Acta Cryst. (2011). E67, m108  [ doi:10.1107/S1600536810052578 ]

Aqua{2-morpholino-N-[1-(2-pyridyl)ethylidene]ethanamine-³N,N',N''}bis(thiocyanato-N)nickel(II)

N. Suleiman Gwaram, N. A. Ikmal Hisham, H. Khaledi and H. Mohd Ali

Online 24 December 2010

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.003 Å
• R factor = 0.025
• wR factor = 0.058
• Data-to-parameter ratio = 14.9

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.12 Ratio
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ni1    --  N5      ..       6.11 su   
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          2      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600          4      

Alert level G
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          4      
PLAT794_ALERT_5_G Note: Tentative Bond Valency for Ni1     .......       2.11      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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