Acta Cryst. (2010). E66, m1042-m1043  [ doi:10.1107/S160053681002893X ]

Tetraethylammonium tricarbonylchlorido(quinoxaline-2-carboxylato-²N¹,O)rhenate(I)

J. Suthiram, J. R. Zeevaart, H. G. Visser and A. Roodt

Online 31 July 2010

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.006 Å
• R factor = 0.027
• wR factor = 0.065
• Data-to-parameter ratio = 19.8

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Re1    --  C2      ..       5.81 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Re1    --  C3      ..       7.47 su   
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          1      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         13      
PLAT971_ALERT_2_C Large Calcd. Non-Metal Positive Residual Density       1.53 eA-3 
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         19      

Alert level G
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......         12      
PLAT153_ALERT_1_G The su's on the Cell Axes   are Equal (x 100000)        500 Ang. 
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal  (x 10000)        500 Deg. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   3 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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