[HTML version][PDF version][Article Abstract][CIF][3d view][Structure Factors][Supplementary Material][Issue contents]  [Open access]

[Contents scheme]

Acta Cryst. (2010). E66, m1489  [ doi:10.1107/S1600536810043643 ]

Bis[[mu]-2-(4-hydroxyphenyl)acetato]-[kappa]3O,O':O;[kappa]3O:O,O'-bis{aqua(4,4'-bipyridine-[kappa]N)bis[2-(4-hydroxyphenyl)acetato-[kappa]2O,O']ytterbium(III)} monohydrate

J.-L. Liu, J.-F. Liu and G.-L. Zhao

Online 31 October 2010


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X) Yb1 -- O10 .. 16.37 su PLAT919_ALERT_3_B Reflection # Likely Affected by the Beamstop ... 2 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 3
Alert level C PLAT230_ALERT_2_C Hirshfeld Test Diff for N2 -- C58 .. 5.63 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Yb1 -- O11 .. 8.15 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Yb2 -- O7 .. 5.12 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Yb2 -- O16 .. 5.68 su PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O7 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O10 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O14 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C7 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C39 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C36 PLAT334_ALERT_2_C Small Average Benzene C-C Dist. C33 -C38 1.37 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 42 PLAT918_ALERT_3_C Reflection(s) # with I(obs) much smaller I(calc) 1 PLAT141_ALERT_4_C su on a - Axis Small or Missing (x 100000) ..... 10 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference N4 -- C64 .. 0.16 Ang.
Alert level G PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 9 PLAT154_ALERT_1_G The su's on the Cell Angles are Equal (x 10000) 100 Deg. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 6 PLAT794_ALERT_5_G Note: Tentative Bond Valency for Yb1 ....... 2.89 PLAT794_ALERT_5_G Note: Tentative Bond Valency for Yb2 ....... 2.87
0 ALERT level A = In general: serious problem 3 ALERT level B = Potentially serious problem 15 ALERT level C = Check and explain 5 ALERT level G = General alerts; check 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 12 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster