# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' [Cu(bppnOH)(NO3)2] - P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 339.66 _exptl_crystal_F_000 916.00 _reflns_d_resolution_high 0.7497 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.3499 _cell_length_b 14.7703 _cell_length_c 14.5134 _cell_angle_alpha 90.000 _cell_angle_beta 95.055 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5460.16 4559.60 145.98 o 4 0 0 4079.94 4168.62 177.81 o 6 0 0 547.71 546.32 80.45 o 8 0 0 175.27 157.69 46.31 o 10 0 0 222.16 120.55 72.05 o 1 1 0 2123.43 2610.62 40.47 o 2 1 0 4373.99 4139.38 98.32 o 3 1 0 2996.22 3108.17 95.48 o 4 1 0 1865.20 1904.95 82.60 o 5 1 0 392.18 340.70 48.78 o 6 1 0 1639.89 1728.71 96.91 o 7 1 0 1008.06 924.52 80.49 o 8 1 0 38.27 -18.54 37.80 o 9 1 0 16.34 6.64 26.82 o 10 1 0 110.75 118.20 60.82 o 0 2 0 6132.67 6687.99 121.34 o 1 2 0 5418.66 6150.30 80.01 o 2 2 0 1243.59 1474.19 34.06 o 3 2 0 23.27 19.49 9.12 o 4 2 0 5037.35 4878.56 143.22 o 5 2 0 1651.89 1439.03 114.52 o 6 2 0 439.41 473.23 37.30 o 7 2 0 13.36 15.45 16.72 o 8 2 0 19.70 -6.08 22.83 o 9 2 0 772.10 828.89 55.69 o 10 2 0 48.86 51.33 49.94 o 11 2 0 16.07 -13.49 67.20 o 1 3 0 1900.56 1919.56 37.31 o 2 3 0 105.90 79.63 10.19 o 3 3 0 1853.40 1699.44 41.19 o 4 3 0 16.99 14.72 9.68 o 5 3 0 684.22 723.37 38.77 o 6 3 0 8.72 -0.74 11.70 o 7 3 0 2458.18 2367.99 74.17 o 8 3 0 23.38 12.90 22.91 o 9 3 0 15.19 68.59 32.86 o 10 3 0 21.20 63.63 50.77 o 0 4 0 338.98 561.94 134.51 o 1 4 0 482.93 509.08 31.26 o 2 4 0 263.60 344.14 27.80 o 3 4 0 100.54 114.90 23.44 o 4 4 0 1849.73 1712.12 53.39 o 5 4 0 2495.33 2335.16 61.53 o 6 4 0 266.67 317.38 29.72 o 7 4 0 74.37 83.36 24.85 o 8 4 0 31.96 30.35 24.35 o 9 4 0 359.46 319.68 66.09 o 10 4 0 47.93 62.82 52.06 o 1 5 0 151.61 125.51 21.35 o 2 5 0 3328.80 3345.55 90.76 o 3 5 0 257.84 286.55 34.40 o 4 5 0 701.57 645.55 32.75 o 5 5 0 187.69 199.21 25.08 o 6 5 0 1655.25 1564.08 83.18 o 7 5 0 67.48 49.38 27.46 o 8 5 0 348.83 571.17 141.54 o 9 5 0 3.96 2.52 39.65 o 10 5 0 117.25 50.60 78.97 o 0 6 0 6453.70 5328.17 150.20 o 1 6 0 85.20 38.93 16.18 o 2 6 0 1086.25 1174.53 60.04 o 3 6 0 135.38 152.56 26.56 o 4 6 0 2302.70 2166.26 89.08 o 5 6 0 1468.09 1337.15 77.68 o 6 6 0 75.27 54.67 25.40 o 7 6 0 24.66 