# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' iak75 in P-1 (100K)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 319.79 _exptl_crystal_F_000 1472.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.8435 _cell_length_b 12.6134 _cell_length_c 22.4695 _cell_angle_alpha 81.029 _cell_angle_beta 82.769 _cell_angle_gamma 79.265 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 31.82 50.68 14.25 o 3 0 0 3843.89 4191.06 99.25 o 4 0 0 6210.09 6803.43 142.36 o 5 0 0 6434.96 6410.21 173.91 o 6 0 0 786.64 785.29 47.43 o 7 0 0 1013.44 1136.87 61.08 o 8 0 0 1060.24 1085.23 80.08 o 9 0 0 1018.34 988.14 133.60 o 10 0 0 218.15 199.25 61.10 o 11 0 0 53.13 71.93 74.22 o 12 0 0 59.47 38.91 45.44 o 13 0 0 1113.86 1254.91 111.63 o -13 1 0 2267.63 2602.61 234.47 o -12 1 0 108.72 88.19 90.86 o -11 1 0 1362.66 1616.89 122.04 o -10 1 0 2757.46 2775.34 134.59 o -9 1 0 438.05 493.14 55.01 o -8 1 0 237.23 319.30 42.62 o -7 1 0 2712.56 2646.85 88.67 o -6 1 0 5.84 7.78 19.76 o -5 1 0 395.59 368.56 58.97 o -4 1 0 8897.91 9300.34 318.35 o -3 1 0 35.28 57.50 18.60 o -2 1 0 30273.30 32656.52 992.73 o 1 1 0 62992.70 73305.45 2002.88 o 2 1 0 2145.60 2609.49 45.88 o 3 1 0 4876.17 5332.56 106.76 o 4 1 0 2114.39 2387.85 59.07 o 5 1 0 19658.23 19747.93 382.69 o 6 1 0 17758.85 17520.37 305.11 o 7 1 0 2530.69 2577.85 61.30 o 8 1 0 183.42 239.09 24.38 o 9 1 0 189.81 191.18 33.25 o 10 1 0 3736.05 3766.60 111.24 o 11 1 0 1751.77 1638.12 124.46 o 12 1 0 40.35 -2.40 49.92 o 13 1 0 181.17 241.11 60.49 o -13 2 0 608.58 576.43 144.88 o -12 2 0 149.81 74.70 90.01 o -11 2 0 878.98 654.28 126.66 o -10 2 0 984.22 1159.15 84.45 o -9 2 0 3186.15 3310.27 117.94 o -8 2 0 1324.04 1441.77 77.15 o -7 2 0 1121.33 1399.86 89.53 o -6 2 0 376.09 426.97 58.95 o -5 2 0 7163.42 4688.31 190.82 o -4 2 0 139.51 267.26 46.11 o -3 2 0 996.81 1307.10 84.81 o -2 2 0 3485.37 3593.60 100.81 o -1 2 0 23.82 4.13 5.40 o 0 2 0 1652.25 1812.67 47.46 o 1 2 0 26999.32 28540.42 420.31 o 2 2 0 64.80 149.11 12.93 o 3 2 0 10091.38 10221.13 289.01 o 4 2 0 2173.70 2193.21 77.19 o 5 2 0 4623.09 4525.60 104.64 o 6 2 0 22690.30 22602.65 608.30 o 7 2 0 9898.62 9917.07 174.08 o 8 2 0 61.01 49.24 30.78 o 9 2 0 10.70 -20.38 28.57 o 10 2 0 1002.22 1244.61 71.00 o 11 2 0 1660.95 1799.95 90.69 o 12 2 0 972.53 899.96 72.67 o 13 2 0 263.44 198.29 