# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' x in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 397.95 _exptl_crystal_F_000 1416.00 _reflns_d_resolution_high 0.7330 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.6298 _cell_length_b 10.4264 _cell_length_c 28.7365 _cell_angle_alpha 84.843 _cell_angle_beta 88.128 _cell_angle_gamma 72.619 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2410.83 2795.16 74.59 o 2 0 0 33547.90 33868.07 577.26 o 3 0 0 10253.11 10333.04 149.83 o 4 0 0 38798.01 39863.66 557.54 o 5 0 0 13989.56 14325.44 210.58 o 6 0 0 14704.53 15062.50 250.58 o 7 0 0 5362.83 5335.29 112.77 o 8 0 0 3327.88 3257.99 86.50 o 9 0 0 2143.52 2097.74 75.46 o 10 0 0 804.45 866.06 63.23 o 11 0 0 859.57 866.65 66.66 o 12 0 0 11.27 133.42 91.89 o -12 1 0 0.60 22.53 96.77 o -11 1 0 350.79 322.58 58.46 o -10 1 0 85.69 109.59 47.95 o -9 1 0 1914.27 1811.75 72.78 o -8 1 0 96.39 147.86 45.08 o -7 1 0 5951.11 5764.62 119.97 o -6 1 0 4924.01 4868.78 91.17 o -5 1 0 8549.82 8554.46 149.04 o -4 1 0 23830.72 24096.41 383.31 o -3 1 0 5933.24 5999.11 102.72 o -2 1 0 64287.29 62970.99 972.30 o -1 1 0 157.88 189.49 10.59 o 0 1 0 93566.80 66196.49 2397.61 o 1 1 0 4352.28 4590.13 80.85 o 2 1 0 9639.73 10206.53 160.11 o 3 1 0 4863.59 5202.34 86.06 o 4 1 0 59986.76 60326.76 913.83 o 5 1 0 6345.34 5990.21 90.77 o 6 1 0 8407.06 8126.30 128.28 o 7 1 0 6582.64 6470.46 109.13 o 8 1 0 3716.29 3749.72 80.75 o 9 1 0 2594.63 2590.13 80.97 o 10 1 0 573.17 628.05 52.51 o 11 1 0 1847.14 1866.16 81.82 o 12 1 0 51.30 1.17 67.22 o -11 2 0 119.41 46.66 69.72 o -10 2 0 2.01 55.69 53.71 o -9 2 0 738.97 777.82 58.57 o -8 2 0 143.52 193.58 48.93 o -7 2 0 1234.46 1385.40 57.46 o -6 2 0 2000.58 1977.34 61.04 o -5 2 0 5184.48 5072.20 91.29 o -4 2 0 12628.64 12887.09 197.57 o -3 2 0 4333.38 4592.52 84.99 o -2 2 0 14337.62 14469.02 210.57 o -1 2 0 3407.93 3796.51 56.38 o 0 2 0 3040.70 2884.47 67.77 o 1 2 0 1511.34 1314.58 34.13 o 2 2 0 69668.46 69081.77 964.85 o 3 2 0 2552.21 2726.35 50.44 o 4 2 0 34206.23 34933.92 459.18 o 5 2 0 2196.41 1946.07 36.91 o 6 2 0 11719.42 11819.51 166.37 o 7 2 0 7099.79 6907.86 106.85 o 8 2 0 3801.01 3849.03 74.09 o 9 2 0 3693.78 3649.14 75.85 o 10 2 0 495.63 586.58 45.04 o 11 2 0 1637.46 1733.44 78.98 o 12 2 0 11.65 77.90 110.37 o -11 3 0 3.95 55.36 141.49 o -10 3 0 62.90 120.73 57.01 o -9 3 0 23.70 -2.32 46.46 o -8 3 0 4.76 52.04 41.11 o -7 3 0 167.28 204.47 41.02 o -6 3 0 135.10 121.79 33.82 o -5 3 0 2072.45 2094.53 62.51 o -4 3 0 3480.33 3694.82 63.14 o -3 3 0 514.90 651.28 32.60 o -2 3 0 671.37 594.26 27.39 o -1 3 0 1551.35 1597.57 47.95 o 0 3 0 11887.58 11790.08 246.18 o 1 3 0 1467.55 1656.46 46.85 o 2 3 0 14133.87 14584.21 306.03 o 3 3 0 1560.10 1627.13 31.53 o 4 3 0 22238.97 22629.45 262.13 o 5 3 0 10371.20 11204.24 147.05 o 6 3 0 9255.80 9366.00 125.54 o 7 3 0 5672.06 5726.04 81.16 o 8 3 0 3982.48 3998.18 68.61 o 9 3 0 3373.57 3358.46 65.54 o 10 3 0 330.46 347.51 38.61 o 11 3 0 997.47 1090.95 61.27 o 12 3 0 50.36 61.70 107.51 o -10 4 0 30.45 86.17 75.04 o -9 4 0 32.62 100.60 54.02 o -8 4 0 132.96 151.24 49.29 o -7 4 0 170.45 156.96 43.70 o -6 4 0 258.97 260.30 39.79 o -5 4 0 262.13 287.16 38.16 o -4 4 0 606.02 704.72 32.39 o -3 4 0 11.97 16.68 16.64 o -2 4 0 1059.76 1139.17 38.73 o -1 4 0 315.65 342.00 25.81 o 0 4 0 2233.78 2213.94 89.20 o 1 4 0 1314.01 1455.76 65.04 o 2 4 0 298.43 376.50 36.57 o 3 4 0 1946.56 2092.39 41.85 o 4 4 0 6443.00 6604.41 83.77 o 5 4 0 3172.84 3311.33 49.00 o 6 4 0 4533.05 4735.54 66.72 o 7 4 0 1441.97 1498.38 34.22 o 8 4 0 2076.99 2173.86 43.84 o 9 4 0 2160.65 2237.67 54.58 o 10 4 0 146.78 141.85 40.95 o 11 4 0 963.14 990.38 63.94 o -10 5 0 18.15 -58.93 116.11 o -9 5 0 185.30 252.37 69.17 o -8 5 0 557.86 596.93 68.65 o -7 5 0 420.71 480.33 62.65 o -6 5 0 443.88 432.66 42.27 o -5 5 0 512.55 538.27 42.00 o -4 5 0 670.92 628.63 61.25 o -3 5 0 318.04 322.62 30.22 o -2 5 0 1140.77 1133.12 53.49 o -1 5 0 155.34 187.62 24.66 o 0 5 0 2079.74 2163.29 56.93 o 1 5 0 64.57 51.41 18.58 o 2 5 0 1035.18 1198.27 42.69 o 3 5 0 1779.79 1968.87 58.47 o 4 5 0 1311.75 1383.23 35.25 o 5 5 0 136.24 238.15 18.57 o 6 5 0 324.30 336.86 18.89 o 7 5 0 598.78 632.49 36.62 o 8 5 0 838.80 861.99 41.68 o 9 5 0 536.18 561.07 39.34 o 10 5 0 260.18 326.30 43.93 o 11 5 0 362.50 424.22 73.73 o -9 6 0 743.09 821.78 130.72 o -8 6 0 221.76 176.44 65.08 o -7 6 0 1016.00 1101.50 65.11 o -6 6 0 340.07 345.87 48.43 o -5 6 0 1924.41 1864.72 91.68 o -4 6 0 6970.35 6858.43 245.06 o -3 6 0 2329.00 2386.00 82.45 o -2 6 0 3890.59 3660.23 117.19 o -1 6 0 128.05 156.43 43.26 o 0 6 0 1305.03 1373.84 64.33 o 1 6 0 149.49 165.60 25.17 o 2 6 