# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ip73 in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 821.15 _exptl_crystal_F_000 4096.00 _reflns_d_resolution_high 0.7500 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 27.8403 _cell_length_b 16.3449 _cell_length_c 24.8487 _cell_angle_alpha 90.000 _cell_angle_beta 111.395 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 259851.02 278151.31 2300.35 o 8 0 0 370364.31 381626.28 5066.16 o 10 0 0 50638.18 56487.86 1734.97 o 12 0 0 218207.20 232984.34 6586.82 o 14 0 0 84915.27 89097.89 2847.60 o 16 0 0 1241.12 610.77 365.13 o 18 0 0 80502.89 79997.34 624.05 o 20 0 0 33532.71 36891.72 504.55 o 22 0 0 185.53 962.62 385.05 o 24 0 0 24252.42 22140.34 464.71 o 26 0 0 32077.90 32071.96 590.85 o 28 0 0 3584.10 3511.92 431.52 o 30 0 0 1806.54 2330.21 444.80 o 32 0 0 21716.44 19856.60 511.19 o 34 0 0 2410.92 1938.52 557.66 o 3 1 0 119845.97 133404.72 8743.58 o 5 1 0 5155.77 5309.60 249.77 o 7 1 0 3155.03 3266.39 199.19 o 9 1 0 321212.31 344340.59 5822.89 o 11 1 0 19272.70 17975.69 435.03 o 13 1 0 7048.09 6850.44 202.19 o 15 1 0 16296.32 16219.37 388.32 o 17 1 0 33516.35 32461.70 373.52 o 19 1 0 3465.42 4310.06 600.81 o 21 1 0 39354.26 39756.01 394.16 o 23 1 0 64706.09 60477.88 680.47 o 25 1 0 3501.30 4003.30 293.37 o 27 1 0 9211.03 8993.13 314.52 o 29 1 0 18624.69 18761.44 369.47 o 31 1 0 2632.46 3115.04 431.52 o 33 1 0 7998.45 7855.75 1009.10 o 2 2 0 169388.30 187147.30 2243.91 o 4 2 0 62837.89 74751.09 3930.16 o 6 2 0 47306.20 46232.24 455.41 o 8 2 0 18799.60 19304.97 311.04 o 10 2 0 6242.82 6965.28 262.82 o 12 2 0 103171.30 104783.88 692.56 o 14 2 0 25301.67 25175.22 661.18 o 16 2 0 895.07 762.50 187.44 o 18 2 0 41946.50 41596.04 352.68 o 20 2 0 20107.47 20660.56 290.89 o 22 2 0 930.26 867.50 279.28 o 24 2 0 32456.01 31370.14 376.00 o 26 2 0 13949.62 14747.83 326.03 o 28 2 0 1076.88 1024.46 302.06 o 30 2 0 17799.05 18127.14 345.01 o 32 2 0 19776.08 19753.62 570.94 o 34 2 0 291.24 663.34 640.64 o 1 3 0 30758.70 26734.38 1029.01 o 3 3 0 7392.38 6685.25 703.71 o 5 3 0 19759.51 19672.41 567.62 o 7 3 0 19430.26 19235.75 360.28 o 9 3 0 178976.31 181616.02 1465.91 o 11 3 0 37388.09 39461.59 366.93 o 13 3 0 19659.99 22688.93 289.40 o 15 3 0 50329.70 49962.88 1339.43 o 17 3 0 49243.61 52045.48 821.41 o 19 3 0 1027.11 1901.36 463.80 o 21 3 0 27260.56 26484.63 444.99 o 23 3 0 43068.62 42665.81 372.65 o 25 3 0 204.74 618.70 349.70 o 27 3 0 17360.23 17146.49 