# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' PFLJ175 in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 160.39 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.7529 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 3.8917 _cell_length_b 17.1185 _cell_length_c 9.4048 _cell_angle_alpha 90.000 _cell_angle_beta 91.359 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4006.06 3982.63 66.27 o 4 0 0 1133.34 1200.84 34.06 o 1 1 0 3436.91 3492.17 42.21 o 2 1 0 78.15 83.73 3.69 o 3 1 0 1245.79 1244.05 18.95 o 4 1 0 552.46 574.23 17.16 o 5 1 0 590.65 529.23 47.79 o 0 2 0 3190.30 3455.19 74.46 o 1 2 0 7756.78 7495.95 91.48 o 2 2 0 1742.44 1696.10 22.28 o 3 2 0 271.95 270.65 8.35 o 4 2 0 55.80 40.81 9.70 o 5 2 0 460.11 545.81 59.81 o 1 3 0 1533.15 1624.04 20.40 o 2 3 0 1142.27 1177.57 16.81 o 3 3 0 3.86 3.67 4.19 o 4 3 0 2486.71 2790.36 51.63 o 5 3 0 44.95 37.33 18.52 o 0 4 0 41.17 23.61 3.81 o 1 4 0 8184.59 8013.90 102.15 o 2 4 0 402.03 399.49 9.58 o 3 4 0 1633.30 1662.63 24.51 o 4 4 0 0.34 1.12 9.10 o 5 4 0 653.69 673.30 45.74 o 1 5 0 43.02 43.75 2.85 o 2 5 0 904.40 905.42 15.36 o 3 5 0 336.96 304.35 10.48 o 4 5 0 1340.88 1393.32 26.90 o 5 5 0 115.59 105.53 35.35 o 0 6 0 24609.23 27988.04 618.09 o 1 6 0 1702.36 1731.72 23.84 o 2 6 0 3806.95 3752.70 44.17 o 3 6 0 657.81 682.01 17.51 o 4 6 0 909.60 980.58 22.56 o 1 7 0 133.78 125.15 4.58 o 2 7 0 496.27 473.54 9.98 o 3 7 0 1494.66 1441.07 26.00 o 4 7 0 1.37 1.66 9.02 o 0 8 0 11297.52 12257.23 321.39 o 1 8 0 1162.94 1153.03 17.44 o 2 8 0 2743.51 2690.37 38.46 o 3 8 0 96.21 93.47 8.29 o 4 8 0 278.63 348.25 15.85 o 1 9 0 120.80 116.63 7.59 o 2 9 0 9.41 2.01 4.86 o 3 9 0 151.69 158.66 9.85 o 4 9 0 1249.65 1368.57 30.13 o 0 10 0 2161.88 2557.65 62.25 o 1 10 0 6075.67 6025.01 87.43 o 2 10 0 1879.92 1728.28 30.04 o 3 10 0 417.71 421.77 17.16 o 4 10 0 122.88 139.76 13.51 o 1 11 0 305.71 294.49 10.39 o 2 11 0 317.25 306.93 14.00 o 3 11 0 20.59 24.40 8.09 o 4 11 0 797.59 860.91 30.08 o 0 12 0 4442.45 4945.93 116.21 o 1 12 0 3790.02 3876.51 66.38 o 2 12 0 170.57 175.91 9.81 o 3 12 0 1315.27 1266.72 41.70 o 4 12 0 128.26 132.92 13.11 o 1 13 0 321.59 332.66 14.88 o 2 13 0 766.87 746.74 22.82 o 3 13 0 841.35 851.36 20.35 o 4 13 0 84.79 97.95 17.23 o 0 14 0 5226.45 5688.71 133.81 o 1 14 0 111.81 101.46 10.46 o 2 14 0 1135.07 1050.76 24.79 o 3 14 0 652.43 679.35 24.36 o 1 15 0 592.55 580.45 20.76 o 2 15 0 141.89 128.38 11.78 o 3 15 0 355.60 355.54 16.92 o 0 16 0 392.51 396.30 31.77 