0 1534.60 1329.01 66.82 o 3 6 0 200.60 277.67 29.59 o 4 6 0 345.29 437.86 31.89 o 5 6 0 1.92 44.49 20.16 o 6 6 0 224.13 229.85 29.92 o 7 6 0 179.03 238.55 29.39 o 8 6 0 114.34 99.60 30.64 o 9 6 0 139.78 157.62 55.75 o 10 6 0 47.27 85.21 37.26 o 11 6 0 28.29 170.62 55.12 o 12 6 0 2.18 -30.76 106.12 o -8 7 0 178.51 272.25 75.62 o -7 7 0 1140.39 1276.48 143.18 o -6 7 0 1137.35 1139.66 140.07 o -5 7 0 1902.52 1994.19 91.37 o -4 7 0 5030.67 4952.64 137.61 o -3 7 0 3666.59 3628.10 257.72 o -2 7 0 6024.13 5370.46 129.71 o -1 7 0 478.80 698.35 90.32 o 0 7 0 6891.96 7069.69 140.26 o 1 7 0 366.49 460.41 44.06 o 2 7 0 8681.20 8141.85 175.66 o 3 7 0 348.87 428.65 38.47 o 4 7 0 3466.45 3516.84 177.89 o 5 7 0 7.15 16.96 28.70 o 6 7 0 2535.96 2495.74 76.42 o 7 7 0 405.01 432.02 36.22 o 8 7 0 1822.29 1639.28 61.07 o 9 7 0 408.87 404.84 42.52 o 10 7 0 60.62 155.58 48.68 o 11 7 0 7.53 -54.40 54.40 o 12 7 0 3.67 -7.69 107.65 o -8 8 0 51.99 -105.99 105.99 o -7 8 0 1151.61 1261.32 134.08 o -6 8 0 936.90 836.51 81.07 o -5 8 0 2306.26 2374.66 103.42 o -4 8 0 3164.88 2955.60 108.03 o -3 8 0 2170.83 2172.70 87.95 o -2 8 0 6123.11 6579.33 233.11 o -1 8 0 700.02 774.52 53.61 o 0 8 0 8979.72 9315.78 209.73 o 1 8 0 1134.62 1254.54 63.75 o 2 8 0 13063.88 12634.18 259.14 o 3 8 0 79.10 87.98 50.90 o 4 8 0 9411.17 9202.37 234.54 o 5 8 0 33.52 -14.49 42.73 o 6 8 0 5703.26 5306.08 127.82 o 7 8 0 1338.47 1321.93 61.13 o 8 8 0 932.80 1094.19 60.56 o 9 8 0 499.20 559.84 94.56 o 10 8 0 621.42 641.88 77.03 o 11 8 0 100.66 137.34 56.03 o 12 8 0 65.94 67.53 88.38 o -7 9 0 956.44 793.77 306.81 o -6 9 0 413.52 323.48 102.46 o -5 9 0 2106.93 1826.82 191.47 o -4 9 0 1231.88 1229.46 121.72 o -3 9 0 1785.05 1858.82 210.69 o -2 9 0 6557.64 6672.72 228.30 o -1 9 0 2684.81 2861.30 116.48 o 0 9 0 11135.71 11491.00 242.18 o 1 9 0 670.24 734.31 59.17 o 2 9 0 9567.44 9551.44 251.35 o 3 9 0 204.11 257.09 59.01 o 4 9 0 11309.33 10718.62 329.98 o 5 9 0 217.40 196.50 55.87 o 6 9 0 4996.29 4730.83 124.98 o 7 9 0 1133.94 1145.17 64.54 o 8 9 0 2521.70 2551.43 116.56 o 9 9 0 387.90 429.08 69.66 o 10 9 0 570.13 553.13 86.51 o 11 9 0 353.06 212.87 76.72 o 12 9 0 110.14 172.58 99.77 o -6 10 0 192.15 177.23 266.83 o -5 10 0 934.60 912.87 143.03 o -4 10 0 478.77 512.27 111.59 o -3 10 0 1325.77 1549.29 237.61 o -2 10 0 2768.64 2665.80 