337.60 o 29 3 0 26354.82 26735.80 600.81 o 31 3 0 1131.37 980.69 341.00 o 33 3 0 13373.68 11514.54 376.00 o 0 4 0 111510.78 112002.92 1420.70 o 2 4 0 53726.39 51337.71 1095.40 o 4 4 0 46655.37 49312.88 1035.65 o 6 4 0 17155.78 16232.13 942.71 o 8 4 0 72670.88 72561.59 651.02 o 10 4 0 45217.81 47361.08 385.77 o 12 4 0 50369.88 53600.18 763.29 o 14 4 0 39145.44 36210.96 420.21 o 16 4 0 6.15 500.66 186.57 o 18 4 0 35296.22 36962.62 751.25 o 20 4 0 66303.81 66217.93 1102.53 o 22 4 0 5.48 315.34 323.13 o 24 4 0 40512.20 39029.41 610.77 o 26 4 0 25352.67 25937.60 349.70 o 28 4 0 254.76 555.25 305.38 o 30 4 0 7868.43 8031.30 362.92 o 32 4 0 8245.83 7984.40 366.84 o 1 5 0 5832.51 6857.40 456.53 o 3 5 0 28964.87 25034.85 770.10 o 5 5 0 7405.12 6340.04 544.38 o 7 5 0 38975.81 42123.43 1457.21 o 9 5 0 28145.03 26002.50 337.62 o 11 5 0 76324.73 79635.92 428.31 o 13 5 0 233.15 286.99 223.34 o 15 5 0 41066.10 39876.51 316.49 o 17 5 0 48747.52 50110.23 1237.07 o 19 5 0 2336.42 2517.18 212.47 o 21 5 0 53212.59 52596.58 731.34 o 23 5 0 28738.02 28404.52 460.71 o 25 5 0 284.72 444.53 292.69 o 27 5 0 21321.91 19787.65 1065.53 o 29 5 0 23059.88 23254.77 936.07 o 31 5 0 205.89 486.91 314.41 o 33 5 0 15948.96 15915.59 385.92 o 0 6 0 149463.36 155254.59 1334.40 o 2 6 0 81128.20 75469.85 4604.00 o 4 6 0 18411.87 17546.30 637.32 o 6 6 0 111084.59 116082.81 5506.87 o 8 6 0 21974.74 21249.78 614.09 o 10 6 0 14163.29 15626.92 439.52 o 12 6 0 95465.88 93948.80 1257.31 o 14 6 0 63273.25 63904.59 868.53 o 16 6 0 2034.09 2232.23 228.81 o 18 6 0 37711.35 38740.57 1144.12 o 20 6 0 41557.10 42661.82 452.46 o 22 6 0 7.50 167.51 253.13 o 24 6 0 20752.09 19998.74 506.06 o 26 6 0 23657.92 22656.40 379.64 o 28 6 0 28.14 -40.56 337.98 o 30 6 0 7198.82 7010.73 360.42 o 32 6 0 13421.26 13463.85 383.69 o 1 7 0 21862.56 24490.28 843.12 o 3 7 0 42643.88 34096.34 1511.47 o 5 7 0 8345.41 7608.05 604.13 o 7 7 0 6410.29 8110.81 424.88 o 9 7 0 91332.34 96501.36 916.15 o 11 7 0 64336.51 60707.58 1089.68 o 13 7 0 2622.14 3261.44 265.59 o 15 7 0 31025.37 30425.29 316.40 o 17 7 0 34050.71 36402.12 1704.21 o 19 7 0 336.98 390.59 215.39 o 21 7 0 22930.49 22795.09 487.62 o 23 7 0 25736.99 24910.24 795.26 o 25 7 0 2837.37 3184.22 333.38 o 27 7 0 11102.86 12081.17 330.73 o 29 7 0 13767.69 14677.71 1005.78 o 31 7 0 980.46 690.34 319.11 o 0 8 0 405506.91 408743.25 1865.50 o 2 8 0 68624.52 65959.91 1455.96 o 4 8 0 4225.53 3598.86 272.92 o 6 8 0 85931.02 87532.74 4340.60 