16.13 25.59 o 8 6 0 24.92 -0.82 30.03 o 9 6 0 14.86 35.10 46.61 o 10 6 0 6.96 -49.92 73.11 o 1 7 0 8478.43 8227.13 176.34 o 2 7 0 6662.65 6459.42 155.79 o 3 7 0 3333.21 2975.88 100.40 o 4 7 0 317.84 312.97 41.70 o 5 7 0 1671.65 1535.61 79.61 o 6 7 0 93.11 106.46 30.64 o 7 7 0 1524.15 1703.98 96.23 o 8 7 0 249.47 177.68 47.32 o 9 7 0 7.31 18.24 45.55 o 10 7 0 114.33 208.92 82.69 o 0 8 0 7.40 0.40 20.88 o 1 8 0 206.86 200.04 35.42 o 2 8 0 15.74 25.67 18.91 o 3 8 0 4803.83 4502.11 133.68 o 4 8 0 4.27 -6.67 16.05 o 5 8 0 2877.15 2824.54 113.19 o 6 8 0 263.05 210.82 43.75 o 7 8 0 43.53 60.56 33.14 o 8 8 0 21.99 7.63 33.37 o 9 8 0 420.43 694.97 101.74 o 10 8 0 0.04 -73.58 73.58 o 1 9 0 2077.68 2154.51 93.08 o 2 9 0 1940.19 1901.46 87.26 o 3 9 0 1273.74 1298.66 74.88 o 4 9 0 82.18 82.98 30.81 o 5 9 0 437.38 477.75 59.82 o 6 9 0 4.17 37.79 29.73 o 7 9 0 282.06 237.21 50.47 o 8 9 0 10.60 4.64 35.42 o 9 9 0 1.24 63.04 55.13 o 0 10 0 1134.73 1281.92 140.31 o 1 10 0 789.61 845.64 125.79 o 2 10 0 329.53 264.57 43.16 o 3 10 0 19.41 10.22 23.91 o 4 10 0 2618.01 2663.15 237.84 o 5 10 0 779.80 779.10 79.01 o 6 10 0 1403.58 1551.37 96.34 o 7 10 0 44.00 -19.95 32.70 o 8 10 0 214.28 134.86 68.20 o 9 10 0 272.62 231.29 70.78 o 1 11 0 0.23 -3.29 23.01 o 2 11 0 1030.38 1055.98 76.00 o 3 11 0 49.01 45.94 26.27 o 4 11 0 442.68 515.92 65.66 o 5 11 0 82.40 108.01 38.43 o 6 11 0 136.70 123.74 42.01 o 7 11 0 0.24 36.35 36.40 o 8 11 0 73.54 83.94 48.77 o 9 11 0 0.07 -41.92 54.01 o 0 12 0 1187.15 1349.36 161.60 o 1 12 0 618.05 665.24 71.26 o 2 12 0 1.01 -4.82 26.50 o 3 12 0 233.97 244.38 47.24 o 4 12 0 731.38 707.65 88.25 o 5 12 0 471.07 513.51 69.09 o 6 12 0 56.81 3.09 32.59 o 7 12 0 4.27 6.92 36.53 o 8 12 0 53.46 101.48 115.70 o 1 13 0 150.60 130.29 86.95 o 2 13 0 17.03 12.55 28.02 o 3 13 0 559.59 586.47 74.42 o 4 13 0 1.50 -26.38 26.38 o 5 13 0 89.82 76.55 39.53 o 6 13 0 77.92 101.58 44.54 o 7 13 0 18.18 18.22 41.16 o 8 13 0 3.05 -49.99 61.04 o 0 14 0 255.65 176.63 89.55 o 1 14 0 902.91 1029.83 108.52 o 2 14 0 1108.27 1181.07 93.55 o 3 14 0 494.45 485.57 73.09 o 4 14 0 70.65 30.35 47.59 o 5 14 0 1064.28 1056.56 94.17 o 6 14 0 9.22 29.07 42.75 o 7 14 0 1.70 34.37 42.26 o 1 15 0 89.69 76.88 54.53 o 2 15 0 1486.30 1410.31 105.77 o 3 15 0 37.21 29.30 37.65 o 4 15 0 145.30 162.19 50.61 o 5 15 0 0.12 42.78 42.67 o 6 15 0 49.67 113.22 49.61 o 7 15 0 15.66 35.73 49.22 o 0 16 0 1255.71 1398.33 202.06 o 1 16 0 12.73 -16.95 47.17 o 2 16 0 7.91 -36.75 48.29 o 3 16 0 30.18 22.26 46.08 o 4 16 0 383.16 115.10 96.14 o 5 16 0 76.37 27.00 44.75 o 6 16 0 136.72 80.43 51.25 o 1 17 0 39.50 33.39 64.49 o 2 17 0 863.31 301.58 380.58 o 3 17 0 44.61 20.24 32.71 o 4 17 0 77.03 23.54 40.12 o 5 17 0 6.78 4.09 44.43 o 0 18 0 106.42 63.17 108.01 o 1 18 0 76.17 153.57 90.74 o 2 18 0 17.01 22.93 58.07 o 3 18 0 208.75 67.86 208.03 o 4 18 0 125.43 23.98 103.02 o 1 19 0 24.08 -7.12 107.18 o 2 19 0 6.80 2.65 62.37 o -9 0 1 797.71 765.42 143.74 o -7 0 1 540.24 487.88 98.90 o -5 0 1 534.48 461.02 68.97 o -3 0 1 2010.74 1594.48 98.19 o -1 0 1 63.31 187.29 22.00 o 1 0 1 23945.27 25667.34 371.88 o 3 0 1 1560.94 1430.87 80.80 o 5 0 1 11780.69 11517.43 355.97 o 7 0 1 1367.50 1390.24 92.73 o 9 0 1 120.25 181.83 67.31 o 11 0 1 23.24 89.08 88.25 o -10 1 1 99.87 76.16 128.12 o -9 1 1 237.98 174.57 54.23 o -8 1 1 270.87 344.82 52.45 o -7 1 1 185.01 209.13 48.54 o -6 1 1 908.06 986.61 107.54 o -5 1 1 1486.88 1565.40 86.80 o -4 1 1 1495.14 1346.71 84.29 o -3 1 1 5899.01 5654.05 200.11 o -2 1 1 1968.90 2441.15 58.54 o -1 1 1 12685.04 14648.37 141.70 o 0 1 1 4843.67 5758.45 60.62 o 1 1 1 78.68 90.91 10.41 o 2 1 1 1176.13 805.09 30.46 o 3 1 1 1720.17 1655.92 51.81 o 4 1 1 1677.39 1461.52 56.16 o 5 1 1 159.10 123.14 25.09 o 6 1 1 717.65 748.75 50.48 o 7 1 1 737.89 779.58 57.31 o 8 1 1 29.30 26.67 19.16 o 9 1 1 6.20 91.21 41.24 o 10 1 1 32.19 -34.47 40.38 o 11 1 1 84.13 -81.98 84.94 o -10 2 1 10.12 82.81 72.40 o -9 2 1 225.64 282.74 45.29 o -8 2 1 639.53 688.66 50.14 o -7 2 1 85.09 113.06 39.39 o -6 2 1 174.93 191.00 35.76 o -5 2 1 20.69 9.03 17.47 o -4 2 1 1759.78 1694.14 65.38 o -3 2 1 28.33 24.02 12.75 o -2 2 1 1693.49 1950.66 45.61 o -1 2 1 16.34 27.46 6.82 o 0 2 1 10344.54 11203.08 113.61 o 1 2 1 5628.12 6236.42 82.35 o 2 2 1 4018.40 4218.49 69.44 o 3 2 1 273.32 303.29 31.97 o 4 2 1 1328.98 1321.78 44.25 o 5 2 1 3357.71 3380.03 80.86 o 6 2 1 1927.53 1979.40 66.63 o 7 2 1 558.22 607.80 42.17 o 8 2 1 0.95 -15.44 15.44 o 9 2 1 37.06 15.45 39.30 o 10 2 1 422.71 368.71 77.78 o -10 3 1 339.64 432.75 112.86 o -9 3 1 75.19 143.82 36.10 o -8 3 1 27.93 40.10 25.25 o -7 3 1 531.89 580.30 39.73 o -6 3 1 2104.85 2067.05 74.24 o -5 3 1 351.88 432.24 34.19 o -4 3 1 1219.53 1371.01 50.16 o -3 3 1 32.38 30.34 11.11 o -2 3 1 10120.17 9836.84 175.81 o -1 3 1 11723.67 12722.68 185.54 o 0 3 1 28450.22 28518.32 301.24 o 1 3 1 5803.19 6743.49 101.61 o 2 3 1 1267.51 1167.95 33.92 o 3 3 1 78.43 105.39 15.15 o 4 3 1 401.64 319.63 22.04 o 5 3 1 644.82 720.76 34.48 o 6 3 1 176.65 219.77 25.38 o 7 3 1 221.47 264.13 30.68 o 8 3 1 570.61 709.86 52.70 o 9 3 1 6.12 -7.45 38.23 o 10 3 1 31.60 92.90 54.02 o -10 4 1 14.43 43.89 69.21 o -9 4 1 220.63 245.92 42.90 o -8 4 1 787.52 780.39 88.96 o -7 4 1 557.33 562.27 51.78 o -6 4 1 47.78 25.15 15.24 o -5 4 1 342.89 374.49 27.58 o -4 4 1 5641.97 5428.28 91.10 o -3 4 1 255.64 233.37 17.89 o -2 4 1 888.36 768.79 40.07 o -1 4 1 28.49 31.24 8.16 o 0 4 1 191.15 242.23 20.37 o 1 4 1 1149.36 1028.82 32.55 o 2 4 1 3106.77 2838.37 58.05 o 3 4 1 2611.78 2707.22 62.56 o 4 4 1 2156.34 2142.65 61.46 o 5 4 1 2631.99 2586.48 74.39 o 6 4 1 2157.50 2177.48 74.85 o 7 4 1 576.97 556.70 57.72 o 8 4 1 68.35 48.38 31.41 o 9 4 1 120.17 134.74 52.33 o 10 4 1 252.88 354.05 77.85 o -10 5 1 17.02 14.55 59.74 o -9 5 1 148.85 172.39 48.34 o -8 5 1 42.10 39.06 29.87 o -7 5 1 439.81 395.34 52.74 o -6 5 1 0.40 -15.12 18.81 o -5 5 1 2457.66 2444.73 95.06 o -4 5 1 1590.27 1663.28 48.93 o -3 5 1 74.37 104.16 30.63 o -2 5 1 2168.04 2085.12 71.73 o -1 5 1 4105.61 4028.44 99.50 o 0 5 1 3369.50 3101.85 169.64 o 1 5 1 25.69 32.69 10.29 o 2 5 1 1260.85 1201.05 37.63 o 3 5 1 2813.07 2626.81 69.56 o 4 5 1 143.28 132.12 19.37 o 5 5 1 1837.55 1937.12 64.65 o 6 5 1 107.50 159.64 33.33 o 7 5 1 118.27 109.31 35.30 o 8 5 1 59.24 25.97 32.39 o 9 5 1 239.03 340.05 86.66 o 10 5 1 2.70 -9.30 43.54 o -10 6 1 0.92 45.66 79.03 o -9 6 1 264.00 233.12 56.73 o -8 6 1 3.84 10.29 30.59 o -7 6 1 314.36 422.83 58.33 o -6 6 1 0.34 17.31 22.58 o -5 6 1 689.04 629.99 51.89 o -4 6 1 665.44 544.82 44.57 o -3 6 1 3436.44 3279.42 101.94 o -2 6 1 618.42 594.51 41.64 o -1 6 1 26.85 69.11 19.74 o 0 6 1 5820.43 5908.44 132.48 o 1 6 1 16357.56 17205.25 220.35 o 2 6 1 346.01 344.07 33.55 o 3 6 1 316.19 321.13 23.97 o 4 6 1 203.26 191.61 22.33 o 5 6 1 4311.88 4124.52 127.64 o 6 6 1 7.01 23.15 21.79 o 7 6 1 179.28 223.48 42.81 o 8 6 1 22.32 15.85 30.63 o 9 6 1 95.62 57.91 45.79 o 10 6 1 48.73 89.85 58.14 o -10 7 1 145.94 185.14 105.17 o -9 7 1 92.76 113.38 46.81 o -8 7 1 1.06 -30.82 30.82 o -7 7 1 11.72 19.22 27.10 o -6 7 1 1090.72 1136.14 75.18 o -5 7 1 1827.46 1844.15 148.52 o -4 7 1 1554.09 1484.79 120.09 o -3 7 1 32.83 20.43 19.64 o -2 7 1 1482.64 1487.55 69.49 o -1 7 1 7906.58 7584.72 218.33 o 0 7 1 481.16 605.55 61.50 o 1 7 1 283.52 243.53 38.80 o 2 7 1 5686.62 5455.54 101.72 o 3 7 1 292.88 255.89 21.00 o 4 7 1 2312.47 2192.11 89.18 o 5 7 1 1002.53 984.88 65.59 o 6 7 1 10.88 48.12 27.77 o 7 7 1 29.83 41.08 28.12 o 8 7 1 128.53 132.02 52.15 o 9 7 1 292.50 509.05 129.19 o 10 7 1 24.54 26.26 49.47 o -10 8 1 52.45 66.84 82.57 o -9 8 1 0.01 32.22 42.72 o -8 8 1 354.28 407.87 62.86 o -7 8 1 147.08 167.96 43.59 o -6 8 1 39.90 50.21 28.39 o -5 8 1 395.93 458.35 63.17 o -4 8 1 3731.28 3424.51 120.54 o -3 8 1 749.99 710.47 72.26 o -2 8 1 241.39 225.29 35.39 o -1 8 1 87.09 64.67 24.58 o 0 8 1 4883.49 4813.38 133.42 o 1 8 1 2.34 -16.76 16.76 o 2 8 1 4170.73 4076.07 141.08 o 3 8 1 320.66 333.92 43.73 o 4 8 1 946.26 1023.93 85.16 o 5 8 1 163.51 185.28 38.25 o 6 8 1 770.89 839.54 67.77 o 7 8 1 164.32 146.38 41.40 o 8 8 1 182.18 51.97 44.50 o 9 8 1 3.62 26.03 64.36 o 10 8 1 133.33 28.69 54.55 o -9 9 1 2.05 -48.77 48.77 o -8 9 1 0.08 -16.15 34.40 o -7 9 1 277.76 279.27 54.26 o -6 9 1 524.38 550.22 67.80 o -5 9 1 354.00 490.44 82.81 o -4 9 1 26.68 23.65 20.35 o -3 9 1 23.49 34.66 20.52 o -2 9 1 1647.01 1652.06 83.03 o -1 9 1 46.33 22.68 20.08 o 0 9 1 1600.87 1494.67 77.45 o 1 9 1 220.60 285.26 42.47 o 2 9 1 506.06 460.23 49.30 o 3 9 1 848.79 859.02 91.94 o 4 9 1 718.38 662.09 57.92 o 5 9 1 41.30 48.87 26.47 o 6 9 1 301.24 345.14 54.27 o 7 9 1 52.51 74.61 35.95 o 8 9 1 361.09 515.92 154.86 o 9 9 1 28.37 99.97 67.08 o -9 10 1 57.05 30.31 52.15 o -8 10 1 2.20 22.74 38.59 o -7 10 1 170.17 220.92 51.69 o -6 10 1 13.48 -25.37 25.37 o -5 10 1 487.30 497.07 63.63 o -4 10 1 1448.33 1553.70 89.36 o -3 10 1 2469.02 2132.54 101.01 o -2 10 1 46.27 62.11 25.81 o -1 10 1 147.47 215.62 45.19 o 0 10 1 312.77 293.91 45.97 o 1 10 1 4407.46 4139.59 175.88 o 2 10 1 505.61 495.58 56.64 o 3 10 1 569.48 686.86 71.05 o 4 10 1 