o 1 16 0 629.24 629.37 21.87 o 2 16 0 3142.29 2994.87 59.43 o 3 16 0 69.55 60.29 11.82 o 1 17 0 941.39 968.14 28.32 o 2 17 0 314.71 282.63 18.01 o 3 17 0 92.60 86.36 15.28 o 0 18 0 6.28 10.41 20.46 o 1 18 0 1867.69 1781.82 57.35 o 2 18 0 135.14 134.21 17.34 o 1 19 0 11.49 19.90 13.33 o 2 19 0 148.88 148.42 16.57 o 0 20 0 1252.21 1179.72 56.86 o 1 20 0 968.01 935.68 50.93 o 2 20 0 457.93 401.49 56.58 o 1 21 0 13.68 24.79 17.36 o 0 22 0 669.15 695.27 72.01 o -5 0 1 57.20 -36.00 41.72 o -3 0 1 2999.31 2955.57 52.54 o -1 0 1 3469.79 3694.89 103.59 o 1 0 1 8808.29 8657.31 151.79 o 3 0 1 4252.26 4334.65 89.22 o 5 0 1 71.46 64.29 27.15 o -5 1 1 97.19 59.59 28.77 o -4 1 1 218.57 245.71 13.83 o -3 1 1 72.23 74.18 5.66 o -2 1 1 622.19 584.96 9.21 o -1 1 1 3425.97 3573.41 40.22 o 0 1 1 16.97 30.64 1.46 o 1 1 1 3871.62 3865.24 46.70 o 2 1 1 2508.41 2262.42 30.20 o 3 1 1 455.15 451.86 11.36 o 4 1 1 214.68 215.93 12.15 o 5 1 1 65.38 51.15 27.43 o -5 2 1 46.13 3.57 25.67 o -4 2 1 347.89 360.26 16.19 o -3 2 1 1232.93 1257.02 18.31 o -2 2 1 10419.37 10215.94 119.36 o -1 2 1 25103.09 24294.30 282.86 o 0 2 1 100.40 100.70 2.68 o 1 2 1 7403.59 8682.11 327.61 o 2 2 1 3890.50 3730.04 46.42 o 3 2 1 3133.02 3133.01 44.75 o 4 2 1 961.37 1020.95 22.46 o 5 2 1 14.73 22.86 26.29 o -5 3 1 610.35 810.72 48.94 o -4 3 1 203.75 222.20 13.61 o -3 3 1 207.62 231.65 7.94 o -2 3 1 494.32 481.58 8.97 o -1 3 1 10086.42 9479.85 111.56 o 0 3 1 148.43 157.89 3.88 o 1 3 1 601.96 544.21 14.63 o 2 3 1 122.57 123.11 4.87 o 3 3 1 2156.44 2101.95 29.96 o 4 3 1 40.82 21.84 8.39 o -5 4 1 13.19 -30.07 30.07 o -4 4 1 548.54 557.23 19.19 o -3 4 1 603.43 618.44 13.40 o -2 4 1 9993.77 9521.60 120.84 o -1 4 1 2323.51 2217.44 27.87 o 0 4 1 7687.09 8411.34 105.75 o 1 4 1 11.40 24.68 8.24 o 2 4 1 3651.07 3328.65 41.86 o 3 4 1 887.32 846.27 15.25 o 4 4 1 1473.06 1572.54 43.95 o 5 4 1 25.95 -15.43 37.72 o -5 5 1 321.12 321.76 70.87 o -4 5 1 75.15 71.28 10.80 o -3 5 1 1138.84 1184.44 20.46 o -2 5 1 4.03 8.16 3.59 o -1 5 1 1052.35 1040.56 14.44 o 0 5 1 790.95 807.36 12.31 o 1 5 1 477.95 486.17 9.35 o 2 5 1 3331.89 3067.02 37.97 o 3 5 1 1508.92 1508.18 26.86 o 4 5 1 17.01 21.68 9.14 o -4 6 1 679.98 700.57 21.55 o -3 6 1 988.90 960.62 17.92 o -2 6 1 1087.18 1025.76 16.47 o -1 6 1 5951.79 5517.91 66.63 o 0 6 1 2557.02 2700.77 36.70 o 1 6 1 1724.98 2122.17 43.97 o 2 6 1 1359.58 1240.54 17.47 o 3 6 1 3385.85 3472.73 49.95 o 4 6 1 120.38 132.20 10.75 o -4 7 1 246.15 265.78 16.41 o -3 7 1 421.60 