# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ic14316 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 204.33 _exptl_crystal_F_000 868.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.5685 _cell_length_b 12.5224 _cell_length_c 16.3983 _cell_angle_alpha 82.088 _cell_angle_beta 77.476 _cell_angle_gamma 67.212 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 461.38 545.74 19.27 o 2 0 0 6695.12 6718.23 193.47 o 3 0 0 3432.72 3173.10 104.37 o 4 0 0 4321.24 4523.18 168.25 o 5 0 0 12154.45 12155.95 464.13 o 6 0 0 290.80 239.31 34.19 o 7 0 0 2765.43 2503.49 123.44 o 8 0 0 645.62 565.23 61.51 o 9 0 0 1805.10 1746.04 116.81 o 10 0 0 1246.03 1170.07 98.81 o 11 0 0 331.68 460.54 68.46 o 12 0 0 145.02 146.50 75.54 o -12 1 0 426.61 419.16 96.58 o -11 1 0 123.57 229.75 75.30 o -10 1 0 47.57 118.27 44.95 o -9 1 0 11.19 26.99 32.05 o -8 1 0 255.78 287.26 47.24 o -7 1 0 1118.76 1010.03 76.10 o -6 1 0 236.21 220.83 34.99 o -5 1 0 71.72 101.16 17.69 o -4 1 0 727.58 712.07 38.23 o -3 1 0 264.45 349.60 23.67 o -2 1 0 3456.96 3524.33 108.30 o -1 1 0 4181.01 4091.18 120.51 o 1 1 0 10242.04 11977.77 403.27 o 2 1 0 12137.84 13716.39 454.07 o 3 1 0 4796.76 5402.64 191.10 o 4 1 0 1881.00 1867.50 81.09 o 5 1 0 295.08 353.64 62.85 o 6 1 0 11350.46 11790.21 414.92 o 7 1 0 615.80 523.68 54.28 o 8 1 0 1631.86 1604.64 103.98 o 9 1 0 842.74 910.35 82.51 o 10 1 0 49.28 38.90 51.17 o 11 1 0 1354.17 1247.19 108.08 o 12 1 0 2.83 35.46 50.69 o -11 2 0 46.82 53.29 58.35 o -10 2 0 64.00 84.45 128.58 o -9 2 0 50.78 171.73 55.11 o -8 2 0 1325.69 1048.90 100.24 o -7 2 0 2230.12 2184.14 117.56 o -6 2 0 630.61 569.93 41.67 o -5 2 0 0.01 -17.52 11.68 o -4 2 0 2741.55 2799.48 96.92 o -3 2 0 165.49 185.73 19.92 o -2 2 0 3440.87 3399.61 133.74 o -1 2 0 3999.70 3413.13 104.17 o 0 2 0 3045.99 2464.58 75.08 o 1 2 0 207.57 192.90 12.74 o 2 2 0 2097.47 2412.17 76.72 o 3 2 0 4100.34 4873.45 148.34 o 4 2 0 509.45 551.58 62.39 o 5 2 0 715.86 697.39 51.79 o 6 2 0 2178.67 2273.86 103.89 o 7 2 0 1085.81 1230.73 83.42 o 8 2 0 0.87 15.94 32.41 o 9 2 0 14.93 40.99 32.95 o 10 2 0 643.06 646.46 72.91 o 11 2 0 92.06 43.83 42.50 o 12 2 0 209.75 311.19 66.19 o -11 3 0 372.95 478.23 108.84 o -10 3 0 439.92 310.97 76.32 o -9 3 0 528.74 488.00 80.07 o -8 3 0 42.43 47.33 47.79 o -7 3 0 562.47 576.17 58.54 o -6 