o 8 8 0 77409.94 56902.98 32025.50 o 10 8 0 2876.10 3631.05 286.98 o 12 8 0 74893.23 74098.61 1311.16 o 14 8 0 52863.39 55830.12 544.06 o 16 8 0 1202.07 1141.85 250.07 o 18 8 0 28599.45 30033.65 697.53 o 20 8 0 35961.28 35226.66 350.21 o 22 8 0 1242.35 1388.69 261.60 o 24 8 0 23389.36 23591.76 339.12 o 26 8 0 25199.30 24833.16 564.30 o 28 8 0 3643.01 3698.04 323.91 o 30 8 0 5471.44 4433.47 358.90 o 32 8 0 10794.58 9466.36 379.47 o 1 9 0 45412.76 47042.79 637.32 o 3 9 0 223574.58 227738.64 4496.03 o 5 9 0 31418.24 31980.38 1015.22 o 7 9 0 20944.65 21933.69 979.75 o 9 9 0 97386.05 105583.21 949.35 o 11 9 0 33703.22 32263.74 392.35 o 13 9 0 2766.59 2295.64 291.90 o 15 9 0 45146.18 46016.98 356.05 o 17 9 0 25434.53 27286.80 2453.46 o 19 9 0 1088.73 1158.48 217.51 o 21 9 0 25477.36 24820.39 319.28 o 23 9 0 30329.89 30207.36 336.97 o 25 9 0 2124.01 2390.28 285.10 o 27 9 0 6005.73 5568.04 347.73 o 29 9 0 12022.00 11896.72 985.86 o 31 9 0 2471.90 2985.42 683.79 o 0 10 0 90596.94 81325.10 916.15 o 2 10 0 30017.63 29382.83 458.38 o 4 10 0 10216.59 9989.84 314.16 o 6 10 0 107971.09 113037.91 4645.48 o 8 10 0 7258.30 6384.45 367.41 o 10 10 0 8813.18 9064.22 304.77 o 12 10 0 40961.55 40109.71 906.19 o 14 10 0 17358.35 17345.06 349.32 o 16 10 0 146.84 180.57 270.73 o 18 10 0 24229.40 25526.84 624.76 o 20 10 0 26622.65 24559.11 645.22 o 22 10 0 1505.32 1892.73 298.52 o 24 10 0 17333.97 17934.27 306.08 o 26 10 0 21147.54 21021.87 1384.19 o 28 10 0 19.33 429.56 342.95 o 30 10 0 2957.57 2905.38 564.30 o 1 11 0 34929.09 33501.67 567.62 o 3 11 0 53642.34 53993.29 1570.07 o 5 11 0 19904.10 20456.76 527.96 o 7 11 0 21673.88 21266.67 1708.52 o 9 11 0 47415.87 42412.60 3040.56 o 11 11 0 5647.41 5493.90 282.72 o 13 11 0 4945.64 5092.46 307.85 o 15 11 0 36802.85 36149.64 471.35 o 17 11 0 9573.58 11047.48 304.15 o 19 11 0 2470.62 3157.32 675.34 o 21 11 0 15687.99 15220.82 324.80 o 23 11 0 20086.37 20295.45 326.30 o 25 11 0 89.43 233.36 336.56 o 27 11 0 15301.52 14692.63 501.23 o 29 11 0 17324.75 16625.23 1185.02 o 0 12 0 34828.81 30730.93 643.96 o 2 12 0 4572.43 4570.93 361.07 o 4 12 0 6561.69 6494.65 374.21 o 6 12 0 28522.66 29836.27 544.91 o 8 12 0 7500.32 7022.43 315.04 o 10 12 0 20414.11 17943.76 774.77 o 12 12 0 15338.08 16469.96 671.49 o 14 12 0 12720.33 12610.47 529.65 o 16 12 0 877.57 976.32 304.11 o 18 12 0 16917.54 17997.45 374.55 o 20 12 0 16738.22 16698.62 779.75 o 22 12 0 1892.61 1799.30 275.10 o 24 12 0 17302.03 16434.45 