55.25 o -12 3 0 3.17 99.58 103.48 o -11 3 0 621.61 431.10 122.58 o -10 3 0 540.21 542.25 62.85 o -9 3 0 1555.73 1791.93 92.38 o -8 3 0 973.57 1105.06 98.20 o -7 3 0 2285.24 2211.96 104.87 o -6 3 0 1206.26 1241.05 76.44 o -5 3 0 3881.70 3989.81 129.98 o -4 3 0 21068.06 20371.81 684.57 o -3 3 0 16590.64 16665.02 294.25 o -2 3 0 13468.44 13911.51 456.33 o -1 3 0 8479.07 8427.85 191.28 o 0 3 0 5724.86 6069.38 78.75 o 1 3 0 778.81 598.19 28.26 o 2 3 0 32.22 11.36 9.97 o 3 3 0 3415.63 3878.62 71.87 o 4 3 0 21759.75 22691.66 495.90 o 5 3 0 7509.55 7639.82 155.11 o 6 3 0 6778.26 6950.70 194.04 o 7 3 0 6831.67 7073.84 203.95 o 8 3 0 3294.98 3607.10 136.07 o 9 3 0 50.78 7.95 30.12 o 10 3 0 8.51 30.07 35.99 o 11 3 0 594.72 587.25 61.86 o 12 3 0 738.88 660.99 68.52 o 13 3 0 309.03 282.06 61.33 o -9 4 0 416.32 448.52 69.09 o -8 4 0 6773.80 6751.49 339.83 o -7 4 0 247.74 266.34 50.52 o -6 4 0 1850.62 1835.86 123.31 o -5 4 0 4.47 19.53 34.04 o -4 4 0 16430.88 15559.87 428.19 o -3 4 0 32939.78 32677.70 972.10 o -2 4 0 15967.06 16482.14 384.76 o -1 4 0 3243.26 3192.64 65.95 o 0 4 0 4641.10 5153.29 71.01 o 1 4 0 23709.40 24179.90 360.49 o 2 4 0 22416.62 22862.24 311.13 o 3 4 0 7677.00 7799.31 124.48 o 4 4 0 12126.79 12435.93 180.79 o 5 4 0 2977.12 2852.13 50.47 o 6 4 0 1229.39 1065.62 65.18 o 7 4 0 13.86 15.48 67.04 o 8 4 0 1436.39 1424.18 91.33 o 9 4 0 651.79 667.11 55.34 o 10 4 0 885.88 983.00 69.32 o 11 4 0 1165.58 1135.97 78.57 o 12 4 0 93.27 59.62 81.40 o 13 4 0 311.68 210.61 74.00 o -8 5 0 2683.28 2481.39 169.99 o -7 5 0 3207.47 3235.34 182.24 o -6 5 0 20.91 35.35 17.98 o -5 5 0 1937.77 2087.13 61.33 o -4 5 0 1229.66 1277.29 67.00 o -3 5 0 7350.62 6517.84 169.52 o -2 5 0 10167.13 9845.55 230.89 o -1 5 0 104.02 127.30 15.86 o 0 5 0 331.31 352.72 21.73 o 1 5 0 3950.18 3687.45 72.51 o 2 5 0 41411.49 40866.07 556.67 o 3 5 0 21567.48 21892.27 296.70 o 4 5 0 6356.51 6635.96 99.02 o 5 5 0 5240.82 5505.85 96.10 o 6 5 0 1182.22 1295.27 33.83 o 7 5 0 19577.05 19251.29 400.19 o 8 5 0 6342.05 6155.08 156.36 o 9 5 0 6891.75 6806.61 173.55 o 10 5 0 4566.51 4662.02 166.80 o 11 5 0 131.15 144.65 48.43 o 12 5 0 2878.87 2873.95 121.87 o 13 5 0 56.10 73.54 73.49 o -8 6 0 1356.35 1403.63 74.91 o -7 6 0 1380.92 1387.25 106.08 o -6 6 0 2275.55 2185.11 120.46 o -5 6 0 228.19 186.27 33.89 o -4 6 