3 0 824.40 877.15 54.85 o -5 3 0 3133.58 3053.95 109.53 o -4 3 0 912.65 955.28 50.44 o -3 3 0 221.25 282.02 24.97 o -2 3 0 1381.09 1142.12 47.49 o -1 3 0 506.93 451.75 24.22 o 0 3 0 26827.94 26365.61 856.84 o 1 3 0 15956.21 15468.78 442.27 o 2 3 0 2350.11 2220.93 73.26 o 3 3 0 6980.02 7984.01 237.46 o 4 3 0 951.56 1103.90 70.70 o 5 3 0 1004.03 1100.16 66.05 o 6 3 0 47.05 56.47 22.13 o 7 3 0 127.03 177.34 33.56 o 8 3 0 495.72 557.45 59.50 o 9 3 0 169.84 176.96 40.37 o 10 3 0 154.39 146.31 86.83 o 11 3 0 245.66 178.54 50.11 o 12 3 0 10.23 15.86 43.51 o 13 3 0 1297.50 1117.69 127.41 o -10 4 0 1019.27 991.39 124.79 o -9 4 0 60.16 -10.02 43.60 o -8 4 0 1218.64 956.70 124.55 o -7 4 0 1593.72 1231.44 112.98 o -6 4 0 736.92 732.69 52.25 o -5 4 0 3480.95 3200.17 115.62 o -4 4 0 626.88 671.82 62.35 o -3 4 0 3349.64 2904.70 100.37 o -2 4 0 1383.26 1363.82 55.71 o -1 4 0 2670.49 2295.78 107.21 o 0 4 0 5354.05 4737.52 157.25 o 1 4 0 12637.54 12605.05 365.80 o 2 4 0 22225.40 23556.50 670.59 o 3 4 0 164.81 181.49 18.64 o 4 4 0 3.56 3.68 11.88 o 5 4 0 6.29 -1.89 12.13 o 6 4 0 2664.97 2909.30 103.19 o 7 4 0 1254.99 1333.70 87.59 o 8 4 0 97.50 116.02 43.49 o 9 4 0 19.94 69.68 35.00 o 10 4 0 154.20 145.66 43.77 o 11 4 0 803.95 880.74 146.14 o 12 4 0 14.16 17.19 59.51 o 13 4 0 428.83 363.36 96.88 o -10 5 0 483.30 518.29 96.36 o -9 5 0 766.79 714.00 100.29 o -8 5 0 833.00 884.28 103.93 o -7 5 0 3.83 43.52 41.48 o -6 5 0 1074.84 1055.29 90.90 o -5 5 0 0.41 -27.73 23.14 o -4 5 0 7763.51 7231.03 363.37 o -3 5 0 565.44 571.45 37.27 o -2 5 0 1547.72 1433.19 60.58 o -1 5 0 2880.26 2353.44 82.16 o 0 5 0 2775.91 2680.37 89.31 o 1 5 0 28275.96 26566.37 759.55 o 2 5 0 147.78 165.01 21.46 o 3 5 0 4972.36 4989.83 156.91 o 4 5 0 2924.69 3004.25 102.69 o 5 5 0 8619.03 9665.92 292.91 o 6 5 0 8208.18 8465.28 262.65 o 7 5 0 2119.17 2095.29 87.50 o 8 5 0 2240.08 2555.54 134.05 o 9 5 0 942.91 947.88 165.00 o 10 5 0 300.66 267.56 54.89 o 11 5 0 999.00 958.49 96.47 o 12 5 0 278.57 354.16 71.09 o 13 5 0 496.06 467.11 95.59 o -9 6 0 73.25 102.13 61.80 o -8 6 0 111.08 113.66 96.52 o -7 6 0 106.64 108.71 52.16 o -6 6 0 1204.72 1089.01 83.31 o -5 6 0 262.98 223.41 41.33 o -4 6 0 288.18 316.95 48.19 o -3 6 0 568.98 637.84 105.46 o -2 6 0 1027.40 1043.06 52.03 o -1 6 0 921.36 855.27 83.24 o 0 6 0 4080.62 3550.43 