6.85 15.02 24.63 o 5 10 1 402.12 311.31 51.45 o 6 10 1 26.02 63.56 33.42 o 7 10 1 346.96 491.13 70.06 o 8 10 1 4.43 52.82 49.66 o 9 10 1 67.24 21.77 89.08 o -9 11 1 88.60 129.79 73.42 o -8 11 1 3.37 -7.34 47.01 o -7 11 1 141.70 221.06 55.24 o -6 11 1 75.59 102.50 38.18 o -5 11 1 1784.29 1852.98 132.28 o -4 11 1 50.92 44.39 29.76 o -3 11 1 280.22 335.55 51.97 o -2 11 1 66.39 0.09 28.38 o -1 11 1 591.50 724.81 66.57 o 0 11 1 11.14 0.62 27.55 o 1 11 1 490.00 470.83 60.25 o 2 11 1 415.74 376.86 56.02 o 3 11 1 2174.67 2278.64 109.55 o 4 11 1 44.20 97.53 33.62 o 5 11 1 159.48 165.25 45.36 o 6 11 1 14.95 25.56 32.73 o 7 11 1 222.39 276.90 57.64 o 8 11 1 92.56 87.23 51.01 o 9 11 1 179.09 164.91 106.35 o -8 12 1 123.73 113.41 51.57 o -7 12 1 22.18 29.41 39.69 o -6 12 1 4.57 4.61 33.52 o -5 12 1 68.94 134.98 42.33 o -4 12 1 691.25 733.90 81.77 o -3 12 1 505.73 506.74 66.90 o -2 12 1 15.49 26.93 28.89 o -1 12 1 11.18 -31.27 31.27 o 0 12 1 3.69 18.49 43.25 o 1 12 1 1281.37 1418.37 90.91 o 2 12 1 1921.52 1911.37 154.64 o 3 12 1 149.61 150.92 41.93 o 4 12 1 248.13 266.43 52.76 o 5 12 1 7.91 -26.57 26.57 o 6 12 1 300.82 301.36 56.22 o 7 12 1 37.50 75.53 56.92 o 8 12 1 24.33 18.36 74.06 o -8 13 1 21.34 24.59 51.54 o -7 13 1 70.82 -7.73 37.49 o -6 13 1 572.78 529.51 76.71 o -5 13 1 1.13 -19.26 32.56 o -4 13 1 431.24 374.36 62.81 o -3 13 1 68.09 50.48 35.77 o -2 13 1 464.32 520.29 69.89 o -1 13 1 14.44 64.50 44.62 o 0 13 1 756.83 861.66 105.93 o 1 13 1 11.32 31.06 32.25 o 2 13 1 485.71 678.94 79.96 o 3 13 1 45.08 60.46 53.29 o 4 13 1 702.10 708.09 84.04 o 5 13 1 25.62 7.28 33.43 o 6 13 1 105.43 107.67 47.76 o 7 13 1 50.60 -8.31 36.09 o 8 13 1 296.59 75.10 59.62 o -7 14 1 112.10 53.27 46.38 o -6 14 1 8.49 -37.05 48.47 o -5 14 1 7.90 15.87 39.34 o -4 14 1 769.44 827.08 93.23 o -3 14 1 187.15 181.93 50.34 o -2 14 1 1087.57 1178.36 92.85 o -1 14 1 266.84 312.66 79.59 o 0 14 1 3083.76 2857.75 177.58 o 1 14 1 359.10 371.22 65.47 o 2 14 1 756.64 903.39 102.33 o 3 14 1 147.49 112.49 41.50 o 4 14 1 2.81 -2.37 35.31 o 5 14 1 74.20 72.73 43.70 o 6 14 1 483.87 339.54 181.19 o 7 14 1 4.13 30.80 48.58 o -7 15 1 25.41 44.47 51.25 o -6 15 1 250.93 37.89 79.25 o -5 15 1 375.71 244.77 71.22 o -4 15 1 62.43 42.61 45.47 o -3 15 1 74.01 86.79 41.84 o -2 