399.21 11.45 o -2 7 1 667.67 602.68 12.26 o -1 7 1 8.38 13.12 2.86 o 0 7 1 38.46 36.10 2.86 o 1 7 1 9.42 12.43 2.91 o 2 7 1 1833.33 1692.34 22.83 o 3 7 1 55.59 52.04 7.26 o 4 7 1 147.09 160.15 12.08 o -4 8 1 1.56 5.54 11.25 o -3 8 1 2714.34 2625.95 41.83 o -2 8 1 1256.35 1116.53 18.86 o -1 8 1 10971.31 11191.08 148.35 o 0 8 1 320.87 388.74 8.08 o 1 8 1 7916.95 8632.24 109.75 o 2 8 1 250.57 229.72 8.48 o 3 8 1 3738.20 3585.85 55.38 o 4 8 1 2.09 -3.29 9.39 o -4 9 1 566.42 639.17 20.83 o -3 9 1 11.08 9.23 6.57 o -2 9 1 247.64 264.50 10.15 o -1 9 1 1319.07 1221.95 22.47 o 0 9 1 48.29 56.35 3.51 o 1 9 1 176.09 250.14 12.01 o 2 9 1 983.33 921.51 16.19 o 3 9 1 387.92 347.23 16.93 o 4 9 1 587.94 645.44 20.10 o -4 10 1 246.74 253.54 15.23 o -3 10 1 56.68 45.82 7.74 o -2 10 1 6060.27 5807.23 87.13 o -1 10 1 311.69 475.20 12.62 o 0 10 1 2912.71 3133.72 48.50 o 1 10 1 2217.46 2090.35 32.91 o 2 10 1 2757.40 2696.81 40.35 o 3 10 1 5.76 -0.71 7.02 o 4 10 1 1044.00 1098.83 33.17 o -4 11 1 59.24 49.91 12.45 o -3 11 1 387.91 387.69 16.90 o -2 11 1 22.99 41.93 6.73 o -1 11 1 1282.38 1308.27 24.79 o 0 11 1 503.42 547.51 15.66 o 1 11 1 474.83 574.96 14.16 o 2 11 1 1582.94 1497.67 25.20 o 3 11 1 1043.03 1011.06 23.05 o 4 11 1 151.78 159.03 16.89 o -4 12 1 442.07 451.93 20.64 o -3 12 1 389.38 408.97 15.07 o -2 12 1 2535.16 2437.35 41.22 o -1 12 1 518.85 456.90 14.87 o 0 12 1 4549.88 4737.13 90.18 o 1 12 1 122.95 122.26 9.26 o 2 12 1 2382.10 2314.70 40.47 o 3 12 1 1279.39 1243.61 33.84 o 4 12 1 106.37 108.43 15.23 o -4 13 1 21.51 5.23 16.12 o -3 13 1 756.42 779.26 20.16 o -2 13 1 659.76 589.92 17.75 o -1 13 1 80.58 65.80 8.56 o 0 13 1 1.76 -3.39 6.45 o 1 13 1 1.35 11.60 7.25 o 2 13 1 663.58 596.10 20.01 o 3 13 1 109.37 104.67 10.31 o 4 13 1 65.72 67.42 23.93 o -4 14 1 91.20 133.44 46.58 o -3 14 1 1487.37 1549.11 32.75 o -2 14 1 63.60 55.50 9.59 o -1 14 1 2769.29 2996.24 68.95 o 0 14 1 2610.79 2716.21 55.63 o 1 14 1 4371.34 4314.07 81.53 o 2 14 1 224.82 209.45 14.37 o 3 14 1 1321.71 1329.98 32.41 o -3 15 1 156.47 130.74 14.11 o -2 15 1 175.42 181.27 12.91 o -1 15 1 640.73 603.64 21.16 o 0 15 1 71.12 85.77 14.14 o 1 15 1 223.14 252.54 14.50 o 2 15 1 478.03 419.29 25.33 o 3 15 1 3.36 -1.50 9.36 o -3 16 1 251.39 227.71 28.69 o -2 16 1 1253.55 1164.87 28.25 o -1 16 1 2306.78 2280.70 49.60 o 0 16 1 419.72 430.62 18.16 o 1 16 1 2123.02 2192.85 43.93 o 2 16 1 441.80 328.08 19.37 o 3 16 1 366.10 360.69 17.68 o -3 17 1 107.28 93.83 15.52 o -2 17 1 232.45 197.03 