137.02 o 1 6 0 715.20 598.70 48.81 o 2 6 0 66.85 34.34 12.84 o 3 6 0 2454.32 2281.54 81.80 o 4 6 0 9.91 -8.94 13.56 o 5 6 0 508.84 588.05 41.52 o 6 6 0 1012.29 1015.06 56.78 o 7 6 0 9284.86 9601.72 297.52 o 8 6 0 94.11 85.16 31.26 o 9 6 0 2273.14 2557.88 142.58 o 10 6 0 135.61 180.43 46.45 o 11 6 0 167.57 159.01 68.36 o 12 6 0 1746.09 1795.02 138.07 o 13 6 0 1.33 125.44 62.12 o -9 7 0 2.04 -0.98 99.28 o -8 7 0 0.33 29.24 54.30 o -7 7 0 522.29 266.44 67.81 o -6 7 0 244.39 290.24 48.40 o -5 7 0 201.06 226.89 41.64 o -4 7 0 69.63 59.01 29.41 o -3 7 0 373.96 377.30 50.93 o -2 7 0 1785.46 1800.10 97.27 o -1 7 0 196.39 181.05 21.28 o 0 7 0 2785.56 2674.86 113.97 o 1 7 0 573.34 629.30 38.02 o 2 7 0 2306.26 2258.71 82.77 o 3 7 0 1518.61 1629.58 66.65 o 4 7 0 43.86 66.03 17.45 o 5 7 0 79.26 69.57 19.18 o 6 7 0 17.43 53.16 19.88 o 7 7 0 1664.34 1953.45 87.72 o 8 7 0 73.84 106.66 33.32 o 9 7 0 844.10 1006.02 124.67 o 10 7 0 1036.96 1075.15 157.08 o 11 7 0 521.74 587.34 87.00 o 12 7 0 608.73 619.09 83.40 o 13 7 0 253.87 178.01 115.35 o -8 8 0 225.50 241.98 131.17 o -7 8 0 132.80 -47.68 45.49 o -6 8 0 412.36 417.82 59.38 o -5 8 0 3.62 -8.20 36.20 o -4 8 0 1819.11 1816.08 112.45 o -3 8 0 318.99 310.65 50.13 o -2 8 0 24.48 22.54 25.18 o -1 8 0 366.15 337.98 40.64 o 0 8 0 296.12 278.88 26.52 o 1 8 0 4242.40 4355.22 145.44 o 2 8 0 680.20 764.33 45.46 o 3 8 0 1761.69 1714.15 75.13 o 4 8 0 53.49 25.56 16.03 o 5 8 0 21.75 14.66 16.79 o 6 8 0 1024.46 1094.87 62.62 o 7 8 0 2061.29 2284.56 98.49 o 8 8 0 42.56 67.96 31.40 o 9 8 0 190.28 163.38 43.05 o 10 8 0 152.33 133.34 66.34 o 11 8 0 64.43 64.04 45.19 o 12 8 0 52.83 53.40 51.11 o 13 8 0 26.99 94.86 70.16 o -7 9 0 1195.63 912.66 119.18 o -6 9 0 952.08 965.39 91.09 o -5 9 0 140.96 186.49 47.52 o -4 9 0 517.78 552.58 63.83 o -3 9 0 520.65 560.03 83.85 o -2 9 0 3932.88 3754.79 163.17 o -1 9 0 400.99 395.35 47.37 o 0 9 0 421.67 453.70 48.17 o 1 9 0 514.90 508.90 41.32 o 2 9 0 1223.39 1312.81 63.42 o 3 9 0 2536.09 2408.61 93.62 o 4 9 0 95.41 127.06 21.29 o 5 9 0 189.93 194.35 30.35 o 6 9 0 0.91 33.59 22.09 o 7 9 0 2235.87 2328.87 101.16 o 8 9 0 1467.95 1599.44 101.92 o 9 9 0 1733.13 1787.61 117.43 o 10 9 0 431.77 327.81 70.10 o 11 9 0 670.24 520.36 91.64 o 12 9 0 353.65 375.28 87.98 o 13 9 0 51.32 39.55 65.29 o -6 10 0 44.11 31.47 162.34 