# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' J in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 395.55 _exptl_crystal_F_000 1612.00 _reflns_d_resolution_high 0.7661 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.6999 _cell_length_b 16.1522 _cell_length_c 18.4294 _cell_angle_alpha 83.294 _cell_angle_beta 72.374 _cell_angle_gamma 71.380 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11171.07 11424.42 179.43 o 2 0 0 83951.02 80866.13 933.71 o 3 0 0 1323.63 1538.46 35.81 o 4 0 0 13238.02 13952.69 202.52 o 5 0 0 18226.59 18035.80 260.26 o 6 0 0 133.55 85.60 16.24 o 7 0 0 15539.16 15035.98 234.49 o 8 0 0 11426.43 11049.10 188.90 o 9 0 0 1183.69 1177.88 52.92 o 10 0 0 1623.03 1526.32 63.11 o 11 0 0 109.23 57.36 26.65 o 12 0 0 1302.27 1265.83 111.22 o 13 0 0 1064.27 1028.32 78.30 o -13 1 0 313.00 499.33 116.74 o -12 1 0 36.24 12.42 27.61 o -11 1 0 553.77 519.79 70.56 o -10 1 0 1.40 -10.67 19.48 o -9 1 0 5905.53 5638.55 122.48 o -8 1 0 7348.12 7342.37 141.02 o -7 1 0 9318.71 9100.77 157.75 o -6 1 0 12584.24 12465.44 195.73 o -5 1 0 6216.98 6419.05 111.81 o -4 1 0 9203.24 9698.06 149.04 o -3 1 0 5002.33 5380.70 100.80 o -2 1 0 76043.99 75104.18 968.09 o -1 1 0 60316.14 60550.12 1619.19 o 1 1 0 25116.98 25432.76 507.96 o 2 1 0 3644.16 3859.06 54.51 o 3 1 0 329.46 365.38 16.81 o 4 1 0 36593.72 36817.00 441.91 o 5 1 0 3511.77 3573.59 65.65 o 6 1 0 35835.54 34798.23 480.13 o 7 1 0 1979.23 1909.86 57.44 o 8 1 0 5804.39 5447.33 139.22 o 9 1 0 1966.46 1929.41 64.57 o 10 1 0 512.01 517.94 50.55 o 11 1 0 2458.33 2485.44 106.78 o 12 1 0 145.05 120.29 33.04 o 13 1 0 3194.01 3164.26 141.69 o 14 1 0 1638.59 1576.04 156.72 o -12 2 0 49.76 26.28 46.32 o -11 2 0 611.04 573.81 47.47 o -10 2 0 7930.29 7770.07 158.25 o -9 2 0 165.70 230.27 30.93 o -8 2 0 10095.56 10005.05 176.77 o -7 2 0 4871.49 5068.64 105.01 o -6 2 0 589.91 562.34 32.03 o -5 2 0 222.41 283.63 21.69 o -4 2 0 178.70 179.22 14.90 o -3 2 0 61435.83 61433.82 803.74 o -2 2 0 18538.23 18694.39 254.79 o -1 2 0 21609.99 20925.87 582.29 o 0 2 0 8833.30 9783.62 395.20 o 1 2 0 6.51 -4.42 4.42 o 2 2 0 57396.52 57369.79 665.94 o 3 2 0 6447.03 6779.25 127.13 o 4 2 0 20912.21 20670.20 257.56 o 5 2 0 45413.45 43949.50 528.73 o 6 2 0 2652.74 2707.19 57.68 o 7 2 0 8579.75 8446.48 147.66 o 8 2 0 13.32 21.12 15.40 o 9 2 0 512.60 552.65 39.36 o 10 2 0 4691.33 4610.79 111.35 o 11 2 0 657.62 651.54 49.08 o 12 2 0 4791.52 4885.10 125.37 o 13 2 0 371.06 370.14 65.45 o 14 2 0 885.50 863.63 