0 805.26 801.20 50.85 o -3 6 0 69.48 60.63 30.21 o -2 6 0 5418.32 5174.03 86.80 o -1 6 0 127.77 127.76 17.44 o 0 6 0 361.58 310.56 24.72 o 1 6 0 371.85 342.28 18.16 o 2 6 0 8191.18 7842.18 105.88 o 3 6 0 36379.30 36014.59 439.80 o 4 6 0 2770.21 2459.61 49.85 o 5 6 0 2801.85 2866.94 69.54 o 6 6 0 53.81 48.40 21.00 o 7 6 0 14861.25 14653.90 220.07 o 8 6 0 10318.35 9899.02 234.82 o 9 6 0 6210.69 6255.36 195.20 o 10 6 0 4626.37 4564.77 143.00 o 11 6 0 2447.31 2448.58 110.13 o 12 6 0 2512.31 2739.08 123.22 o 13 6 0 737.02 633.12 101.19 o -10 7 0 154.72 156.02 60.56 o -9 7 0 318.23 283.51 60.37 o -8 7 0 1559.18 1655.47 108.38 o -7 7 0 889.28 1180.32 77.79 o -6 7 0 838.91 911.37 67.75 o -5 7 0 3599.88 3642.18 127.80 o -4 7 0 406.32 503.17 58.80 o -3 7 0 5169.87 5039.93 240.07 o -2 7 0 145.67 132.26 25.31 o -1 7 0 508.03 361.29 22.26 o 0 7 0 2364.97 2155.21 51.37 o 1 7 0 9152.57 9162.25 119.03 o 2 7 0 48.80 56.57 16.55 o 3 7 0 8372.92 8630.13 127.02 o 4 7 0 2277.74 2008.11 60.36 o 5 7 0 11.50 -48.12 24.06 o 6 7 0 872.37 869.87 42.28 o 7 7 0 47.29 -1.17 27.52 o 8 7 0 10037.56 10156.82 286.95 o 9 7 0 10385.79 9885.09 358.84 o 10 7 0 14.09 -54.97 40.69 o 11 7 0 708.74 603.27 70.63 o 12 7 0 42.58 -3.17 82.61 o 13 7 0 2108.47 2403.92 261.80 o -10 8 0 43.96 44.51 68.05 o -9 8 0 620.45 682.11 73.82 o -8 8 0 1292.28 1276.22 90.80 o -7 8 0 614.12 665.35 57.10 o -6 8 0 184.42 297.38 62.27 o -5 8 0 188.48 115.82 64.35 o -4 8 0 3775.33 3824.64 147.69 o -3 8 0 24.09 73.41 36.36 o -2 8 0 2590.08 2357.28 71.21 o -1 8 0 119.55 87.18 53.23 o 0 8 0 478.30 511.47 48.89 o 1 8 0 5676.68 5378.44 80.90 o 2 8 0 15.82 -2.06 27.40 o 3 8 0 6200.22 6218.65 98.41 o 4 8 0 671.64 664.46 32.06 o 5 8 0 29.55 18.09 17.43 o 6 8 0 9605.64 9793.19 150.10 o 7 8 0 1027.71 1080.73 49.26 o 8 8 0 2149.79 2124.26 66.30 o 9 8 0 4133.28 4201.59 94.67 o 10 8 0 5.23 -82.80 50.43 o 11 8 0 23.89 -17.80 51.30 o 12 8 0 768.55 691.25 79.81 o 13 8 0 1288.04 1528.15 145.37 o -10 9 0 1696.74 1845.30 121.88 o -9 9 0 902.39 749.58 83.02 o -8 9 0 2160.59 2407.68 124.31 o -7 9 0 256.23 197.10 54.30 o -6 9 0 678.29 631.92 59.97 o -5 9 0 554.68 540.38 86.01 o -4 9 0 39.60 18.15 34.29 o -3 9 0 40.58 54.80 33.27 o -2 9 0 3066.48 2895.06 113.71 o -1 9 0 8129.09 7773.82 166.75 o 0 9 0 2149.71 2226.22 84.32 o 1 9 0 1336.08 1472.92 40.25 