# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' f80109b in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 341.44 _exptl_crystal_F_000 1188.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.0250 _cell_length_b 13.7050 _cell_length_c 17.7270 _cell_angle_alpha 74.595 _cell_angle_beta 85.646 _cell_angle_gamma 67.238 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5701.49 6674.94 108.37 o 2 0 0 20934.37 21893.24 336.68 o 3 0 0 1404.99 1287.63 26.86 o 4 0 0 3084.12 3559.68 63.53 o 5 0 0 8564.63 9169.72 150.52 o 6 0 0 5412.35 5309.61 95.09 o 7 0 0 156.07 172.95 13.07 o 8 0 0 424.04 414.47 21.49 o 9 0 0 85.34 61.36 20.97 o 10 0 0 88.86 42.77 20.45 o 11 0 0 131.66 144.53 27.79 o 12 0 0 18.75 -8.78 17.36 o 13 0 0 5.33 -9.81 18.49 o -12 1 0 69.17 52.17 23.35 o -11 1 0 55.67 25.62 21.07 o -10 1 0 85.78 69.22 21.38 o -9 1 0 6.82 -2.17 10.95 o -8 1 0 142.06 132.54 23.24 o -7 1 0 1659.17 1737.23 65.29 o -6 1 0 2264.45 2102.26 44.84 o -5 1 0 619.75 488.99 16.60 o -4 1 0 15607.84 17407.75 362.82 o -3 1 0 1014.68 981.21 21.69 o -2 1 0 12355.68 12831.32 202.26 o -1 1 0 18025.66 19946.19 416.64 o 0 1 0 130.51 244.84 8.16 o 2 1 0 1967.66 1792.08 32.34 o 3 1 0 16.38 18.49 6.72 o 4 1 0 6870.87 6704.48 111.06 o 5 1 0 2820.67 2744.48 53.51 o 6 1 0 3742.96 3749.15 71.18 o 7 1 0 2345.09 2161.10 48.45 o 8 1 0 240.21 227.28 15.81 o 9 1 0 334.47 346.29 32.54 o 10 1 0 320.44 296.70 32.23 o 11 1 0 24.04 -9.50 19.22 o 12 1 0 221.35 215.29 30.99 o 13 1 0 11.13 -2.07 17.46 o -12 2 0 3.75 -18.29 18.29 o -11 2 0 99.46 72.11 23.35 o -10 2 0 36.76 -12.09 16.94 o -9 2 0 28.00 14.77 12.71 o -8 2 0 71.60 106.51 17.87 o -7 2 0 51.06 18.70 12.40 o -6 2 0 123.24 139.67 21.07 o -5 2 0 1355.75 1244.88 58.78 o -4 2 0 2139.84 2059.35 40.16 o -3 2 0 9334.36 9853.56 157.88 o -2 2 0 35457.60 36385.65 559.35 o -1 2 0 17131.09 17357.90 268.76 o 0 2 0 13686.32 15051.46 316.54 o 1 2 0 2954.97 3037.58 50.41 o 2 2 0 2783.52 2607.64 45.51 o 3 2 0 17.65 42.25 7.13 o 4 2 0 473.87 531.93 17.36 o 5 2 0 1081.44 858.70 24.48 o 6 2 0 9782.39 10002.28 166.02 o 7 2 0 1028.96 975.95 30.06 o 8 2 0 2290.81 2272.67 53.00 o 9 2 0 27.04 23.86 12.40 o 10 2 0 665.41 680.08 46.28 o 11 2 0 703.42 691.13 48.97 o 12 2 0 38.39 7.54 23.66 o 13 2 0 262.68 196.70 32.65 o -11 3 0 20.25 0.41 19.11 o -10 3 0 80.77 47.83 21.38 o -9 3 0 72.36 53.41 15.50 o -8 3 0 115.37 95.35 16.12 o -7 3 0 337.32 292.26 20.97 o -6 3 0 64.80 99.69 15.19 o -5 3 0 1537.40 1574.21 56.82 o -4 3 0 8900.91 9566.98 155.62 o -1 3 0 314.06 319.88 10.84 o 0 3 0 1905.22 1871.53 46.18 o 1 3 0 2323.35 2379.23 42.75 o 2 3 0 2.71 4.61 3.93 o 3 3 0 3715.16 