o -5 10 0 1307.47 1574.23 118.30 o -4 10 0 159.81 205.44 48.65 o -3 10 0 1482.69 1582.22 140.67 o -2 10 0 621.90 627.53 73.44 o -1 10 0 428.92 361.95 87.54 o 0 10 0 1848.56 1819.60 105.57 o 1 10 0 171.62 200.54 34.52 o 2 10 0 3041.21 3091.65 115.80 o 3 10 0 178.38 219.38 28.05 o 4 10 0 1394.32 1515.19 74.81 o 5 10 0 1208.29 1200.69 66.01 o 6 10 0 290.32 315.16 54.33 o 7 10 0 1270.90 1459.76 98.94 o 8 10 0 0.85 11.92 41.29 o 9 10 0 3076.30 2959.19 208.99 o 10 10 0 223.71 265.54 66.44 o 11 10 0 870.98 804.83 202.94 o 12 10 0 205.83 277.75 83.76 o -5 11 0 554.63 614.63 77.58 o -4 11 0 59.19 15.44 42.00 o -3 11 0 301.15 322.85 57.36 o -2 11 0 9.75 40.29 33.77 o -1 11 0 256.10 226.35 44.84 o 0 11 0 110.33 110.93 64.82 o 1 11 0 551.86 565.53 57.59 o 2 11 0 1055.05 1121.86 99.70 o 3 11 0 2224.89 2047.28 88.43 o 4 11 0 1460.09 1383.83 93.27 o 5 11 0 139.68 211.35 37.19 o 6 11 0 196.46 135.44 35.16 o 7 11 0 384.98 406.56 54.41 o 8 11 0 3459.62 3185.61 162.44 o 9 11 0 196.45 218.58 60.46 o 10 11 0 379.05 348.14 75.46 o 11 11 0 702.48 618.14 98.78 o 12 11 0 503.10 469.58 88.50 o -4 12 0 53.35 4.38 81.23 o -3 12 0 0.05 -55.00 36.67 o -2 12 0 8.68 21.57 40.47 o -1 12 0 362.32 308.04 53.73 o 0 12 0 2.82 46.06 43.96 o 1 12 0 17.54 72.75 40.81 o 2 12 0 1.31 -56.01 41.01 o 3 12 0 229.58 210.35 82.36 o 4 12 0 76.10 163.55 92.72 o 5 12 0 10.31 27.76 27.78 o 6 12 0 661.15 567.31 62.86 o 7 12 0 711.73 652.16 69.23 o 8 12 0 273.32 267.54 51.91 o 9 12 0 402.54 395.76 72.65 o 10 12 0 0.83 38.22 55.47 o 11 12 0 1113.63 975.08 127.75 o 12 12 0 376.22 399.37 90.64 o -3 13 0 209.96 269.51 73.21 o -2 13 0 27.78 26.74 51.04 o -1 13 0 383.90 453.23 85.90 o 0 13 0 410.59 432.84 104.68 o 1 13 0 368.19 347.86 74.14 o 2 13 0 0.82 58.70 44.02 o 3 13 0 5.78 95.79 48.58 o 4 13 0 62.86 -4.92 39.44 o 5 13 0 87.56 69.88 48.58 o 6 13 0 148.71 153.70 42.08 o 7 13 0 317.81 303.61 52.05 o 8 13 0 304.97 357.27 86.09 o 9 13 0 523.86 507.35 119.37 o 10 13 0 353.83 288.34 73.73 o 11 13 0 58.71 58.21 111.02 o -1 14 0 1228.24 1213.92 313.71 o 0 14 0 49.43 55.79 70.86 o 1 14 0 273.03 259.19 66.02 o 2 14 0 253.51 447.84 83.52 o 3 14 0 759.22 752.30 243.26 o 4 14 0 1000.17 1352.73 139.98 o 5 14 0 0.04 11.66 51.54 o 6 14 0 667.33 687.26 98.35 o 7 14 0 40.09 73.81 54.85 o 8 14 0 750.71 665.65 77.03 o 9 14 0 819.61 