o 2 9 0 431.59 486.12 58.12 o 3 9 0 4001.00 3981.20 70.00 o 4 9 0 15725.69 15642.54 238.58 o 5 9 0 5113.63 4985.32 118.14 o 6 9 0 10679.79 10897.48 167.15 o 7 9 0 8492.92 8488.57 152.17 o 8 9 0 33.81 6.79 27.85 o 9 9 0 306.66 293.21 41.10 o 10 9 0 6.12 -37.82 28.63 o 11 9 0 1052.32 1032.65 69.84 o 12 9 0 103.76 32.52 64.80 o -9 10 0 2184.49 2206.22 134.78 o -8 10 0 1936.04 2229.84 129.09 o -7 10 0 4000.68 4090.87 328.05 o -6 10 0 482.39 354.58 65.43 o -5 10 0 410.13 325.15 50.60 o -4 10 0 155.80 86.97 62.89 o -3 10 0 1132.18 1154.95 74.26 o -2 10 0 1173.12 1128.90 44.89 o -1 10 0 3369.93 3262.24 75.70 o 0 10 0 9077.87 8631.88 147.96 o 1 10 0 3265.87 3032.25 78.26 o 2 10 0 2843.31 2850.92 89.24 o 3 10 0 633.45 550.07 31.64 o 4 10 0 17087.35 17282.21 221.17 o 5 10 0 16659.27 17013.36 219.21 o 6 10 0 3363.36 3379.37 80.58 o 7 10 0 3331.29 3448.33 88.77 o 8 10 0 103.74 134.64 35.25 o 9 10 0 1267.53 1269.95 61.55 o 10 10 0 1365.56 1377.17 63.88 o 11 10 0 1817.84 1454.19 114.91 o 12 10 0 785.73 849.67 81.70 o -8 11 0 744.10 852.14 132.21 o -7 11 0 1012.63 1033.12 101.11 o -6 11 0 1579.61 1527.39 112.78 o -5 11 0 102.67 202.67 93.92 o -4 11 0 1620.13 1541.58 98.44 o -3 11 0 386.65 420.57 43.03 o -2 11 0 370.54 447.41 60.91 o -1 11 0 619.60 555.10 39.33 o 0 11 0 1174.14 1102.72 50.19 o 1 11 0 826.36 790.81 49.69 o 2 11 0 156.33 89.49 30.31 o 3 11 0 2388.51 2369.45 60.66 o 4 11 0 65.82 16.81 24.28 o 5 11 0 12507.28 12428.78 183.68 o 6 11 0 2035.34 1989.20 87.50 o 7 11 0 81.23 61.01 38.20 o 8 11 0 2075.34 2113.04 76.06 o 9 11 0 928.92 988.90 59.88 o 10 11 0 3129.20 3104.33 92.95 o 11 11 0 3285.53 3208.65 136.23 o -7 12 0 329.27 448.05 82.53 o -6 12 0 37.76 -6.26 62.87 o -5 12 0 472.40 495.07 80.68 o -4 12 0 347.26 447.13 91.32 o -3 12 0 859.95 750.00 54.17 o -2 12 0 426.93 509.78 38.99 o -1 12 0 1562.56 1582.46 75.24 o 0 12 0 562.58 498.39 54.73 o 1 12 0 915.58 898.45 79.91 o 2 12 0 1794.60 1760.33 59.30 o 3 12 0 61.02 84.20 30.13 o 4 12 0 229.52 188.82 29.83 o 5 12 0 2068.84 1973.54 60.93 o 6 12 0 2282.21 2319.57 78.23 o 7 12 0 43.39 40.38 38.75 o 8 12 0 514.01 460.09 59.55 o 9 12 0 54.19 92.03 40.32 o 10 12 0 4393.52 4587.61 128.61 o 11 12 0 3931.31 3753.90 150.91 o -6 13 0 489.32 452.55 88.01 o -5 13 0 33.40 -24.08 64.96 o -4 13 0 55.79 90.13 73.71 o -3 13 0 684.68 538.72 