3944.06 52.83 o 4 3 0 1543.48 1553.86 34.30 o 5 3 0 3297.84 3357.20 64.15 o 6 3 0 8462.09 9415.28 157.85 o 7 3 0 11407.52 12131.66 201.35 o 8 3 0 16.76 30.68 12.50 o 9 3 0 2899.69 2958.84 67.15 o 10 3 0 966.15 886.69 33.89 o 11 3 0 36.87 23.35 22.73 o 12 3 0 544.42 541.44 46.08 o 13 3 0 83.44 58.06 28.00 o -11 4 0 134.34 114.57 24.90 o -10 4 0 0.07 -12.91 12.91 o -9 4 0 154.15 139.05 19.84 o -8 4 0 105.57 80.17 16.01 o -7 4 0 19.93 18.49 13.74 o -6 4 0 184.30 128.21 16.32 o -5 4 0 8.73 -0.21 11.26 o -4 4 0 1017.97 1061.97 24.57 o -3 4 0 7762.27 7926.09 129.88 o -2 4 0 3044.37 2974.20 53.56 o -1 4 0 121.95 109.20 9.04 o 1 4 0 1101.02 1194.53 27.32 o 2 4 0 26586.79 27112.65 406.03 o 3 4 0 10964.16 11450.53 380.48 o 4 4 0 2692.13 2977.52 42.68 o 5 4 0 2325.33 2078.56 45.15 o 6 4 0 1545.70 1577.62 39.36 o 7 4 0 3470.25 3795.23 76.14 o 8 4 0 6099.71 6152.92 114.47 o 9 4 0 381.95 359.20 22.93 o 10 4 0 1301.56 1276.27 41.74 o 11 4 0 2036.40 2004.59 82.13 o 12 4 0 1.48 5.99 23.55 o 13 4 0 756.95 677.08 53.31 o 14 4 0 74.66 58.27 26.55 o -10 5 0 53.48 70.15 17.46 o -9 5 0 295.55 283.79 24.38 o -8 5 0 3.62 -14.05 14.05 o -7 5 0 322.64 308.58 23.14 o -6 5 0 199.12 156.82 16.84 o -5 5 0 86.28 48.45 13.84 o -4 5 0 38.36 16.63 11.67 o -3 5 0 1830.59 1961.54 34.90 o -2 5 0 634.44 756.85 18.49 o -1 5 0 17.12 21.82 5.84 o 1 5 0 853.96 812.40 26.76 o 2 5 0 1985.13 1949.60 40.50 o 3 5 0 5669.11 5467.78 73.70 o 4 5 0 10172.40 10667.81 166.69 o 5 5 0 1703.32 1672.04 39.05 o 6 5 0 11280.69 12198.09 201.24 o 7 5 0 12729.75 13413.51 222.32 o 8 5 0 8.29 -1.76 14.05 o 9 5 0 2768.79 2719.38 64.46 o 10 5 0 1437.43 1401.17 44.22 o 11 5 0 162.98 148.66 18.80 o 12 5 0 1501.97 1483.81 72.63 o 13 5 0 102.60 84.09 29.03 o 14 5 0 274.74 302.28 41.32 o -10 6 0 38.30 31.30 15.70 o -9 6 0 261.27 307.44 25.83 o -8 6 0 311.28 305.28 24.69 o -7 6 0 1.48 -12.81 12.81 o -6 6 0 0.23 2.38 12.19 o -5 6 0 35.52 43.49 13.33 o -4 6 0 11.16 -10.12 11.78 o -3 6 0 11.44 19.94 11.47 o -2 6 0 1807.06 1858.99 34.28 o -1 6 0 58.44 53.44 7.37 o 0 6 0 1941.89 2093.43 43.91 o 1 6 0 279.99 229.02 13.59 o 2 6 0 1292.79 1218.08 31.26 o 3 6 0 10204.29 10244.68 164.75 o 4 6 0 695.89 607.85 16.04 o 5 6 0 6589.19 7039.92 94.42 o 6 6 0 41.71 24.48 9.92 o 7 6 0 2271.22 2477.02 57.13 o 8 6 0 7363.05 7423.61 135.44 o 9 6 0 651.61 680.49 30.27 o 10 6 0 1594.29 1676.59 49.90 o 11 6 0 1016.97 1036.70 39.98 o 12 6 0 9.43 0.00 15.08 o 13 6 0 205.29 205.69 32.96 o 14 6 0 208.67 269.12 41.01 o -9 7 0 43.29 74.07 18.70 o -8 7 0 147.85 132.96 20.87 o -7 7 0 520.23 556.83 31.10 o -6 7 0 2.51 6.30 11.98 o -5 7 0 626.35 593.40 28.93 o -4 7 