Acta Cryst. (2010). E66, m1472  [ doi:10.1107/S1600536810042881 ]

Bis{-N-[(dimethylamino)dimethylsilyl]-2,6-dimethylanilido}-²N:N';²N':N-dicopper(I)

J. Chen

Online 30 October 2010

Key indicators

• Single-crystal X-ray study
• T = 203 K
• Mean (C-C) = 0.004 Å
• R factor = 0.033
• wR factor = 0.098
• Data-to-parameter ratio = 16.5

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......       0.98      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.595         51      

Alert level G
PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety         C7     
PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety         C8     
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          7     
            N2  -CU1 -N1  -C1    -45.80  1.40   2.677   1.555   1.555   1.555  
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          9     
            N2  -CU1 -N1  -SI1   123.50  1.30   2.677   1.555   1.555   1.555  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   2 ALERT level C = Check and explain
   4 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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