64.84 o -2 13 0 61.30 25.60 30.79 o -1 13 0 72.73 27.00 34.97 o 0 13 0 4130.03 3989.64 98.28 o 1 13 0 3408.91 3317.14 91.38 o 2 13 0 2444.73 2562.31 132.63 o 3 13 0 315.73 578.92 62.55 o 4 13 0 67.63 132.06 31.63 o 5 13 0 13.90 11.63 30.57 o 6 13 0 303.75 243.45 42.76 o 7 13 0 12.16 23.72 41.32 o 8 13 0 3167.37 3068.42 104.55 o 9 13 0 6.71 76.42 45.86 o 10 13 0 343.11 278.45 53.15 o -4 14 0 470.91 542.27 125.62 o -3 14 0 5.07 -7.59 42.15 o -2 14 0 24.34 -51.42 63.03 o -1 14 0 553.90 490.69 46.19 o 0 14 0 328.45 314.28 43.01 o 1 14 0 2759.55 2629.75 105.14 o 2 14 0 1834.79 1814.28 83.77 o 3 14 0 2486.77 2359.43 162.77 o 4 14 0 402.05 427.94 48.94 o 5 14 0 1169.48 1057.11 53.89 o 6 14 0 1906.68 1762.09 79.05 o 7 14 0 30.28 16.59 44.03 o 8 14 0 1571.98 1524.65 153.39 o -2 15 0 194.09 180.08 51.26 o -1 15 0 292.12 251.00 43.79 o 0 15 0 3025.32 3040.62 92.81 o 1 15 0 14.24 -46.45 41.75 o 2 15 0 1120.16 1074.68 72.05 o 3 15 0 81.59 128.82 48.54 o 4 15 0 447.91 391.48 50.49 o 5 15 0 192.11 141.46 45.16 o 6 15 0 1375.97 1233.20 70.94 o 7 15 0 2344.15 2222.79 99.61 o 1 16 0 1562.03 1593.15 85.56 o 2 16 0 121.74 37.14 50.75 o 3 16 0 721.99 653.61 66.95 o 4 16 0 176.13 176.10 64.00 o -3 -16 1 160.62 144.64 52.84 o -2 -16 1 2.18 -10.87 48.07 o -1 -16 1 527.52 420.85 60.14 o -7 -15 1 66.74 157.52 51.74 o -6 -15 1 48.90 122.72 45.31 o -5 -15 1 626.82 547.64 55.28 o -4 -15 1 338.13 308.09 49.68 o -3 -15 1 18.00 -42.36 45.06 o -2 -15 1 2175.01 2188.47 134.91 o -1 -15 1 156.93 31.25 44.78 o 0 -15 1 379.37 431.58 49.88 o 1 -15 1 1708.38 1655.51 72.07 o 2 -15 1 631.35 459.96 71.36 o -8 -14 1 8.56 91.57 48.52 o -7 -14 1 1439.85 1419.78 81.96 o -6 -14 1 774.54 807.97 60.36 o -5 -14 1 847.62 820.18 49.48 o -4 -14 1 4839.91 4590.41 114.65 o -3 -14 1 934.09 889.47 66.63 o -2 -14 1 4630.80 4661.99 144.64 o -1 -14 1 2972.66 3290.43 93.90 o 0 -14 1 134.04 30.48 36.15 o 1 -14 1 1.13 -8.95 33.85 o 2 -14 1 216.78 128.39 67.59 o 3 -14 1 686.16 575.58 58.38 o 4 -14 1 80.59 38.50 68.83 o -9 -13 1 254.83 180.30 64.72 o -8 -13 1 1388.55 1538.87 81.70 o -7 -13 1 772.06 760.93 62.73 o -6 -13 1 637.86 640.30 52.68 o -5 -13 1 123.08 117.85 34.14 o -4 -13 1 5412.54 5484.79 106.20 o -3 -13 1 4338.00 4092.51 102.72 o -2 -13 1 2321.68 2582.85 90.12 o -1 -13 1 4368.00 4686.43 110.58 o 0 -13 1 590.83 704.82 