95.25 o -13 3 0 1.62 5.71 61.07 o -12 3 0 2713.67 2833.37 142.17 o -11 3 0 2798.50 2873.21 174.88 o -10 3 0 2342.20 2361.91 120.80 o -9 3 0 10069.59 10019.37 184.72 o -8 3 0 431.63 515.37 36.68 o -7 3 0 352.34 329.00 28.57 o -6 3 0 53.91 34.31 15.55 o -5 3 0 3753.08 3951.11 80.60 o -4 3 0 74195.40 75465.84 886.72 o -3 3 0 183.39 180.06 15.80 o -2 3 0 39640.04 39727.31 602.84 o -1 3 0 3730.72 3837.41 91.85 o 0 3 0 1200.64 1257.66 47.45 o 1 3 0 1673.10 1825.40 38.21 o 2 3 0 18.28 25.62 4.76 o 3 3 0 71929.32 70878.62 824.22 o 4 3 0 12428.41 12382.04 162.68 o 5 3 0 4802.25 4769.60 78.90 o 6 3 0 4746.41 4324.25 77.94 o 7 3 0 11.76 12.70 13.71 o 8 3 0 256.24 304.50 28.76 o 9 3 0 886.38 830.42 45.76 o 10 3 0 6780.32 6698.78 140.91 o 11 3 0 7370.66 7084.52 152.01 o 12 3 0 263.46 248.99 37.31 o 13 3 0 2024.73 2080.17 125.52 o 14 3 0 59.52 48.24 49.84 o -12 4 0 163.34 143.87 69.16 o -11 4 0 5014.89 4820.54 186.43 o -10 4 0 2766.81 2840.27 132.96 o -9 4 0 509.09 574.92 58.94 o -8 4 0 2.37 0.54 16.99 o -7 4 0 22.39 19.15 15.36 o -6 4 0 7239.63 7171.90 130.83 o -5 4 0 17614.00 17924.29 299.09 o -4 4 0 6699.16 6613.44 102.68 o -3 4 0 43418.94 43329.98 518.23 o -2 4 0 1915.33 2011.42 49.77 o -1 4 0 2062.09 2181.81 60.87 o 0 4 0 3311.40 3430.27 50.80 o 1 4 0 21182.34 22685.16 417.12 o 2 4 0 117625.57 114314.00 1199.29 o 3 4 0 333.36 349.57 13.27 o 4 4 0 63439.70 63268.04 742.91 o 5 4 0 9365.93 9363.76 133.11 o 6 4 0 10.78 8.06 9.67 o 7 4 0 3587.46 3523.13 81.26 o 8 4 0 440.22 410.09 32.67 o 9 4 0 10125.60 10159.97 182.08 o 10 4 0 1430.24 1436.77 61.27 o 11 4 0 2591.76 2620.22 87.73 o 12 4 0 649.56 655.92 59.32 o 13 4 0 8.20 24.00 39.29 o 14 4 0 368.71 345.10 67.93 o -12 5 0 3395.30 2902.89 199.70 o -11 5 0 152.17 142.55 70.98 o -10 5 0 591.38 678.89 77.19 o -9 5 0 101.43 48.79 45.13 o -8 5 0 711.17 687.51 52.46 o -7 5 0 9670.69 9936.33 174.90 o -6 5 0 447.58 478.06 31.38 o -5 5 0 7052.51 6293.11 115.43 o -4 5 0 12253.06 11822.44 165.11 o -3 5 0 2112.15 2057.30 44.22 o -2 5 0 5689.62 6056.78 126.65 o -1 5 0 203.02 221.06 15.05 o 0 5 0 29030.98 30615.40 366.80 o 1 5 0 33338.10 35269.25 485.99 o 2 5 0 23974.71 23386.75 239.90 o 3 5 0 43470.45 43388.61 433.90 o 4 5 0 84.42 93.90 10.94 o 5 5 0 3.95 21.64 19.34 o 6 5 0 2890.65 2855.56 59.32 o 7 5 0 2759.37 2627.94 60.40 o 8 5 0 14278.29 13665.50 199.05 o 9 5 0 62.41 84.06 28.89 o 10 5 0 10407.28 10424.02 192.36 o 11 5 0 799.94 780.89 60.18 o 12 5 0 72.24 76.80 42.43 o 13 5 0 484.91 486.88 73.52 o 14 