121.72 o -1 10 0 1149.67 1201.49 88.32 o 0 10 0 5581.26 5773.95 187.39 o 1 10 0 717.60 844.58 143.48 o 2 10 0 7526.60 6887.10 202.44 o 3 10 0 88.71 127.25 66.43 o 4 10 0 7428.07 7045.58 209.07 o 5 10 0 650.42 603.48 74.35 o 6 10 0 2677.99 2580.88 97.07 o 7 10 0 171.46 242.19 66.99 o 8 10 0 2245.19 2233.50 113.92 o 9 10 0 571.46 548.50 82.80 o 10 10 0 489.11 502.06 85.36 o 11 10 0 394.67 551.13 92.03 o -4 11 0 188.77 127.83 239.15 o -3 11 0 949.76 1103.11 127.47 o -2 11 0 930.30 1055.93 115.54 o -1 11 0 448.72 457.51 98.41 o 0 11 0 1963.03 2228.59 143.94 o 1 11 0 346.70 428.83 72.54 o 2 11 0 5085.15 4953.80 233.48 o 3 11 0 33.70 -24.93 62.93 o 4 11 0 3377.39 3521.42 306.93 o 5 11 0 183.80 33.48 90.18 o 6 11 0 3263.43 3199.92 196.58 o 7 11 0 391.67 338.25 81.38 o 8 11 0 1372.92 1355.26 122.80 o 9 11 0 584.09 458.78 88.28 o 10 11 0 393.74 433.72 133.40 o -3 12 0 186.17 243.17 107.43 o -2 12 0 193.70 176.86 156.87 o -1 12 0 362.14 248.42 99.60 o 0 12 0 996.25 1006.15 217.62 o 1 12 0 166.76 223.31 101.37 o 2 12 0 1993.38 1987.69 116.30 o 3 12 0 23.81 63.40 67.84 o 4 12 0 1675.36 1614.22 123.47 o 5 12 0 203.92 200.62 78.39 o 6 12 0 1901.86 2110.76 225.28 o 7 12 0 178.43 168.89 86.89 o 8 12 0 763.32 815.91 99.08 o 9 12 0 371.35 328.89 93.56 o -1 13 0 69.05 166.09 155.33 o 0 13 0 256.69 271.02 107.01 o 1 13 0 2.84 120.02 102.15 o 2 13 0 424.58 470.29 117.54 o 3 13 0 0.41 92.73 80.01 o 4 13 0 733.85 770.03 96.66 o 5 13 0 88.06 54.27 83.67 o 6 13 0 643.52 799.03 103.80 o 7 13 0 188.68 223.40 92.62 o 8 13 0 314.44 233.06 120.58 o 2 14 0 5.16 -34.81 110.57 o 3 14 0 0.35 90.74 119.96 o 4 14 0 60.62 172.75 85.82 o 5 14 0 12.85 209.81 89.23 o -5 -14 1 1025.33 632.55 137.73 o -4 -14 1 0.18 -43.60 86.60 o -3 -14 1 989.81 1125.54 107.10 o -8 -13 1 56.60 -109.95 113.86 o -7 -13 1 797.18 850.34 110.48 o -6 -13 1 28.26 37.91 83.98 o -5 -13 1 1128.91 1026.38 105.37 o -4 -13 1 1.30 -57.89 77.08 o -3 -13 1 1460.79 1517.37 112.50 o -2 -13 1 109.04 216.51 105.99 o -1 -13 1 1571.61 1564.99 243.76 o 0 -13 1 246.36 529.10 114.26 o 1 -13 1 781.76 896.60 203.00 o -9 -12 1 175.66 212.77 145.12 o -8 -12 1 4.23 86.55 82.12 o -7 -12 1 337.69 247.54 85.81 o -6 -12 1 10.27 15.22 76.80 o -5 -12 1 914.90 867.15 112.68 o -4 -12 1 109.40 62.50 76.13 o -3 -12 1 1257.85 1244.82 107.45 o -2 -12 1 83.02 80.95 71.69 