49.58 o 1 -13 1 1257.20 1292.43 75.33 o 2 -13 1 141.59 101.03 31.64 o 3 -13 1 717.04 652.24 58.49 o 4 -13 1 3596.02 3592.03 140.72 o 5 -13 1 0.57 -68.16 63.73 o 6 -13 1 7.81 -100.93 65.72 o -10 -12 1 1636.19 1824.78 80.70 o -9 -12 1 1370.83 1426.22 71.77 o -8 -12 1 80.34 -20.33 37.75 o -7 -12 1 281.34 192.31 42.91 o -6 -12 1 2600.56 2455.26 79.91 o -5 -12 1 3529.25 3590.04 81.06 o -4 -12 1 199.51 220.10 30.45 o -3 -12 1 2352.03 2293.92 90.12 o -2 -12 1 2314.44 2342.73 67.01 o -1 -12 1 1074.95 1053.34 53.66 o 0 -12 1 3233.16 3025.23 102.41 o 1 -12 1 503.28 465.27 41.67 o 2 -12 1 10922.41 10778.17 210.32 o 3 -12 1 2021.35 1964.25 78.06 o 4 -12 1 3288.19 3278.15 128.83 o 5 -12 1 4636.66 4711.40 156.35 o 6 -12 1 33.47 -62.27 81.83 o 7 -12 1 612.80 589.18 106.01 o -11 -11 1 1684.73 1585.25 90.07 o -10 -11 1 291.10 351.48 60.83 o -9 -11 1 4486.46 4695.22 114.85 o -8 -11 1 1133.01 1209.72 62.96 o -7 -11 1 161.72 150.79 36.36 o -6 -11 1 208.97 102.74 32.06 o -5 -11 1 137.47 251.98 30.83 o -4 -11 1 1090.16 1065.03 59.39 o -3 -11 1 29.52 -0.70 22.30 o -2 -11 1 2166.64 2112.55 51.85 o -1 -11 1 151.74 117.46 29.17 o 0 -11 1 1587.58 1453.94 66.25 o 1 -11 1 69.89 -25.48 24.25 o 2 -11 1 6462.51 6502.96 120.91 o 3 -11 1 9513.34 9719.69 234.23 o 4 -11 1 4811.64 4949.58 151.86 o 5 -11 1 6230.82 5559.38 165.54 o 6 -11 1 2313.66 2439.52 132.40 o 7 -11 1 589.20 397.85 151.42 o 8 -11 1 1208.51 1216.65 109.76 o -12 -10 1 1.41 -4.88 49.81 o -11 -10 1 1202.47 1142.65 76.85 o -10 -10 1 140.12 147.00 38.27 o -9 -10 1 272.58 269.50 40.06 o -8 -10 1 2670.18 2617.30 80.39 o -7 -10 1 703.68 632.35 46.23 o -6 -10 1 721.94 736.32 43.94 o -5 -10 1 1907.27 2140.24 70.03 o -4 -10 1 1331.40 1636.02 83.89 o -3 -10 1 1580.73 1545.66 46.28 o -2 -10 1 571.07 576.96 36.26 o -1 -10 1 85.31 81.39 30.53 o 0 -10 1 1928.42 1752.46 64.31 o 1 -10 1 173.73 131.59 28.44 o 2 -10 1 1710.39 1672.88 52.97 o 3 -10 1 6915.41 6536.47 194.75 o 4 -10 1 740.69 656.80 64.85 o 5 -10 1 542.50 410.10 55.09 o 6 -10 1 1197.50 1238.27 81.58 o 7 -10 1 22.27 2.05 63.17 o 8 -10 1 3852.62 4014.41 167.92 o 9 -10 1 1013.42 1061.87 102.29 o -12 -9 1 503.88 398.74 79.25 o -11 -9 1 1101.00 975.62 92.87 o -10 -9 1 35.36 10.41 30.21 o -9 -9 1 1749.16 1953.87 68.53 o -8 -9 1 510.30 529.08 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