5 0 9.35 -28.43 42.76 o -12 6 0 79.05 63.13 64.40 o -11 6 0 696.41 683.81 110.40 o -10 6 0 41.45 36.85 41.90 o -9 6 0 1013.44 827.64 106.35 o -8 6 0 4778.56 4657.75 165.90 o -7 6 0 771.20 794.32 53.43 o -6 6 0 15423.64 15498.09 288.91 o -5 6 0 2345.59 2390.61 62.12 o -4 6 0 7636.52 7756.70 132.15 o -3 6 0 947.38 1048.76 31.49 o -2 6 0 21.50 42.06 10.52 o -1 6 0 32053.15 31601.57 386.64 o 0 6 0 1626.76 1670.88 29.70 o 1 6 0 33795.93 34611.36 359.65 o 2 6 0 26457.59 27618.19 265.26 o 3 6 0 3385.62 3545.44 49.67 o 4 6 0 5436.84 5859.35 75.04 o 5 6 0 84.91 76.46 12.23 o 6 6 0 21303.10 21096.08 274.35 o 7 6 0 11843.51 11876.13 173.27 o 8 6 0 4228.39 4216.54 85.73 o 9 6 0 9085.88 9047.01 168.53 o 10 6 0 240.74 159.80 29.03 o 11 6 0 131.05 128.47 33.66 o 12 6 0 51.68 127.10 46.95 o 13 6 0 584.43 697.60 85.38 o 14 6 0 3409.92 3567.86 179.64 o -11 7 0 38.41 -22.52 51.08 o -10 7 0 398.57 400.46 67.45 o -9 7 0 624.55 774.32 82.06 o -8 7 0 5828.98 5587.13 279.73 o -7 7 0 8312.49 8201.45 324.77 o -6 7 0 771.24 795.13 51.74 o -5 7 0 2224.40 2228.68 88.89 o -4 7 0 18.73 15.98 11.98 o -3 7 0 1354.90 1266.02 36.27 o -2 7 0 17642.00 17762.06 232.38 o -1 7 0 49.90 104.44 12.92 o 0 7 0 85776.77 88681.09 897.86 o 1 7 0 2584.27 2739.57 42.98 o 2 7 0 748.05 726.15 23.72 o 3 7 0 12050.80 13559.31 150.29 o 4 7 0 437.58 397.91 23.21 o 5 7 0 11593.71 10973.43 139.47 o 6 7 0 2944.15 2933.92 87.10 o 7 7 0 12148.48 11819.98 173.06 o 8 7 0 5691.81 5369.35 100.62 o 9 7 0 545.44 544.18 39.87 o 10 7 0 19.99 11.36 30.86 o 11 7 0 32.35 -2.50 27.95 o 12 7 0 4112.47 4110.59 169.49 o 13 7 0 1968.55 1994.54 127.98 o 14 7 0 1007.44 842.37 98.48 o -11 8 0 421.56 484.11 103.58 o -10 8 0 175.59 156.56 66.62 o -9 8 0 3967.77 4288.95 176.04 o -8 8 0 3214.02 3169.98 315.41 o -7 8 0 2149.92 2229.12 114.90 o -6 8 0 5026.83 4908.63 278.77 o -5 8 0 12.96 12.93 19.92 o -4 8 0 6909.86 7206.71 157.50 o -3 8 0 3651.68 3555.70 93.87 o -2 8 0 18558.87 19114.13 250.79 o -1 8 0 18592.22 18238.11 238.38 o 0 8 0 2777.17 2900.31 46.69 o 1 8 0 660.97 573.83 20.29 o 2 8 0 876.96 976.64 23.28 o 3 8 0 9058.59 9105.92 102.32 o 4 8 0 25786.60 26645.04 280.36 o 5 8 0 5471.36 5490.67 75.91 o 6 8 0 33263.64 32962.79 411.88 o 7 8 0 242.59 250.01 22.29 o 8 8 0 136.11 132.80 24.68 o 9 8 0 39.68 38.56 25.29 o 10 8 0 657.77 658.31 92.84 o 11 8 0 6259.19 6305.60 276.22 o 12 8 0 166.81 233.53 56.79 o 13 8 0 3512.14 3448.63 180.43 o 14 8 0 755.66 733.05 95.40 o -10 9 0 3637.09 3805.91 231.74 o -9 9 0 132.69 