14.54 o -1 17 1 76.55 69.45 12.40 o 0 17 1 6.74 16.50 10.53 o 1 17 1 7.97 27.53 11.67 o 2 17 1 2.94 0.22 11.61 o 3 17 1 251.22 272.81 39.59 o -2 18 1 833.50 795.27 31.56 o -1 18 1 27.78 46.83 12.78 o 0 18 1 3085.87 3244.28 83.00 o 1 18 1 398.08 402.62 21.02 o 2 18 1 761.84 691.40 42.52 o -2 19 1 62.59 62.89 15.91 o -1 19 1 23.28 28.68 15.21 o 0 19 1 92.67 69.89 17.24 o 1 19 1 40.81 36.39 13.93 o 2 19 1 66.42 57.88 15.82 o -2 20 1 204.82 153.73 35.02 o -1 20 1 442.14 471.28 23.71 o 0 20 1 2071.80 2092.10 51.81 o 1 20 1 527.44 547.92 25.47 o -1 21 1 59.14 60.39 21.53 o 0 21 1 109.83 130.34 18.69 o 1 21 1 20.17 -6.48 19.72 o 0 22 1 196.47 184.56 57.29 o -4 0 2 1539.82 1759.10 103.73 o -2 0 2 4329.24 4389.04 68.98 o 0 0 2 25725.60 25999.31 457.36 o 2 0 2 14596.91 13924.41 239.44 o 4 0 2 58.38 49.36 12.07 o -5 1 2 337.98 324.04 70.58 o -4 1 2 219.60 231.08 15.53 o -3 1 2 2117.34 2200.57 33.28 o -2 1 2 316.64 261.29 5.87 o -1 1 2 930.59 1037.35 13.06 o 0 1 2 597.80 665.71 14.86 o 1 1 2 1699.20 1658.62 21.68 o 2 1 2 1.86 3.89 2.76 o 3 1 2 123.13 137.83 7.35 o 4 1 2 90.38 86.22 9.19 o -5 2 2 302.50 324.04 68.58 o -4 2 2 309.04 345.13 16.33 o -3 2 2 1694.65 1716.64 28.76 o -2 2 2 31.67 30.45 3.21 o -1 2 2 6456.06 7195.93 82.47 o 0 2 2 7080.84 7123.34 88.40 o 1 2 2 11416.97 10689.48 133.18 o 2 2 2 2575.41 2484.58 31.84 o 3 2 2 694.33 684.68 14.04 o 4 2 2 156.07 162.09 11.61 o 5 2 2 32.93 62.58 27.72 o -5 3 2 50.86 73.44 41.72 o -4 3 2 832.26 917.33 24.61 o -3 3 2 177.93 188.35 7.91 o -2 3 2 2222.22 2147.03 27.29 o -1 3 2 16.98 20.66 2.45 o 0 3 2 2364.41 2195.83 28.70 o 1 3 2 12.98 5.01 1.92 o 2 3 2 27.95 23.64 3.49 o 3 3 2 166.90 157.73 7.48 o 4 3 2 1500.52 1572.02 30.83 o -4 4 2 90.77 84.96 10.76 o -3 4 2 4759.40 4895.20 63.39 o -2 4 2 1002.81 1036.50 15.02 o -1 4 2 3295.43 4403.81 87.70 o 0 4 2 79.87 70.60 3.25 o 1 4 2 16014.96 15082.95 186.42 o 2 4 2 66.97 71.70 3.84 o 3 4 2 744.27 716.50 14.30 o 4 4 2 43.74 43.79 8.92 o -4 5 2 312.40 323.11 15.06 o -3 5 2 2188.94 2184.86 32.89 o -2 5 2 3792.87 3712.25 51.01 o -1 5 2 151.74 171.81 5.49 o 0 5 2 63.37 60.29 3.27 o 1 5 2 204.30 212.86 5.37 o 2 5 2 399.06 441.85 16.49 o 3 5 2 44.71 34.38 5.38 o 4 5 2 832.81 847.58 20.98 o -4 6 2 1813.51 1932.75 39.92 o -3 6 2 1224.33 1231.71 21.37 o -2 6 2 2279.74 2234.64 30.86 o -1 6 2 2871.77 2805.18 37.43 o 0 6 2 6739.28 7077.17 96.28 o 1 6 2 1889.16 1875.38 32.59 o 2 6 2 6919.37 6551.86 80.71 o 3 6 2 1200.72 1224.47 24.83 o 4 6 2 358.67 368.85 15.89 o -4 7 2 62.88 54.08 12.87 o -3 7 2 1458.63 1467.56 24.49 o -2 7 2 61.12 48.87 4.84 o 0 7 2 649.38 685.42 11.31 o 1 7 2 3066.54 3011.16 37.55 o 2 7 2 604.62 628.59 14.12 o 3 7 2 672.40 693.41 15.53 o 4 7 2 43.49 43.66 9.99 o -4 8 2 348.17 365.48 20.75 o -3 8 2 647.51 650.48 15.80 o -2 8 2 1408.01 1340.96 21.43 o 0 8 2 6927.89 7182.42 92.12 o 1 8 2 3873.54 3562.11 44.27 o 2 8 2 4059.04 3933.60 46.83 o 3 8 2 50.51 44.73 7.04 o 4 8 2 329.22 332.56 15.23 o -4 9 2 127.84 132.09 15.55 o -3 9 2 679.49 684.65 18.17 o -2 9 2 752.88 729.83 15.69 o -1 9 2 4.02 15.78 4.59 o 0 9 2 1404.10 1506.19 21.91 o 1 9 2 38.07 44.19 3.60 o 2 9 2 239.70 263.18 8.27 o 3 9 2 412.22 372.54 15.55 o 4 9 2 349.72 389.57 16.34 o -4 10 2 16.36 20.35 13.84 o -3 10 2 1317.89 1266.35 26.71 o -2 10 2 1598.92 1517.85 27.70 o -1 10 2 3502.44 4229.07 69.00 o 0 10 2 2889.90 3196.61 45.18 o 1 10 2 9098.01 8607.82 114.23 o 2 10 2 600.05 551.43 13.13 o 3 10 2 100.82 104.31 8.85 o 4 10 2 187.06 216.03 23.32 o -4 11 2 721.40 775.54 29.04 o -3 11 2 424.68 412.41 16.39 o -2 11 2 233.15 263.28 11.34 o -1 11 2 285.89 271.76 10.76 o 0 11 2 0.99 5.61 4.02 o 1 11 2 40.79 43.52 4.61 o 2 11 2 75.15 74.67 6.97 o 3 11 2 146.50 163.92 14.67 o 4 11 2 616.57 683.83 21.41 o -4 12 2 571.84 656.65 32.76 o -3 12 2 909.11 895.48 21.59 o -2 12 2 5.94 17.36 9.18 o -1 12 2 6589.57 6362.85 109.46 o 0 12 2 1754.63 1856.10 35.56 o 1 12 2 3364.29 3826.49 62.16 o 2 12 2 1068.54 993.39 21.65 o 3 12 2 2074.80 1996.48 42.44 o 4 12 2 1.79 -1.05 15.03 o -4 13 2 172.05 194.55 30.01 o -3 13 2 629.08 584.26 18.37 o -2 13 2 120.96 119.85 10.23 o -1 13 2 30.55 71.35 10.48 o 0 13 2 429.81 430.36 15.99 o 1 13 2 965.29 940.58 22.27 o 2 13 2 1250.81 1159.43 26.25 o 3 13 2 174.50 189.54 11.65 o 4 13 2 92.51 67.51 32.49 o -4 14 2 442.90 503.79 60.87 o -3 14 2 98.16 92.23 11.79 o -2 14 2 1516.74 1458.19 31.22 o -1 14 2 636.33 545.86 20.06 o 0 14 2 1608.21 1679.13 37.02 o 1 14 2 28.00 48.31 8.03 o 2 14 2 2324.08 2231.09 43.85 o 3 14 2 184.39 182.38 11.90 o -3 15 2 645.16 609.04 24.65 o -2 15 2 20.95 16.99 9.79 o -1 15 2 557.25 486.17 20.86 o 0 15 2 87.04 87.18 11.08 o 1 15 2 187.29 193.67 12.12 o 2 15 2 108.35 110.64 10.20 o 3 15 2 863.64 896.02 27.52 o -3 16 2 401.89 395.21 31.01 o -2 16 2 1819.14 1702.83 37.08 o -1 16 2 239.29 284.00 17.01 o 0 16 2 2189.35 2324.27 54.04 o 1 16 2 848.04 868.88 23.71 o 2 16 2 739.38 687.94 23.48 o 3 16 2 18.98 10.73 9.50 o -3 17 2 4.35 -0.72 16.22 o -2 17 2 232.89 231.64 15.62 o -1 17 