Acta Cryst. (2010). E66, m1411  [ doi:10.1107/S1600536810040298 ]

Tetrakis[-2-(3,4-dimethoxyphenyl)acetato]-³O¹,O^1':O¹;³O¹:O¹,O^1';⁴O¹:O^1'-bis{[2-(3,4-dimethoxyphenyl)acetato-²O¹,O^1'](1,10-phenanthroline-²N,N')erbium(III)}

J.-L. Liu, H.-Q. Li and G.-L. Zhao

Online 13 October 2010

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.005 Å
• R factor = 0.023
• wR factor = 0.059
• Data-to-parameter ratio = 17.3

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT230_ALERT_2_C Hirshfeld Test Diff for    O9     --  C21     ..       5.00 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Er1    --  O3      ..       5.04 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Er1    --  O4      ..       6.41 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Er1    --  O8      ..       8.38 su   
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          1      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600          5      
PLAT141_ALERT_4_C su on a - Axis Small or Missing (x 100000) .....         10 Ang. 
PLAT142_ALERT_4_C su on b - Axis Small or Missing (x 100000) .....         10 Ang. 
PLAT774_ALERT_1_C Suspect X-Y Bond in CIF:   ER1    --  ER1     ..       3.86 Ang. 
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600        104      

Alert level G
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal  (x 10000)        100 Deg. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
  10 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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