0 784.53 697.95 30.27 o -3 7 0 5.24 -10.33 11.67 o -2 7 0 1.36 6.51 7.52 o -1 7 0 835.39 898.80 22.34 o 0 7 0 147.50 123.12 9.92 o 1 7 0 79.63 92.73 8.37 o 2 7 0 71.19 100.34 11.77 o 3 7 0 729.51 746.04 25.14 o 4 7 0 9060.86 9061.10 149.62 o 5 7 0 213.53 168.70 13.33 o 6 7 0 2352.15 2495.20 41.27 o 7 7 0 566.76 537.41 24.07 o 8 7 0 29.80 29.34 12.91 o 9 7 0 2983.76 3030.75 70.87 o 10 7 0 360.00 450.84 26.65 o 11 7 0 301.33 317.88 23.86 o 12 7 0 993.04 1057.77 41.74 o 13 7 0 197.03 189.26 22.11 o 14 7 0 296.11 343.50 42.15 o -8 8 0 286.51 300.52 44.01 o -7 8 0 121.86 109.20 33.16 o -6 8 0 1198.58 1140.31 43.39 o -5 8 0 72.81 61.57 14.98 o -4 8 0 2.64 -9.71 12.60 o -3 8 0 782.04 757.66 31.20 o -2 8 0 243.44 236.78 18.18 o -1 8 0 641.81 612.00 19.25 o 0 8 0 21.19 9.47 9.71 o 1 8 0 258.17 229.26 11.73 o 2 8 0 97.58 82.42 14.20 o 3 8 0 747.57 800.65 28.23 o 4 8 0 198.92 187.68 15.58 o 5 8 0 3618.39 3653.86 71.85 o 6 8 0 0.35 -6.10 6.10 o 7 8 0 236.48 207.44 16.32 o 8 8 0 1679.98 1752.93 48.55 o 9 8 0 17.82 28.10 15.08 o 10 8 0 2150.52 2354.70 63.02 o 11 8 0 747.79 761.17 34.81 o 12 8 0 37.84 38.22 17.36 o 13 8 0 763.64 852.91 39.77 o 14 8 0 290.58 318.50 41.32 o -7 9 0 697.96 836.69 66.84 o -6 9 0 4.05 7.44 29.75 o -5 9 0 1151.07 1142.38 70.97 o -4 9 0 474.16 485.24 46.49 o -3 9 0 7.71 -11.05 23.97 o -2 9 0 2186.40 2224.84 91.12 o -1 9 0 166.93 143.60 28.20 o 0 9 0 134.30 121.20 15.31 o 1 9 0 5.64 -2.71 22.16 o 2 9 0 1079.82 1116.29 26.58 o 3 9 0 23.68 -0.55 14.82 o 4 9 0 13.93 6.92 11.18 o 5 9 0 11.52 -11.03 11.03 o 6 9 0 9.74 -7.54 15.50 o 7 9 0 512.33 423.36 34.40 o 8 9 0 4.05 -9.19 10.43 o 9 9 0 1373.90 1451.89 45.56 o 10 9 0 674.15 623.05 31.20 o 11 9 0 262.58 273.97 24.48 o 12 9 0 1062.36 1143.93 45.35 o 13 9 0 67.95 99.28 19.53 o -6 10 0 1086.65 1162.01 78.31 o -5 10 0 463.40 394.12 48.24 o -4 10 0 83.35 108.89 33.37 o -3 10 0 220.61 185.54 31.82 o -2 10 0 234.12 299.08 37.71 o -1 10 0 950.56 938.66 57.44 o 0 10 0 283.57 292.07 29.44 o 1 10 0 11.70 -10.92 10.92 o 2 10 0 178.73 163.74 29.18 o 3 10 0 43.90 48.24 12.58 o 4 10 0 0.13 -10.53 10.53 o 5 10 0 274.57 241.04 18.72 o 6 10 0 84.30 43.80 19.94 o 7 10 0 236.29 292.26 31.72 o 9 10 0 41.39 15.08 12.50 o 10 10 0 531.62 577.80 29.75 o 11 10 0 771.33 750.95 35.64 o 12 10 0 8.21 20.56 16.12 o 13 10 0 482.02 471.70 31.51 o -5 11 0 797.81 803.74 67.25 o -4 11 0 823.22 874.19 66.84 o -3 11 0 92.36 141.84 31.51 o -2 11 0 282.75 348.15 40.60 o -1 11 0 3.32 -6.61 21.69 o 0 11 0 28.35 7.75 20.97 o 1 11 0 161.56 113.94 27.94 o 2 11 0 87.17 79.00 14.48 o 3 11 0 173.23 187.21 30.99 o 4 11 0 4.25 -8.03 14.98 o 5 11 0 26.45 