143.15 60.12 o -8 9 0 2539.92 2606.32 131.46 o -7 9 0 1017.03 908.11 83.31 o -6 9 0 438.28 419.10 58.73 o -5 9 0 1183.70 1243.36 84.23 o -4 9 0 26.92 35.67 21.05 o -3 9 0 19668.39 19168.71 471.97 o -2 9 0 4405.05 4452.50 110.26 o -1 9 0 11038.48 11200.88 180.91 o 0 9 0 2778.69 2726.88 46.88 o 1 9 0 76.25 91.93 11.41 o 2 9 0 36159.73 39337.62 399.24 o 3 9 0 3683.18 3683.19 52.72 o 4 9 0 24115.55 24533.04 246.26 o 5 9 0 33010.82 33662.89 352.26 o 6 9 0 1123.09 1128.88 34.06 o 7 9 0 4287.01 4406.88 84.71 o 8 9 0 559.65 521.86 31.90 o 9 9 0 3363.19 3304.50 90.08 o 10 9 0 8003.63 7907.33 191.33 o 11 9 0 1006.26 927.19 95.65 o 12 9 0 6040.03 6402.45 224.96 o 13 9 0 411.43 345.42 66.96 o 14 9 0 206.08 236.27 65.12 o -9 10 0 2055.35 1977.51 172.42 o -8 10 0 231.37 193.50 55.01 o -7 10 0 525.73 548.87 71.71 o -6 10 0 3652.76 3373.00 144.58 o -5 10 0 1037.65 884.34 75.98 o -4 10 0 21702.78 21396.88 544.54 o -3 10 0 19.34 59.63 23.12 o -2 10 0 6643.72 6290.85 142.36 o -1 10 0 114.95 91.19 24.25 o 0 10 0 98.80 130.09 16.40 o 1 10 0 6815.17 7206.59 101.95 o 2 10 0 115.36 121.12 14.47 o 3 10 0 37999.70 38190.16 349.54 o 4 10 0 10398.25 10344.86 118.77 o 5 10 0 8163.26 8086.52 105.08 o 6 10 0 1695.00 1653.64 38.36 o 7 10 0 1132.66 1136.09 40.61 o 8 10 0 1176.47 1167.26 71.22 o 9 10 0 2894.23 2843.80 83.19 o 10 10 0 11383.92 11007.29 242.91 o 11 10 0 8789.09 9193.76 275.71 o 12 10 0 45.73 32.71 41.30 o 13 10 0 91.14 97.76 51.84 o 14 10 0 33.19 44.53 52.23 o -9 11 0 155.65 147.20 67.57 o -8 11 0 276.40 292.65 79.94 o -7 11 0 163.62 124.20 48.91 o -6 11 0 3563.96 3272.72 146.02 o -5 11 0 5852.66 5686.48 193.67 o -4 11 0 2919.85 3122.48 149.82 o -3 11 0 9761.62 9530.10 257.96 o -2 11 0 2.48 -3.50 22.21 o -1 11 0 2903.55 2893.47 87.29 o 0 11 0 1292.06 1372.67 98.00 o 1 11 0 5070.99 5047.50 90.12 o 2 11 0 36918.16 37816.33 368.38 o 3 11 0 32.65 24.56 8.70 o 4 11 0 8483.59 8601.06 114.73 o 5 11 0 1199.59 1261.06 31.06 o 6 11 0 383.76 399.17 21.48 o 7 11 0 8120.76 8024.06 156.23 o 8 11 0 779.56 776.85 43.40 o 9 11 0 22865.09 22704.40 353.02 o 10 11 0 2764.58 2752.81 135.05 o 11 11 0 1366.87 1171.90 98.67 o 12 11 0 525.61 589.70 81.08 o 13 11 0 8.33 34.38 50.58 o 14 11 0 963.68 887.32 108.90 o -8 12 0 63.09 57.58 62.50 o -7 12 0 7130.61 6910.54 241.96 o -6 12 0 703.96 690.89 81.59 o -5 12 0 3914.95 3855.08 159.90 o -4 12 0 801.60 832.50 79.90 o -3 12 0 25.99 9.65 29.46 o -2 12 0 419.92 398.42 54.06 o -1 12 0 57.78 42.49 23.04 o 0 12 0 9789.95 9838.18 202.35 