o -1 -12 1 1049.55 865.29 117.31 o 0 -12 1 151.70 309.74 99.98 o 1 -12 1 962.87 1003.36 125.56 o 2 -12 1 403.21 447.53 184.55 o 3 -12 1 387.57 459.84 178.40 o -10 -11 1 20.79 0.87 82.47 o -9 -11 1 86.14 140.04 77.93 o -8 -11 1 7.66 63.36 74.74 o -7 -11 1 20.68 15.70 67.41 o -6 -11 1 3.97 2.44 51.61 o -5 -11 1 458.89 459.25 80.33 o -4 -11 1 96.21 181.59 72.12 o -3 -11 1 418.78 312.49 73.89 o -2 -11 1 46.77 182.27 86.81 o -1 -11 1 993.86 1102.51 139.24 o 0 -11 1 230.60 226.78 94.11 o 1 -11 1 970.11 1056.68 119.77 o 2 -11 1 244.18 286.05 97.25 o 3 -11 1 209.32 228.00 104.55 o 4 -11 1 389.56 514.23 116.73 o -11 -10 1 2.87 53.57 79.98 o -10 -10 1 222.43 307.57 80.42 o -9 -10 1 1.57 -62.23 62.23 o -8 -10 1 75.51 69.74 66.37 o -7 -10 1 22.26 -12.64 45.73 o -6 -10 1 68.45 84.75 47.56 o -5 -10 1 113.15 30.21 59.92 o -4 -10 1 22.05 76.54 98.32 o -3 -10 1 73.22 106.73 66.84 o -2 -10 1 81.13 138.77 111.93 o -1 -10 1 272.26 355.48 101.91 o 0 -10 1 15.12 187.61 52.29 o 1 -10 1 1023.44 991.40 82.72 o 2 -10 1 97.66 310.99 71.83 o 3 -10 1 284.20 209.16 109.96 o 4 -10 1 35.22 60.53 99.75 o 5 -10 1 337.21 546.18 116.03 o 6 -10 1 125.25 218.56 239.91 o -12 -9 1 228.30 316.96 79.15 o -11 -9 1 76.38 142.42 72.71 o -10 -9 1 596.79 577.09 79.38 o -9 -9 1 194.25 205.83 66.52 o -8 -9 1 589.06 624.55 56.07 o -7 -9 1 678.25 726.87 57.84 o -6 -9 1 451.68 463.93 49.66 o -5 -9 1 1437.03 1580.70 87.90 o -4 -9 1 407.49 476.09 66.23 o -3 -9 1 1387.06 1353.23 86.43 o -2 -9 1 83.90 150.99 59.74 o -1 -9 1 180.45 235.63 49.46 o 0 -9 1 64.34 236.96 49.25 o 1 -9 1 64.38 136.61 65.19 o 2 -9 1 5.77 106.17 58.06 o 3 -9 1 17.61 -56.51 61.33 o 4 -9 1 0.46 4.33 82.65 o 5 -9 1 173.38 -98.45 129.95 o 6 -9 1 2.60 44.44 136.87 o 7 -9 1 55.51 39.46 133.80 o -12 -8 1 456.10 536.56 91.50 o -11 -8 1 155.86 110.80 59.47 o -10 -8 1 874.49 1049.30 82.23 o -9 -8 1 888.86 1088.43 64.33 o -8 -8 1 1931.50 2016.12 84.16 o -7 -8 1 3240.19 3319.76 97.07 o -6 -8 1 1946.16 1923.23 72.10 o -5 -8 1 6854.32 6670.97 184.32 o -4 -8 1 211.91 370.37 54.19 o -3 -8 1 6115.94 5353.42 196.57 o -2 -8 1 123.67 219.11 43.03 o -1 -8 1 5189.02 5200.19 277.03 o 0 -8 1 219.10 336.72 45.17 o 1 -8 1 3112.11 3152.81 115.02 o 2 -8 1 1149.37 1302.33 67.98 o 3 -8 1 329.18 374.70 62.90 o 4 -8 1 340.49 300.29 59.34 o 5 -8 1 0.81 -16.39 70.81 o 6 -8 1 149.90 