15 1 6.15 -16.08 38.25 o -1 15 1 1344.76 1461.55 183.66 o 0 15 1 32.08 47.16 49.50 o 1 15 1 1.37 40.85 47.29 o 2 15 1 102.28 71.81 45.73 o 3 15 1 691.50 515.21 79.13 o 4 15 1 399.31 354.77 67.53 o 5 15 1 23.99 24.87 40.65 o 6 15 1 59.02 0.99 38.92 o 7 15 1 103.32 72.82 86.12 o -6 16 1 29.76 19.05 42.43 o -5 16 1 192.13 18.02 60.63 o -4 16 1 42.16 -9.75 38.57 o -3 16 1 589.03 596.17 87.66 o -2 16 1 0.83 -35.17 58.56 o -1 16 1 391.08 515.48 104.02 o 0 16 1 199.86 172.84 97.07 o 1 16 1 746.26 813.28 123.94 o 2 16 1 1.23 11.97 46.99 o 3 16 1 1.97 -6.02 44.87 o 4 16 1 0.25 2.13 36.22 o 5 16 1 404.01 87.09 141.52 o 6 16 1 17.59 1.29 49.51 o -5 17 1 259.58 5.92 56.24 o -4 17 1 3.53 -10.63 37.89 o -3 17 1 18.70 68.35 68.32 o -2 17 1 148.78 15.09 103.34 o -1 17 1 68.31 117.81 74.44 o 0 17 1 58.43 74.35 100.32 o 1 17 1 67.39 51.71 57.59 o 2 17 1 4.35 3.99 52.71 o 3 17 1 522.73 553.37 112.53 o 4 17 1 5.30 39.99 43.05 o 5 17 1 141.76 89.85 48.26 o -4 18 1 126.10 51.82 46.49 o -3 18 1 40.76 96.85 59.27 o -2 18 1 148.83 138.37 92.39 o -1 18 1 44.09 110.15 110.67 o 0 18 1 26.77 32.50 73.77 o 1 18 1 113.68 29.32 146.16 o 2 18 1 144.85 0.98 96.77 o 3 18 1 2.69 4.16 51.99 o 4 18 1 60.08 12.02 47.43 o -2 19 1 38.53 48.77 85.77 o -1 19 1 12.74 -64.80 64.80 o 0 19 1 25.60 -71.30 71.30 o 1 19 1 1.74 11.71 56.97 o 2 19 1 62.70 -47.04 116.23 o -10 0 2 392.65 389.21 123.03 o -8 0 2 27.91 78.43 59.27 o -6 0 2 577.14 659.30 93.58 o -4 0 2 4824.39 4642.65 207.62 o -2 0 2 115366.61 114720.98 3464.60 o 0 0 2 1488.76 1705.13 43.64 o 2 0 2 3819.25 3820.74 85.70 o 4 0 2 503.38 523.80 42.48 o 6 0 2 2082.43 2081.71 101.74 o 8 0 2 463.51 558.86 112.27 o -10 1 2 166.61 212.26 55.34 o -9 1 2 425.68 487.08 67.12 o -8 1 2 857.93 904.88 71.83 o -7 1 2 1.87 5.01 21.92 o -6 1 2 1019.61 1094.42 83.43 o -5 1 2 528.31 531.16 55.80 o -4 1 2 10204.88 10553.43 243.43 o -3 1 2 5978.13 6072.12 118.76 o -2 1 2 267.38 310.55 16.94 o -1 1 2 2467.05 2655.09 42.58 o 0 1 2 28982.76 30120.14 269.93 o 1 1 2 14.35 27.99 5.97 o 2 1 2 366.97 394.47 18.56 o 3 1 2 203.67 233.25 16.27 o 4 1 2 6047.93 5975.62 91.42 o 5 1 2 983.64 982.55 56.22 o 6 1 2 219.05 205.79 23.78 o 7 1 2 16.27 8.63 15.07 o 8 1 2 19.34 -8.47 27.38 o 9 1 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