132.9 (13)O34B—W10B—O33B—W9B126.9 (15)
O15A—W8A—O27A—W7A60.3 (13)O19B—W10B—O33B—W9B25.1 (15)
O40A—W12A—O28A—W7A127.4 (14)O36B—W10B—O33B—W9B130.3 (15)
O39A—W12A—O28A—W7A131.9 (14)O35B—W10B—O33B—W9B47 (2)
O31A—W12A—O28A—W7A23.7 (14)O37B—W10B—O33B—W9B57.6 (15)
O36A—W12A—O28A—W7A50 (2)O32B—W9B—O33B—W10B126.9 (15)
O37A—W12A—O28A—W7A59.4 (13)O14B—W9B—O33B—W10B51 (2)
O26A—W7A—O28A—W12A126.1 (14)O30B—W9B—O33B—W10B131.1 (15)
O24A—W7A—O28A—W12A132.3 (14)O18B—W9B—O33B—W10B26.0 (15)
O10A—W7A—O28A—W12A52 (2)O15B—W9B—O33B—W10B58.3 (15)
O27A—W7A—O28A—W12A24.2 (14)O38B—W11B—O35B—W10B171.7 (7)
O11A—W7A—O28A—W12A60.0 (13)O22B—W11B—O35B—W10B86.6 (8)
O29A—W8A—O30A—W9A171.0 (7)O25B—W11B—O35B—W10B6.9 (17)
O31A—W8A—O30A—W9A85.4 (7)O39B—W11B—O35B—W10B69.8 (8)
O27A—W8A—O30A—W9A5.7 (17)O37B—W11B—O35B—W10B3.1 (6)
O13A—W8A—O30A—W9A70.4 (7)O34B—W10B—O35B—W11B171.9 (7)
O15A—W8A—O30A—W9A1.8 (6)O33B—W10B—O35B—W11B13.8 (17)
O32A—W9A—O30A—W8A170.7 (7)O19B—W10B—O35B—W11B86.4 (8)
O14A—W9A—O30A—W8A70.0 (8)O36B—W10B—O35B—W11B70.0 (8)
O18A—W9A—O30A—W8A10.3 (17)O37B—W10B—O35B—W11B3.1 (6)
O33A—W9A—O30A—W8A86.5 (7)O34B—W10B—O36B—W12B173.5 (8)
O15A—W9A—O30A—W8A1.8 (6)O33B—W10B—O36B—W12B83.8 (8)
O29A—W8A—O31A—W12A126.3 (14)O19B—W10B—O36B—W12B0.6 (18)
O30A—W8A—O31A—W12A131.2 (14)O35B—W10B—O36B—W12B71.7 (8)
O27A—W8A—O31A—W12A25.0 (14)O37B—W10B—O36B—W12B0.7 (7)
O13A—W8A—O31A—W12A48 (2)O40B—W12B—O36B—W10B170.9 (8)
O15A—W8A—O31A—W12A58.1 (14)O31B—W12B—O36B—W10B84.2 (8)
O40A—W12A—O31A—W8A127.8 (14)O28B—W12B—O36B—W10B8.5 (17)
O28A—W12A—O31A—W8A24.6 (14)O39B—W12B—O36B—W10B72.1 (8)
O39A—W12A—O31A—W8A54 (2)O37B—W12B—O36B—W10B0.7 (7)
O36A—W12A—O31A—W8A131.4 (14)O15B—P1B—O37B—W10B57.2 (9)
O37A—W12A—O31A—W8A59.0 (14)O11B—P1B—O37B—W10B177.9 (7)
O32A—W9A—O33A—W10A130.1 (14)O6B—P1B—O37B—W10B61.5 (10)
O14A—W9A—O33A—W10A51 (2)O15B—P1B—O37B—W11B178.9 (7)
O18A—W9A—O33A—W10A27.9 (14)O11B—P1B—O37B—W11B60.3 (9)
O30A—W9A—O33A—W10A129.1 (14)O6B—P1B—O37B—W11B60.3 (9)
O15A—W9A—O33A—W10A56.6 (14)O15B—P1B—O37B—W12B61.9 (9)
O34A—W10A—O33A—W9A129.8 (14)O11B—P1B—O37B—W12B58.9 (9)
O35A—W10A—O33A—W9A44 (2)O6B—P1B—O37B—W12B179.5 (7)
O36A—W10A—O33A—W9A127.8 (14)O34B—W10B—O37B—P1B177 (4)