404.53 o 26 12 0 21189.79 21567.21 2001.59 o 28 12 0 1389.77 1253.52 354.11 o 1 13 0 16277.98 14959.54 401.18 o 3 13 0 60467.32 62128.68 1565.47 o 5 13 0 25902.59 25957.18 1092.08 o 7 13 0 14604.81 15007.23 492.06 o 9 13 0 30485.70 29525.20 1254.35 o 11 13 0 18478.17 19621.71 566.09 o 13 13 0 274.12 602.88 301.80 o 15 13 0 19313.14 20015.28 772.52 o 17 13 0 16076.78 15876.53 636.11 o 19 13 0 485.61 665.19 327.00 o 21 13 0 10664.90 11496.10 380.71 o 23 13 0 19182.85 18890.82 421.75 o 25 13 0 321.36 340.15 347.60 o 27 13 0 9272.32 8683.30 421.79 o 0 14 0 51660.18 52512.23 3349.27 o 2 14 0 14617.76 12970.80 1715.32 o 4 14 0 13542.94 12974.80 425.77 o 6 14 0 29233.41 30442.58 483.20 o 8 14 0 10178.58 10846.62 486.37 o 10 14 0 3235.05 3202.69 246.34 o 12 14 0 21045.79 22329.97 1008.14 o 14 14 0 54380.62 53763.84 1618.84 o 16 14 0 2542.10 2552.60 417.01 o 18 14 0 23239.44 21264.57 687.07 o 20 14 0 16442.41 17245.63 889.25 o 22 14 0 2345.49 1974.27 349.32 o 24 14 0 9440.04 9699.26 570.94 o 26 14 0 11467.50 9850.06 3106.95 o 1 15 0 12138.88 12297.03 422.49 o 3 15 0 33463.83 34962.17 453.54 o 5 15 0 16102.97 15739.57 428.75 o 7 15 0 549.13 813.69 369.47 o 9 15 0 52428.64 53933.10 1063.63 o 11 15 0 15070.61 14654.37 286.51 o 13 15 0 886.00 1186.43 274.77 o 15 15 0 14366.43 14732.71 616.14 o 17 15 0 20867.19 20482.79 516.88 o 19 15 0 68.84 277.10 311.68 o 21 15 0 8959.88 8743.64 332.26 o 23 15 0 16817.99 16221.92 403.51 o 25 15 0 213.26 782.13 411.60 o 0 16 0 60421.00 58700.12 863.04 o 2 16 0 8157.49 7890.00 419.68 o 4 16 0 2377.07 2573.26 409.84 o 6 16 0 37417.93 36551.73 526.21 o 8 16 0 11815.10 12540.67 352.08 o 10 16 0 320.93 613.39 276.94 o 12 16 0 33830.84 33390.77 653.51 o 14 16 0 27834.32 27628.75 939.06 o 16 16 0 139.41 531.07 268.59 o 18 16 0 18928.78 18122.58 332.56 o 20 16 0 13225.00 14003.78 662.13 o 22 16 0 100.87 243.62 381.73 o 1 17 0 1723.90 2140.03 409.13 o 3 17 0 35269.96 35586.63 525.43 o 5 17 0 14409.67 13891.87 462.46 o 7 17 0 11666.27 10914.04 342.26 o 9 17 0 24829.70 25179.49 391.41 o 11 17 0 4997.37 5129.60 309.83 o 13 17 0 3619.80 3799.40 305.64 o 15 17 0 21304.09 21876.89 370.23 o 17 17 0 3855.31 4114.63 289.41 o 19 17 0 231.28 391.77 266.57 o 21 17 0 11040.22 10802.28 357.40 o 0 18 0 17291.54 18236.74 723.63 o 2 18 0 14119.02 14404.51 490.54 o 4 18 0 6147.99 6094.12 489.63 o 6 18 0 31247.62 31513.64 460.69 o 8 18 0 11134.90 10931.03 402.87 o 10 18 0 1895.36 2142.36 344.26 o 12 18 0 13267.98 