113.41 64.98 o 7 -8 1 15.34 -14.96 71.60 o 8 -8 1 1.11 -14.12 108.17 o -12 -7 1 705.39 885.57 97.11 o -11 -7 1 252.94 211.56 75.96 o -10 -7 1 1356.92 1449.36 119.87 o -9 -7 1 1647.20 1754.89 63.96 o -8 -7 1 4990.91 4907.14 107.47 o -7 -7 1 3274.82 3227.62 79.90 o -6 -7 1 3188.06 3312.19 90.51 o -5 -7 1 11528.27 11255.52 221.73 o -4 -7 1 651.46 669.95 59.58 o -3 -7 1 17112.94 14982.92 290.94 o -2 -7 1 276.71 243.32 36.89 o -1 -7 1 16237.68 16945.15 350.38 o 0 -7 1 978.46 1093.48 47.18 o 1 -7 1 4871.58 4933.15 166.34 o 2 -7 1 349.65 430.06 43.50 o 3 -7 1 1407.18 1400.63 68.44 o 4 -7 1 1463.18 1598.81 77.62 o 5 -7 1 1068.75 1027.55 74.26 o 6 -7 1 514.87 627.73 68.81 o 7 -7 1 61.83 120.78 75.03 o 8 -7 1 170.38 47.67 72.43 o -12 -6 1 883.47 1018.29 99.29 o -11 -6 1 233.95 296.99 72.47 o -10 -6 1 2107.26 2158.75 71.07 o -9 -6 1 3021.77 3031.54 101.84 o -8 -6 1 2417.38 2498.79 70.08 o -7 -6 1 8426.90 8277.34 152.77 o -6 -6 1 4375.50 4256.00 90.40 o -5 -6 1 14412.19 14371.54 269.87 o -4 -6 1 4679.88 4658.43 105.90 o -3 -6 1 27382.36 26476.11 432.49 o -2 -6 1 200.65 150.05 21.25 o -1 -6 1 29390.97 28599.10 575.79 o 0 -6 1 531.18 602.12 35.45 o 1 -6 1 20292.57 20795.28 450.58 o 2 -6 1 1957.30 1991.57 62.06 o 3 -6 1 8924.28 8396.39 184.65 o 4 -6 1 3297.47 3078.29 101.48 o 5 -6 1 1933.53 1857.27 132.81 o 6 -6 1 814.33 905.54 84.57 o 7 -6 1 337.83 367.63 53.18 o 8 -6 1 818.84 915.89 83.08 o 9 -6 1 0.51 53.65 97.82 o -12 -5 1 563.85 693.39 87.90 o -11 -5 1 252.46 326.39 55.45 o -10 -5 1 1714.48 1822.60 72.89 o -9 -5 1 2018.35 2090.35 81.85 o -8 -5 1 2324.91 2246.40 62.60 o -7 -5 1 6671.62 6660.67 115.85 o -6 -5 1 3255.58 2996.09 62.09 o -5 -5 1 18919.31 18633.71 255.15 o -4 -5 1 4740.31 4758.23 80.82 o -3 -5 1 33428.68 33977.09 615.94 o -2 -5 1 41.43 109.28 18.62 o -1 -5 1 27332.67 25823.18 421.47 o 0 -5 1 1146.96 1267.71 83.55 o 1 -5 1 47541.29 46635.97 1900.48 o 2 -5 1 4198.34 4197.29 89.89 o 3 -5 1 19671.27 18589.64 314.62 o 4 -5 1 6502.37 6321.11 115.71 o 5 -5 1 3343.69 3422.72 94.68 o 6 -5 1 3339.79 3068.83 78.74 o 7 -5 1 1526.46 1566.15 74.46 o 8 -5 1 1928.26 1818.77 95.67 o 9 -5 1 60.02 58.30 66.87 o 10 -5 1 529.04 533.66 169.17 o -12 -4 1 323.46 414.52 79.79 o -11 -4 1 143.54 137.14 48.14 o -10 -4 1 1786.88 1675.34 64.59 o 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