o 1 12 0 16126.41 15835.19 456.00 o 2 12 0 3628.08 3657.56 71.67 o 3 12 0 6994.67 7129.15 114.29 o 4 12 0 101.51 117.85 12.12 o 5 12 0 2542.45 2516.45 46.30 o 6 12 0 10410.18 10224.06 143.27 o 7 12 0 7363.22 7141.26 122.53 o 8 12 0 17273.51 17429.17 279.53 o 9 12 0 239.52 295.35 42.79 o 10 12 0 5240.66 5527.72 158.50 o 11 12 0 674.23 608.17 78.59 o 12 12 0 177.34 122.00 54.36 o 13 12 0 2052.01 2032.05 226.83 o -7 13 0 585.23 440.33 99.61 o -6 13 0 3145.59 3440.26 163.98 o -5 13 0 464.22 384.30 65.49 o -4 13 0 625.38 656.74 76.99 o -3 13 0 32.92 72.94 35.35 o -2 13 0 453.60 526.16 129.04 o -1 13 0 20701.06 20988.95 499.33 o 0 13 0 2772.76 2881.26 93.72 o 1 13 0 10093.26 10302.43 213.22 o 2 13 0 6808.44 6814.36 109.02 o 3 13 0 34.14 24.85 11.83 o 4 13 0 4391.31 4501.28 64.71 o 5 13 0 1095.88 1167.87 31.71 o 6 13 0 28669.32 28025.66 332.99 o 7 13 0 20934.25 21156.00 264.99 o 8 13 0 1190.44 1150.67 63.62 o 9 13 0 2357.61 2372.21 111.73 o 10 13 0 245.39 209.27 51.85 o 11 13 0 1689.43 1525.18 114.77 o 12 13 0 1544.56 1764.13 202.48 o 13 13 0 1304.22 1472.86 126.67 o -6 14 0 12.67 17.92 59.32 o -5 14 0 258.40 240.06 59.92 o -4 14 0 62.64 35.55 38.88 o -3 14 0 3457.16 3233.54 285.75 o -2 14 0 10427.59 10538.17 293.91 o -1 14 0 3346.09 3169.06 135.73 o 0 14 0 11862.65 12064.24 589.35 o 1 14 0 162.51 196.63 31.24 o 2 14 0 108.26 106.54 22.33 o 3 14 0 80.52 94.56 22.62 o 4 14 0 3136.66 3124.68 90.79 o 5 14 0 15191.65 15404.16 206.42 o 6 14 0 389.12 360.99 27.04 o 7 14 0 12307.57 12615.88 175.75 o 8 14 0 859.94 928.28 42.77 o 9 14 0 221.72 202.15 38.52 o 10 14 0 451.42 418.07 68.12 o 11 14 0 371.40 330.47 116.27 o 12 14 0 4276.21 4166.23 233.57 o 13 14 0 2263.97 2476.72 158.03 o -5 15 0 149.33 189.71 83.75 o -4 15 0 5101.85 5128.29 202.34 o -3 15 0 1596.57 1386.98 107.05 o -2 15 0 6355.39 5818.23 487.99 o -1 15 0 4101.78 4157.48 320.41 o 0 15 0 141.30 136.51 42.18 o 1 15 0 52.41 101.45 37.82 o 2 15 0 5.56 24.84 17.10 o 3 15 0 10930.70 10501.33 178.65 o 4 15 0 14237.33 14242.44 210.71 o 5 15 0 281.96 318.39 37.26 o 6 15 0 10619.83 10700.31 178.68 o 7 15 0 1170.14 1177.71 40.92 o 8 15 0 92.99 64.38 24.24 o 9 15 0 1320.30 1331.84 69.13 o 10 15 0 127.42 91.15 37.48 o 11 15 0 6064.00 6089.72 227.08 o 12 15 0 304.27 363.59 75.54 o -4 16 0 54.06 56.34 49.97 o -3 16 0 6554.67 6606.28 256.57 o -2 16 0 1958.56 2047.44 261.25 o -1 16 0 594.01 595.39 76.52 o 0 16 0 158.25 85.49 40.97 o 1 16 0 142.08 135.71 48.02 o 2 16 0 10733.57 10812.26 197.96 o 3 16 