13908.16 379.79 o 14 18 0 11750.52 11696.67 372.91 o 16 18 0 4.28 95.76 271.76 o 18 18 0 12897.27 12645.64 404.97 o 1 19 0 4889.73 5750.12 493.24 o 3 19 0 22170.24 21613.19 430.77 o 5 19 0 5410.62 5456.73 373.72 o 7 19 0 4748.30 5160.93 361.90 o 9 19 0 10960.39 10994.40 385.02 o 11 19 0 5380.09 5536.02 373.27 o 13 19 0 1535.07 2089.90 329.57 o 15 19 0 14330.75 15297.86 565.38 o 0 20 0 14619.65 14917.92 549.06 o 2 20 0 7477.09 7800.54 409.33 o 4 20 0 2954.07 3086.84 364.03 o 6 20 0 18867.84 18572.60 670.37 o 8 20 0 4180.24 4335.41 398.84 o 10 20 0 725.98 718.60 369.98 o 12 20 0 11031.83 11158.73 408.30 o 1 21 0 3405.58 3780.12 387.04 o 3 21 0 15117.42 15134.64 433.07 o 5 21 0 5534.15 5659.06 395.10 o 7 21 0 1804.63 1841.56 388.96 o 9 21 0 8021.07 7381.30 460.23 o -33 1 1 2299.92 2750.40 404.97 o -31 1 1 163.94 1064.10 334.91 o -29 1 1 2.78 458.08 302.54 o -27 1 1 69.99 73.03 292.11 o -25 1 1 131.26 86.97 279.28 o -23 1 1 404.83 495.60 283.98 o -21 1 1 3820.00 4360.60 233.41 o -19 1 1 1.02 -155.63 185.80 o -17 1 1 464.60 657.06 191.69 o -15 1 1 372.66 395.56 169.72 o -13 1 1 3398.99 3484.54 172.63 o -11 1 1 3376.76 4327.97 214.80 o -9 1 1 1354.10 1692.79 216.32 o -7 1 1 1506.51 1628.73 219.00 o -5 1 1 45632.99 48015.72 434.69 o -3 1 1 410.17 666.44 285.12 o 3 1 1 51776.12 56469.49 1148.51 o 5 1 1 222661.55 248896.72 5840.34 o 7 1 1 73152.97 79015.00 1035.90 o 9 1 1 26674.04 28466.44 453.05 o 11 1 1 44842.86 48587.76 381.45 o 13 1 1 28427.20 32497.07 787.03 o 15 1 1 2946.76 2148.44 262.88 o 17 1 1 262.95 171.67 291.90 o 19 1 1 6278.54 6870.20 298.20 o 21 1 1 2666.50 2134.39 283.98 o 23 1 1 322.19 292.11 281.66 o 25 1 1 1205.95 1200.85 283.75 o 27 1 1 192.66 402.26 302.06 o 29 1 1 394.96 239.55 333.23 o 31 1 1 69.51 195.47 344.44 o 33 1 1 49.57 72.59 319.11 o -34 2 1 126.93 653.59 353.97 o -32 2 1 0.80 419.04 421.56 o -30 2 1 196.91 1492.19 524.46 o -28 2 1 176.13 104.85 541.06 o -26 2 1 1057.12 1024.34 325.30 o -24 2 1 2516.30 3133.38 398.33 o -22 2 1 1921.69 1834.21 229.78 o -20 2 1 297.82 489.05 188.19 o -18 2 1 163.37 339.14 184.59 o -16 2 1 1394.93 1510.02 256.63 o -14 2 1 531.40 1442.23 188.70 o -12 2 1 10280.00 11642.32 326.42 o -10 2 1 1226.00 1427.38 187.08 o -8 2 1 2006.89 2076.08 192.86 o -6 2 1 12784.92 11843.54 347.22 o -4 2 1 156.37 101.45 363.91 o -2 2 1 5553.47 5695.06 375.59 o 0 2 1 18029.70 14001.19 690.43 o 2 2 1 6166.27 6406.43 823.21 o 4 2 1 26617.26 29688.64 876.32 o 6 2 1 1674.99 2556.42 