Acta Cryst. (2010). E66, m1117-m1118  [ doi:10.1107/S1600536810031776 ]

[-1,2-Bis(4-pyridyl)ethane-²N:N']bis[(4'-phenyl-2,2':6',2''-terpyridine-³N,N',N'')silver(I)] bis(trifluoromethanesulfonate)

Y. Ma, B. Liu and C. Xue

Online 18 August 2010

Key indicators

• Single-crystal X-ray study
• T = 295 K
• Mean (C-C) = 0.005 Å
• R factor = 0.040
• wR factor = 0.119
• Data-to-parameter ratio = 14.4

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT919_ALERT_3_B Reflection(s) # Likely Affected by the Beamstop           1      

Alert level C
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ag1    --  N1      ..       9.00 su   
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         28      
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of          S1     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of         C28     
PLAT480_ALERT_4_C Long H...A H-Bond Reported H20    ..  F1      ..       2.56 Ang. 
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600          7      

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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