O19A—W10A—O33A—W9A27.1 (14)O33B—W10B—O37B—P1B40.8 (9)
O37A—W10A—O33A—W9A55.2 (14)O19B—W10B—O37B—P1B46.6 (8)
O34A—W10A—O35A—W11A170.2 (7)O36B—W10B—O37B—P1B133.5 (9)
O36A—W10A—O35A—W11A68.0 (8)O35B—W10B—O37B—P1B134.7 (9)
O19A—W10A—O35A—W11A86.4 (8)O34B—W10B—O37B—W11B40 (4)
O33A—W10A—O35A—W11A16.5 (16)O33B—W10B—O37B—W11B177.5 (5)
O37A—W10A—O35A—W11A4.3 (7)O19B—W10B—O37B—W11B90.1 (4)
O38A—W11A—O35A—W10A169.6 (8)O36B—W10B—O37B—W11B89.9 (5)
O22A—W11A—O35A—W10A87.1 (8)O35B—W10B—O37B—W11B2.0 (4)
O25A—W11A—O35A—W10A11.2 (17)O34B—W10B—O37B—W12B49 (4)
O39A—W11A—O35A—W10A68.5 (8)O33B—W10B—O37B—W12B93.1 (5)
O37A—W11A—O35A—W10A4.3 (7)O19B—W10B—O37B—W12B179.5 (5)
O34A—W10A—O36A—W12A170.7 (8)O36B—W10B—O37B—W12B0.5 (4)
O35A—W10A—O36A—W12A67.7 (8)O35B—W10B—O37B—W12B91.3 (5)
O19A—W10A—O36A—W12A12.4 (16)O38B—W11B—O37B—P1B170 (3)
O33A—W10A—O36A—W12A86.6 (8)O22B—W11B—O37B—P1B42.9 (8)
O37A—W10A—O36A—W12A3.6 (7)O35B—W11B—O37B—P1B134.7 (9)
O40A—W12A—O36A—W10A169.1 (8)O25B—W11B—O37B—P1B43.7 (8)
O28A—W12A—O36A—W10A13.9 (16)O39B—W11B—O37B—P1B132.6 (9)
O39A—W12A—O36A—W10A68.9 (8)O38B—W11B—O37B—W10B34 (3)
O31A—W12A—O36A—W10A86.8 (8)O22B—W11B—O37B—W10B93.8 (4)
O37A—W12A—O36A—W10A3.6 (7)O35B—W11B—O37B—W10B2.0 (4)
O6A—P1A—O37A—W11A60.7 (10)O25B—W11B—O37B—W10B179.6 (4)
O11A—P1A—O37A—W11A58.9 (10)O39B—W11B—O37B—W10B90.7 (5)
O15A—P1A—O37A—W11A179.9 (7)O38B—W11B—O37B—W12B56 (3)
O6A—P1A—O37A—W10A61.5 (9)O22B—W11B—O37B—W12B177.0 (5)
O11A—P1A—O37A—W10A178.9 (7)O35B—W11B—O37B—W12B91.2 (5)
O15A—P1A—O37A—W10A57.9 (10)O25B—W11B—O37B—W12B90.3 (4)
O6A—P1A—O37A—W12A179.3 (7)O39B—W11B—O37B—W12B1.5 (4)
O11A—P1A—O37A—W12A59.7 (9)O40B—W12B—O37B—P1B176 (3)
O15A—P1A—O37A—W12A61.3 (9)O31B—W12B—O37B—P1B45.2 (8)
O38A—W11A—O37A—P1A177 (3)O28B—W12B—O37B—P1B42.1 (8)
O22A—W11A—O37A—P1A43.7 (9)O36B—W12B—O37B—P1B134.7 (9)
O25A—W11A—O37A—P1A42.4 (9)O39B—W12B—O37B—P1B133.7 (9)
O35A—W11A—O37A—P1A134.8 (10)O40B—W12B—O37B—W10B48 (3)
O39A—W11A—O37A—P1A132.3 (10)O31B—W12B—O37B—W10B90.0 (5)
O38A—W11A—O37A—W10A39 (3)O28B—W12B—O37B—W10B177.3 (4)
O22A—W11A—O37A—W10A93.8 (5)O36B—W12B—O37B—W10B0.5 (4)
O25A—W11A—O37A—W10A179.9 (5)O39B—W12B—O37B—W10B91.1 (5)
O35A—W11A—O37A—W10A2.7 (4)O40B—W12B—O37B—W11B41 (3)