285.61 o 8 2 1 6111.18 6415.07 241.55 o 10 2 1 1416.25 1123.83 205.98 o 12 2 1 17268.06 20377.50 460.83 o 14 2 1 4.40 131.56 264.16 o 16 2 1 542.20 418.01 206.91 o 18 2 1 5.79 240.96 279.04 o 20 2 1 11133.62 10149.74 365.13 o 22 2 1 8240.46 8422.42 833.17 o 24 2 1 127.19 -279.28 279.28 o 26 2 1 111.01 76.35 587.53 o 28 2 1 237.41 484.72 726.95 o 30 2 1 38.52 -189.38 316.84 o 32 2 1 610.66 640.84 690.43 o -33 3 1 238.96 667.54 319.11 o -31 3 1 8.87 293.51 309.72 o -29 3 1 1159.79 1934.35 373.18 o -27 3 1 57.47 -72.12 560.98 o -25 3 1 557.10 960.39 279.05 o -23 3 1 2352.51 2610.67 245.62 o -21 3 1 346.06 410.12 209.71 o -19 3 1 1950.09 1948.12 185.49 o -17 3 1 1152.86 1235.10 308.19 o -15 3 1 1709.65 1468.40 223.21 o -13 3 1 2037.54 2042.34 240.37 o -11 3 1 9130.17 11687.43 279.19 o -9 3 1 5.09 219.55 242.64 o -7 3 1 16128.51 16943.91 317.56 o -5 3 1 5804.38 5945.19 398.69 o -3 3 1 12291.17 10874.33 730.27 o -1 3 1 2864.10 4647.15 663.88 o 1 3 1 20056.43 18180.54 864.59 o 3 3 1 7149.85 6426.34 776.74 o 5 3 1 3816.11 4660.43 590.85 o 7 3 1 7398.94 7976.80 291.09 o 9 3 1 388.85 924.05 256.95 o 11 3 1 13609.63 16498.92 365.08 o 13 3 1 2769.49 3776.56 197.04 o 15 3 1 2202.97 1832.53 223.17 o 17 3 1 47.42 483.53 255.28 o 19 3 1 29.42 -255.03 255.03 o 21 3 1 24142.57 21967.39 326.23 o 23 3 1 0.64 141.63 274.35 o 25 3 1 910.09 1659.24 826.53 o 27 3 1 367.88 523.28 302.76 o 29 3 1 710.30 1172.01 304.70 o 31 3 1 2206.70 2532.80 323.91 o 33 3 1 5.33 723.67 428.20 o -34 4 1 400.02 262.23 319.21 o -32 4 1 257.70 251.71 352.25 o -30 4 1 29.54 387.28 959.30 o -28 4 1 223.03 1140.98 329.74 o -26 4 1 4.61 362.38 288.44 o -24 4 1 48.51 -64.74 317.24 o -22 4 1 1340.41 1301.95 235.94 o -20 4 1 980.47 891.39 216.68 o -18 4 1 424.66 396.30 223.34 o -16 4 1 2510.76 2879.26 213.34 o -14 4 1 6290.78 6711.45 240.99 o -12 4 1 15356.68 17986.52 293.04 o -10 4 1 11392.36 13175.56 272.61 o -8 4 1 7577.82 8180.18 288.18 o -6 4 1 725.49 796.15 370.50 o -4 4 1 696.30 1141.87 604.13 o -2 4 1 7251.21 8530.84 697.07 o 0 4 1 966.45 369.73 422.23 o 2 4 1 5669.07 3512.92 557.67 o 4 4 1 1699.77 1002.46 630.68 o 6 4 1 1522.64 1799.11 504.55 o 8 4 1 13103.14 15129.86 716.99 o 10 4 1 3365.37 3598.05 269.38 o 12 4 1 19517.98 21440.04 436.02 o 14 4 1 4365.46 5246.28 335.38 o 16 4 1 936.61 691.43 233.29 o 18 4 1 5187.21 5204.33 222.11 o 20 4 1 935.14 884.32 278.83 o 22 4 1 45.07 160.78 395.01 o 24 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