0 4559.59 4561.68 95.60 o 4 16 0 5339.85 5500.15 150.66 o 5 16 0 5593.03 5488.63 149.39 o 6 16 0 13.97 3.58 29.19 o 7 16 0 14.28 34.69 25.16 o 8 16 0 338.60 406.76 48.44 o 9 16 0 3250.36 3151.92 162.15 o 10 16 0 4678.32 4750.19 155.87 o 11 16 0 187.65 300.06 54.36 o 12 16 0 3794.30 3964.42 152.92 o -3 17 0 0.17 -39.43 39.43 o -2 17 0 1283.28 1356.91 140.93 o -1 17 0 122.54 114.14 54.41 o 0 17 0 488.45 491.55 72.18 o 1 17 0 3682.74 3861.96 135.06 o 2 17 0 22.77 12.17 36.04 o 3 17 0 13784.02 13302.34 340.89 o 4 17 0 2680.88 2585.85 90.04 o 5 17 0 448.35 373.31 44.10 o 6 17 0 79.98 54.56 26.81 o 7 17 0 13.40 -23.56 23.76 o 8 17 0 6861.93 6680.72 173.43 o 9 17 0 1931.97 1854.35 128.16 o 10 17 0 4169.95 4633.75 260.40 o 11 17 0 3997.94 4350.84 349.43 o -2 18 0 110.50 111.44 79.15 o -1 18 0 1705.59 1747.01 165.20 o 0 18 0 1700.34 1711.26 120.79 o 1 18 0 2021.75 1956.87 121.27 o 2 18 0 8674.29 8047.68 250.76 o 3 18 0 49.38 82.37 42.50 o 4 18 0 2847.26 2775.92 136.29 o 5 18 0 4.74 12.01 28.37 o 6 18 0 744.34 783.42 59.68 o 7 18 0 5778.45 5781.55 147.26 o 8 18 0 260.77 292.51 53.41 o 9 18 0 8107.93 8475.86 407.26 o 10 18 0 402.05 419.45 79.39 o 0 19 0 5734.92 5672.41 219.61 o 1 19 0 4281.96 4349.39 344.20 o 2 19 0 1406.89 1418.99 110.94 o 3 19 0 2365.57 2314.94 130.96 o 4 19 0 29.82 20.83 43.81 o 5 19 0 1736.46 1673.51 112.89 o 6 19 0 2803.58 3304.54 208.50 o 7 19 0 2033.70 1994.76 99.84 o 8 19 0 5556.88 5543.68 330.96 o 9 19 0 6.00 5.71 50.17 o 1 20 0 3248.81 2969.63 158.13 o 2 20 0 586.40 469.95 78.23 o 3 20 0 15.23 -1.29 45.89 o 4 20 0 1971.61 1832.14 126.02 o 5 20 0 215.63 166.75 67.02 o 6 20 0 5834.95 6301.08 226.21 o 7 20 0 3326.53 3485.48 141.48 o 8 20 0 673.30 604.27 89.45 o -7 -20 1 4184.76 4299.07 212.49 o -6 -20 1 850.97 883.58 70.48 o -5 -20 1 4796.68 5059.45 452.14 o -4 -20 1 16.46 -22.96 46.52 o -3 -20 1 17.88 21.81 46.64 o -2 -20 1 1008.02 846.86 95.77 o -9 -19 1 4619.95 4734.85 208.92 o -8 -19 1 891.84 968.92 84.81 o -7 -19 1 4380.98 4454.93 132.70 o -6 -19 1 2945.90 3041.31 107.39 o -5 -19 1 34.58 10.66 29.34 o -4 -19 1 109.50 67.29 49.09 o -3 -19 1 174.12 103.66 49.68 o -2 -19 1 4666.74 4718.95 299.08 o -1 -19 1 4894.44 4691.26 190.84 o 0 -19 1 930.06 761.17 91.31 o -10 -18 1 3674.55 4048.86 420.58 o -9 -18 1 587.65 710.60 93.99 o -8 -18 1 8054.02 8095.41 185.20 o -7 -18 1 703.70 656.56 58.26 o -6 -18 1 332.48 413.36 46.88 o -5 -18 1 309.47 301.49 42.68 o -4 -18 1 265.59 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