2 173.49 178.84 22.70 o 0 17 2 90.47 114.70 13.04 o 1 17 2 18.24 16.57 11.24 o 2 17 2 30.79 13.21 9.17 o 3 17 2 776.79 805.33 65.30 o -3 18 2 770.47 677.85 79.16 o -2 18 2 562.69 525.25 21.61 o -1 18 2 2518.66 2426.59 81.41 o 0 18 2 21.65 23.62 11.52 o 1 18 2 2617.29 2597.55 65.62 o 2 18 2 21.25 11.21 9.49 o -2 19 2 38.64 18.19 13.14 o -1 19 2 190.99 198.06 20.37 o 0 19 2 174.45 203.15 16.98 o 1 19 2 117.00 122.31 17.80 o 2 19 2 211.40 181.40 46.19 o -2 20 2 286.65 176.01 64.59 o -1 20 2 1950.95 1744.22 92.62 o 0 20 2 496.18 525.88 25.97 o 1 20 2 264.88 340.72 24.77 o -1 21 2 57.12 79.30 32.51 o 0 21 2 73.81 101.43 19.42 o 1 21 2 32.18 71.15 34.86 o 0 22 2 1171.47 983.96 70.59 o -3 0 3 377.70 372.49 16.89 o -1 0 3 14725.12 13448.97 265.39 o 1 0 3 3505.68 4042.07 167.55 o 3 0 3 2592.59 2558.70 59.97 o -4 1 3 1308.17 1371.62 36.54 o -3 1 3 19.34 21.02 5.56 o -2 1 3 61.84 90.51 4.15 o -1 1 3 105.17 133.10 9.01 o 0 1 3 587.54 542.25 8.94 o 1 1 3 309.40 332.77 7.89 o 2 1 3 1762.39 1638.79 25.51 o 3 1 3 1380.63 1340.45 25.17 o 4 1 3 1112.17 1133.98 24.57 o -4 2 3 224.44 236.42 17.25 o -3 2 3 736.23 731.91 16.20 o -2 2 3 3813.68 3640.92 42.55 o -1 2 3 6665.86 6926.02 101.21 o 0 2 3 11427.49 11886.40 167.50 o 1 2 3 5453.27 5556.24 72.67 o 2 2 3 243.87 257.28 11.07 o 3 2 3 847.79 807.84 16.69 o 4 2 3 1577.89 1607.71 31.12 o -4 3 3 129.10 148.61 13.92 o 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494.18 482.83 15.85 o -2 7 3 7.72 14.03 3.98 o -1 7 3 557.41 660.59 12.39 o 0 7 3 1981.64 2154.17 30.79 o 1 7 3 616.80 633.89 12.61 o 2 7 3 1652.01 1541.02 24.07 o 3 7 3 17.90 13.66 5.73 o 4 7 3 1387.61 1462.76 34.95 o -4 8 3 173.82 166.66 16.86 o -3 8 3 1526.69 1553.37 30.87 o -2 8 3 380.55 361.00 9.91 o -1 8 3 7877.12 7776.03 111.80 o 0 8 3 2312.29 2548.72 36.08 o 1 8 3 4784.39 5147.80 68.96 o 2 8 3 149.21 147.53 6.26 o 3 8 3 1918.90 1842.15 29.78 o 4 8 3 50.21 50.57 10.10 o -4 9 3 109.95 113.19 18.89 o -3 9 3 7.43 3.12 8.10 o -2 9 3 1169.03 1144.83 22.08 o -1 9 3 3.50 15.34 4.96 o 0 9 3 667.93 795.40 16.14 o 1 9 3 153.13 164.40 6.90 o 2 9 3 593.10 553.58 11.81 o 3 9 3 736.32 685.81 25.31 o 4 9 3 309.46 332.89 17.75 o -4 10 3 204.76 220.04 20.20 o -3 10 3 679.93 651.26 26.50 o -2 10 3 4019.22 3842.50 59.63 o 0 10 3 8407.38 8906.52 128.22 o 1 10 3 2127.73 2072.05 30.28 o 2 10 3 2807.40 2761.25 44.22 o 3 10 3 278.01 273.08 15.91 o 4 10 3 892.74 969.75 24.87 o -4 11 3 0.36 11.30 15.13 o 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