881.47 180.62 o 10 14 0 710.78 773.36 111.10 o 1 15 0 603.53 792.29 115.60 o 2 15 0 91.18 157.08 80.48 o 3 15 0 914.70 1200.28 200.32 o 4 15 0 0.06 95.87 69.82 o 5 15 0 1416.11 1382.74 162.09 o 6 15 0 110.28 78.43 60.64 o 7 15 0 172.81 90.18 57.75 o 8 15 0 772.97 612.09 113.47 o 9 15 0 121.15 114.76 143.52 o 4 16 0 383.48 507.39 100.45 o 5 16 0 161.74 185.62 74.07 o 6 16 0 8.52 -42.48 59.16 o -7 -15 1 133.61 226.92 69.92 o -6 -15 1 784.00 744.75 140.70 o -5 -15 1 331.42 427.48 86.10 o -4 -15 1 886.19 1073.95 131.32 o -3 -15 1 1.87 88.75 58.69 o -2 -15 1 778.46 987.24 128.09 o -1 -15 1 20.41 100.20 61.37 o -10 -14 1 462.87 535.30 100.74 o -9 -14 1 916.91 966.48 235.63 o -8 -14 1 90.53 29.72 60.09 o -7 -14 1 865.03 726.99 214.54 o -6 -14 1 15.25 99.09 53.06 o -5 -14 1 1230.86 1124.65 215.23 o -4 -14 1 791.73 780.20 105.98 o -3 -14 1 918.99 1082.02 126.23 o -2 -14 1 605.64 796.65 199.00 o -1 -14 1 621.67 684.99 104.18 o 0 -14 1 1049.45 1107.95 144.56 o 1 -14 1 34.56 8.86 87.43 o -11 -13 1 342.09 369.24 78.52 o -10 -13 1 261.75 270.52 72.04 o -9 -13 1 34.53 27.29 85.77 o -8 -13 1 480.81 506.06 125.93 o -7 -13 1 162.24 157.82 41.84 o -6 -13 1 697.42 601.61 68.52 o -5 -13 1 48.04 118.74 48.25 o -4 -13 1 182.09 205.76 107.96 o -3 -13 1 1219.36 1454.93 210.24 o -2 -13 1 83.35 49.32 124.86 o -1 -13 1 924.35 908.20 113.54 o 0 -13 1 29.42 167.68 51.89 o 1 -13 1 568.22 550.91 93.46 o 2 -13 1 707.41 913.74 122.14 o 3 -13 1 94.64 168.90 53.59 o -11 -12 1 9.27 26.76 63.67 o -10 -12 1 0.49 -46.19 49.35 o -9 -12 1 167.11 103.79 86.57 o -8 -12 1 206.81 126.14 54.35 o -7 -12 1 5.91 58.61 33.59 o -6 -12 1 7.30 73.14 33.52 o -5 -12 1 19.43 16.29 34.20 o -4 -12 1 56.69 114.89 42.45 o -3 -12 1 133.21 77.95 41.27 o -2 -12 1 71.63 127.81 38.73 o -1 -12 1 7.72 60.34 33.26 o 0 -12 1 900.07 941.80 87.86 o 1 -12 1 37.63 -0.38 38.18 o 2 -12 1 44.44 77.76 42.81 o 3 -12 1 12.62 -28.21 45.86 o 4 -12 1 48.88 82.53 47.97 o -12 -11 1 1208.14 1144.74 143.11 o -11 -11 1 579.62 511.37 93.65 o -10 -11 1 517.71 535.63 87.76 o -9 -11 1 644.92 735.83 146.93 o -8 -11 1 242.51 168.36 53.40 o -7 -11 1 2946.23 2840.66 147.24 o -6 -11 1 177.77 161.52 57.55 o -5 -11 1 282.78 346.31 38.03 o -4 -11 1 769.48 752.23 54.04 o -3 -11 1 43.36 27.99 24.09 o -2 -11 1 1276.96 1423.80 114.38 o -1 -11 1 142.78 235.46 52.21 