Acta Cryst. (2010). E66, m1380-m1381  [ doi:10.1107/S1600536810039814 ]

trans-Carbonylchloridobis[tris(4-chlorophenyl)phosphane]rhodium(I) acetone monosolvate

A. R. Burgoyne, R. Meijboom, A. Muller and B. O. Omondi

Online 9 October 2010

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.003 Å
• R factor = 0.026
• wR factor = 0.069
• Data-to-parameter ratio = 21.3

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Rh1    --  Cl1     ..       7.55 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Rh1    --  C37     ..       7.82 su   
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          1      
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of         C38     
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         30      

Alert level G
PLAT431_ALERT_2_G Short Inter HL..A Contact  Cl1    ..  Cl3     ..       3.34 Ang. 
PLAT431_ALERT_2_G Short Inter HL..A Contact  Cl7    ..  Cl7     ..       3.38 Ang. 
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          4      
PLAT960_ALERT_3_G Number of Intensities with I .LT. - 2*sig(I) ..           5      
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal  (x 10000)        100 Deg. 
PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 =          3      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   6 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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