O39A—W11A—O37A—W10A90.2 (4)O31B—W12B—O37B—W11B179.6 (5)
O38A—W11A—O37A—W12A50 (3)O28B—W12B—O37B—W11B93.1 (4)
O22A—W11A—O37A—W12A177.3 (5)O36B—W12B—O37B—W11B90.1 (5)
O25A—W11A—O37A—W12A91.2 (5)O39B—W12B—O37B—W11B1.5 (4)
O35A—W11A—O37A—W12A91.6 (5)O38B—W11B—O39B—W12B170.1 (7)
O39A—W11A—O37A—W12A1.3 (4)O22B—W11B—O39B—W12B13.4 (17)
O34A—W10A—O37A—P1A180 (54)O35B—W11B—O39B—W12B70.2 (8)
O35A—W10A—O37A—P1A134.3 (9)O25B—W11B—O39B—W12B86.6 (7)
O36A—W10A—O37A—P1A131.7 (9)O37B—W11B—O39B—W12B2.3 (6)
O19A—W10A—O37A—P1A44.4 (9)O40B—W12B—O39B—W11B170.2 (8)
O33A—W10A—O37A—P1A40.4 (8)O31B—W12B—O39B—W11B4.9 (17)
O34A—W10A—O37A—W11A43 (4)O28B—W12B—O39B—W11B85.5 (7)
O35A—W10A—O37A—W11A2.7 (4)O36B—W12B—O39B—W11B70.6 (8)
O36A—W10A—O37A—W11A91.3 (5)O37B—W12B—O39B—W11B2.3 (6)
O19A—W10A—O37A—W11A92.6 (5)C15S—N11S—C12S—O11S178.7 (16)
O33A—W10A—O37A—W11A177.4 (4)C15S—N11S—C12S—N13S2.3 (18)
O34A—W10A—O37A—W12A46 (4)O11S—C12S—N13S—C14S178.2 (17)
O35A—W10A—O37A—W12A91.7 (5)N11S—C12S—N13S—C14S2.8 (19)
O36A—W10A—O37A—W12A2.3 (4)C12S—N13S—C14S—C15S2.3 (19)
O19A—W10A—O37A—W12A178.4 (5)C12S—N11S—C15S—O12S177.1 (16)
O33A—W10A—O37A—W12A93.6 (4)C12S—N11S—C15S—C14S0.9 (18)
O40A—W12A—O37A—P1A179 (2)N13S—C14S—C15S—O12S178.8 (17)
O28A—W12A—O37A—P1A42.1 (8)N13S—C14S—C15S—N11S0.8 (18)
O39A—W12A—O37A—P1A133.6 (9)C25S—N21S—C22S—O21S178.9 (15)
O31A—W12A—O37A—P1A44.1 (8)C25S—N21S—C22S—N23S3(2)
O36A—W12A—O37A—P1A133.5 (9)O21S—C22S—N23S—C24S179.3 (14)
O40A—W12A—O37A—W11A44 (3)N21S—C22S—N23S—C24S0.6 (18)
O28A—W12A—O37A—W11A92.8 (4)C22S—N23S—C24S—C25S1.2 (17)
O39A—W12A—O37A—W11A1.3 (4)C22S—N21S—C25S—O22S175.7 (16)
O31A—W12A—O37A—W11A179.1 (5)C22S—N21S—C25S—C24S3.1 (18)
O36A—W12A—O37A—W11A91.6 (5)N23S—C24S—C25S—O22S176.2 (15)
O40A—W12A—O37A—W10A46 (3)N23S—C24S—C25S—N21S2.6 (17)
O28A—W12A—O37A—W10A177.9 (4)C35S—N31S—C32S—O31S177.4 (15)
O39A—W12A—O37A—W10A90.6 (4)C35S—N31S—C32S—N33S2.8 (18)
O31A—W12A—O37A—W10A91.7 (4)O31S—C32S—N33S—C34S178.4 (17)
O36A—W12A—O37A—W10A2.3 (4)N31S—C32S—N33S—C34S1.8 (19)
O40A—W12A—O39A—W11A171.0 (7)C32S—N33S—C34S—C35S0(2)
O28A—W12A—O39A—W11A84.9 (7)C32S—N31S—C35S—O32S177.4 (15)
O31A—W12A—O39A—W11A7.4 (16)C32S—N31S—C35S—C34S2.6 (19)
O36A—W12A—O39A—W11A70.1 (7)N33S—C34S—C35S—O32S178.7 (15)
O37A—W12A—O39A—W11A2.1 (6)N33S—C34S—C35S—N31S1.4 (19)
O38A—W11A—O39A—W12A170.9 (7)C45S—N41S—C42S—O41S178.4 (18)
O22A—W11A—O39A—W12A11.5 (16)C45S—N41S—C42S—N43S1(2)
O25A—W11A—O39A—W12A86.5 (7)O41S—C42S—N43S—C44S179.6 (18)
O35A—W11A—O39A—W12A69.7 (7)N41S—C42S—N43S—C44S0(2)
O37A—W11A—O39A—W12A2.1 (6)C42S—N43S—C44S—C45S1(2)
O1B—W1B—O2B—W2B129.0 (16)C42S—N41S—C45S—O42S179.0 (19)
O3B—W1B—O2B—W2B25.3 (16)C42S—N41S—C45S—C44S2(2)
O4B—W1B—O2B—W2B55 (2)N43S—C44S—C45S—O42S179.1 (19)
O5B—W1B—O2B—W2B129.2 (17)N43S—C44S—C45S—N41S2(2)
O6B—W1B—O2B—W2B57.8 (16)C55S—N51S—C52S—O51S172.7 (17)
O7B—W2B—O2B—W1B126.0 (16)C55S—N51S—C52S—N53S3.4 (19)
O9B—W2B—O2B—W1B129.4 (17)O51S—C52S—N53S—C54S171.4 (17)
O10B—W2B—O2B—W1B46 (2)N51S—C52S—N53S—C54S5(2)
O8B—W2B—O2B—W1B25.3 (16)O51S—C52S—N53S—C71S0(3)
O11B—W2B—O2B—W1B57.4 (16)N51S—C52S—N53S—C71S176.4 (15)
O1B—W1B—O3B—W3B126.0 (15)C52S—N53S—C54S—C55S4.1 (19)
O2B—W1B—O3B—W3B22.1 (16)C71S—N53S—C54S—C55S175.4 (15)
O4B—W1B—O3B—W3B132.2 (16)C52S—N51S—C55S—O52S177.9 (17)
O5B—W1B—O3B—W3B53 (2)C52S—N51S—C55S—C54S0.8 (19)
O6B—W1B—O3B—W3B60.5 (15)N53S—C54S—C55S—O52S179.4 (17)
O12B—W3B—O3B—W1B124.5 (16)N53S—C54S—C55S—N51S1.9 (18)
O8B—W3B—O3B—W1B22.0 (16)C65S—N61S—C62S—O61S177 (2)
O13B—W3B—O3B—W1B59 (2)C65S—N61S—C62S—N63S3(3)
O14B—W3B—O3B—W1B132.9 (16)O61S—C62S—N63S—C64S175 (2)
O15B—W3B—O3B—W1B61.2 (15)N61S—C62S—N63S—C64S4(2)
O16B—W4B—O4B—W1B171.7 (8)O61S—C62S—N63S—C71S11 (4)
O19B—W4B—O4B—W1B9.6 (18)N61S—C62S—N63S—C71S168.5 (16)
O17B—W4B—O4B—W1B71.5 (8)C62S—N63S—C64S—C65S4(2)
O18B—W4B—O4B—W1B85.4 (8)C71S—N63S—C64S—C65S167.9 (16)
O6B—W4B—O4B—W1B1.7 (7)C62S—N61S—C65S—O62S178 (2)
O1B—W1B—O4B—W4B171.3 (8)C62S—N61S—C65S—C64S0(2)
O3B—W1B—O4B—W4B83.9 (8)N63S—C64S—C65S—O62S179.9 (18)
O2B—W1B—O4B—W4B5.0 (17)N63S—C64S—C65S—N61S2(2)
O5B—W1B—O4B—W4B70.0 (8)C62S—N63S—C71S—N53S116 (2)
O6B—W1B—O4B—W4B1.7 (7)C64S—N63S—C71S—N53S81 (2)
O20B—W5B—O5B—W1B172.7 (7)C52S—N53S—C71S—N63S79 (2)
O21B—W5B—O5B—W1B85.3 (8)C54S—N53S—C71S—N63S91 (2)
Acknowledgements top

Support of this investigation by Ferdowsi University of Mashhad is gratefully acknowledged.

references
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