o 0 -11 1 446.47 507.74 137.54 o 1 -11 1 164.37 167.94 41.83 o 2 -11 1 1.62 0.01 38.70 o 3 -11 1 183.83 212.27 50.15 o 4 -11 1 108.34 131.33 45.36 o 5 -11 1 46.74 41.20 61.58 o -12 -10 1 629.55 696.99 110.69 o -11 -10 1 12.18 35.33 51.52 o -10 -10 1 1468.94 1431.57 144.57 o -9 -10 1 0.83 21.32 44.15 o -8 -10 1 4959.79 4522.46 287.81 o -7 -10 1 978.05 974.94 73.21 o -6 -10 1 2321.06 2161.19 97.52 o -5 -10 1 1482.23 1306.12 83.77 o -4 -10 1 827.10 909.74 57.12 o -3 -10 1 2891.68 2762.26 107.78 o -2 -10 1 1780.07 1821.50 81.43 o -1 -10 1 2390.89 2456.06 122.76 o 0 -10 1 47.74 34.27 28.58 o 1 -10 1 3277.87 2853.44 153.97 o 2 -10 1 1818.86 2061.67 212.68 o 3 -10 1 213.56 192.16 55.79 o 4 -10 1 407.00 466.54 63.18 o 5 -10 1 33.64 153.24 98.59 o 6 -10 1 509.01 595.93 95.89 o -12 -9 1 29.46 155.32 65.57 o -11 -9 1 585.24 635.48 100.31 o -10 -9 1 269.09 311.05 73.17 o -9 -9 1 196.29 192.36 90.36 o -8 -9 1 2339.69 2377.47 135.35 o -7 -9 1 1188.15 1231.72 72.89 o -6 -9 1 2974.41 3207.13 122.75 o -5 -9 1 37.83 91.66 23.07 o -4 -9 1 2185.98 2084.82 87.71 o -3 -9 1 4.37 -2.04 16.57 o -2 -9 1 469.35 516.19 71.58 o -1 -9 1 2392.69 2258.53 90.87 o 0 -9 1 2833.47 2470.14 119.70 o 1 -9 1 3958.09 3890.85 181.63 o 2 -9 1 41.93 27.00 35.83 o 3 -9 1 1143.73 1053.23 85.40 o 4 -9 1 31.50 12.04 32.00 o 5 -9 1 936.39 1058.30 92.34 o 6 -9 1 259.93 243.44 56.56 o 7 -9 1 288.19 377.80 81.65 o -13 -8 1 483.20 292.15 162.78 o -12 -8 1 331.63 218.25 66.77 o -11 -8 1 931.82 947.13 167.89 o -10 -8 1 309.12 268.94 58.50 o -9 -8 1 7.76 30.08 34.93 o -8 -8 1 183.26 182.41 41.23 o -7 -8 1 3850.30 3842.32 140.66 o -6 -8 1 1606.11 1884.61 87.34 o -5 -8 1 32.96 31.71 19.20 o -4 -8 1 0.20 27.23 16.62 o -3 -8 1 33.60 52.83 19.44 o -2 -8 1 3943.53 4419.16 148.10 o -1 -8 1 187.21 216.95 24.71 o 0 -8 1 477.18 518.23 48.92 o 1 -8 1 208.49 192.33 32.78 o 2 -8 1 299.22 353.98 59.86 o 3 -8 1 505.59 464.63 54.26 o 4 -8 1 35.59 43.86 35.70 o 5 -8 1 153.45 148.71 42.31 o 6 -8 1 700.64 732.78 145.37 o 7 -8 1 356.65 314.05 146.91 o 8 -8 1 3.11 54.99 58.11 o -13 -7 1 5.50 11.62 57.31 o -12 -7 1 1169.92 1277.25 117.87 o -11 -7 1 4.90 -11.74 41.82 o -10 -7 1 236.83 235.15 52.96 o -9 -7 1 38.14 30.03 34.06 o -8 -7 1 0.69 -35.90 23.94 o -7 -7 1 481.32 540.77 44.93 o 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