5.68 12.42 o 6 11 0 62.84 -1.96 19.63 o 7 11 0 121.18 105.79 24.90 o 8 11 0 18.07 1.96 19.63 o 9 11 0 401.92 397.74 37.60 o 10 11 0 85.81 53.82 22.42 o 11 11 0 460.71 412.61 41.53 o 12 11 0 454.06 443.19 45.15 o 13 11 0 31.78 15.60 22.93 o -4 12 0 261.56 275.94 42.98 o -3 12 0 331.95 468.09 47.62 o -2 12 0 24.78 17.87 23.55 o -1 12 0 723.77 809.73 58.58 o 0 12 0 457.82 542.16 48.24 o 1 12 0 238.70 249.18 36.26 o 2 12 0 1018.50 940.94 37.68 o 3 12 0 32.26 26.85 12.41 o 4 12 0 3.15 -11.14 11.14 o 5 12 0 133.17 89.36 22.83 o 6 12 0 8.89 -16.63 16.63 o 7 12 0 3.83 -20.97 20.97 o 8 12 0 1.35 -19.22 19.22 o 9 12 0 2.00 -21.49 21.49 o 10 12 0 31.67 -5.06 16.63 o 11 12 0 53.60 32.34 21.90 o 12 12 0 29.54 -19.84 19.84 o -2 13 0 218.07 216.12 38.84 o -1 13 0 118.53 119.94 33.06 o 0 13 0 336.53 387.71 44.73 o 1 13 0 1896.71 1895.39 88.95 o 2 13 0 105.93 113.02 28.72 o 3 13 0 496.63 477.04 28.14 o 4 13 0 484.55 485.55 28.78 o 5 13 0 46.94 4.13 21.38 o 6 13 0 325.21 281.41 35.12 o 7 13 0 28.54 -14.88 20.45 o 9 13 0 13.30 -21.28 21.28 o 10 13 0 47.91 18.49 22.11 o -1 14 0 150.11 146.90 32.75 o 0 14 0 614.79 657.66 56.61 o 1 14 0 66.27 60.75 31.20 o 2 14 0 781.22 827.50 60.02 o 3 14 0 199.24 170.87 33.37 o 4 14 0 103.23 100.87 19.30 o 5 14 0 475.97 485.75 43.29 o 6 14 0 12.47 -18.39 18.39 o 7 14 0 119.67 92.25 27.38 o 8 14 0 48.16 -10.33 22.11 o 9 14 0 20.07 -20.35 20.35 o 10 14 0 0.14 -15.91 21.28 o 2 15 0 48.92 95.56 32.65 o 3 15 0 612.07 643.30 53.10 o 4 15 0 150.61 173.04 29.86 o 5 15 0 66.53 73.97 24.69 o 6 15 0 356.50 335.34 39.36 o 7 15 0 98.31 87.40 28.72 o 8 15 0 46.82 26.24 25.83 o 9 15 0 53.08 33.99 26.65 o -8 -15 1 210.16 219.94 36.47 o -7 -15 1 33.19 39.15 25.62 o -6 -15 1 159.28 181.72 33.99 o -5 -15 1 392.56 500.22 47.11 o -4 -15 1 57.08 53.62 23.55 o -3 -15 1 619.60 736.28 57.85 o -2 -15 1 527.43 622.95 55.17 o -10 -14 1 45.55 12.09 23.86 o -9 -14 1 194.69 201.76 35.02 o -8 -14 1 5.03 -20.25 20.25 o -7 -14 1 400.43 422.74 45.15 o -6 -14 1 423.44 391.54 42.98 o -5 -14 1 144.07 140.81 28.51 o -4 -14 1 669.24 722.55 36.59 o -3 -14 1 44.98 70.77 29.65 o -2 -14 1 1153.13 1140.52 69.53 o -1 -14 1 968.08 997.96 67.67 o 0 -14 1 4.04 11.16 25.31 o -11 -13 1 1.53 -15.60 15.60 o -10 -13 1 32.24 -17.05 18.70 o -9 -13 1 3.45 -20.97 20.97 o -8 -13 1 563.10 505.38 47.11 o -7 -13 1 132.53 86.68 27.27 o -6 -13 1 486.01 470.98 42.98 o -5 -13 1 794.62 766.55 51.86 o -4 -13 1 22.74 24.94 15.31 o -3 -13 1 907.33 951.72 40.57 o -2 -13 1 539.48 571.71 49.17 o -1 -13 1 228.90 220.05 36.88 o 0 -13 1 793.94 870.68 63.64 o 1 -13 1 134.20 199.90 38.84 o 2 -13 1 32.78 44.11 29.03 o -12 -12 1 44.99 -12.91 22.52 o -10 -12 1 38.82 1.24 16.43 o -9 -12 1 124.05 85.13 26.86 o -8 -12 1 14.30 -20.15 20.15 o -7 -12 1 394.82 330.90 36.47 o -6 -12 1 144.89 107.75 25.72 o -5 -12 1 332.46 327.18 36.05 o -4 -12 1 1883.14 1781.64 53.27 o -3 -12 1 313.84 306.53 23.56 o -2 -12 1 915.55 928.23 51.55 o -1 -12 1 1485.27 1532.68 76.34 o 0 -12 1 202.22 198.25 35.43 o 1 -12 1 533.37 579.35 51.03 o 2 -12 1 255.63 283.99 38.84 o 3 -12 1 15.74 3.82 23.97 o 4 -12 1 675.20 742.16 64.26 o -13 -11 1 47.55 44.32 23.97 o -12 -11 1 12.41 -18.80 18.80 o -11 -11 1 24.43 -17.36 17.36 o -10 -11 1 37.05 17.05 18.49 o -9 -11 1 13.84 -9.61 15.60 o -8 -11 1 16.14 -17.46 17.46 o -7 -11 1 0.67 -17.05 17.05 o -6 -11 1 150.21 117.36 25.00 o -5 -11 1 357.90 378.87 38.90 o -4 -11 1 15.60 14.10 12.96 o -3 -11 1 653.53 666.64 47.01 o -2 -11 1 27.30 19.24 19.16 o -1 -11 1 49.02 13.83 14.32 o 0 -11 1 982.18 1068.72 62.71 o 1 -11 1 1683.25 1667.18 82.23 o 2 -11 1 574.53 617.78 52.17 o 3 -11 1 560.42 560.96 50.41 o 4 -11 1 37.79 42.77 35.23 o 5 -11 1 871.57 911.49 72.32 o -13 -10 1 104.06 123.04 20.04 o -12 -10 1 165.35 189.78 21.38 o -11 -10 1 100.00 74.59 17.36 o -10 -10 1 337.60 309.92 34.19 o -9 -10 1 197.13 186.88 27.27 o -8 -10 1 48.42 26.24 17.46 o -7 -10 1 0.07 -12.60 16.74 o -6 -10 1 167.72 145.35 25.62 o -5 -10 1 48.40 62.08 14.83 o -4 -10 1 509.56 515.88 25.93 o -3 -10 1 27.18 8.62 12.09 o -2 -10 1 293.95 284.64 20.13 o -1 -10 1 411.66 392.89 23.15 o 0 -10 1 3.71 -17.72 17.72 o 1 -10 1 2548.97 2740.04 104.34 o 2 -10 1 759.86 839.58 58.16 o 3 -10 1 386.61 433.89 43.70 o 4 -10 1 613.90 650.94 56.61 o 5 -10 1 48.31 119.84 38.43 o 6 -10 1 487.56 518.81 56.92 o -13 -9 1 173.88 176.66 21.69 o -12 -9 1 189.21 175.83 21.49 o -11 -9 1 771.75 803.12 35.85 o -10 -9 1 285.95 306.41 23.04 o -9 -9 1 213.00 235.54 20.25 o -8 -9 1 40.55 6.51 7.23 o -7 -9 1 10.31 -9.30 9.30 o -6 -9 1 3.40 -15.39 15.39 o -5 -9 1 252.15 290.71 19.69 o -4 -9 1 8.67 0.00 13.95 o -3 -9 1 281.64 278.25 25.52 o -2 -9 1 219.59 199.45 17.27 o -1 -9 1 31.07 -4.28 12.33 o 0 -9 1 3786.80 3731.79 118.08 o 1 -9 1 318.91 309.30 37.29 o 2 -9 1 3913.59 3949.05 130.37 o 3 -9 1 1585.20 1700.04 80.89 o 4 -9 1 253.97 245.25 37.81 o 5 -9 1 1683.18 1774.42 89.67 o 6 -9 1 1155.50 1141.97 74.49 o 7 -9 1 0.31 -25.21 35.23 o -14 -8 1 52.01 77.79 29.65 o -13 -8 1 279.65 328.21 26.96 o -12 -8 1 762.84 750.74 35.64 o -11 -8 1 5.51 12.50 13.95 o -10 -8 1 1539.43 1493.63 47.83 o -9 -8 1 779.54 804.87 32.85 o -8 -8 1 16.52 -10.54 10.54 o -7 -8 1 404.72 432.96 33.37 o -6 -8 1 0.20 -1.34 8.88 o -5 -8 1 124.19 109.38 14.51 o -4 -8 1 493.80 504.50 22.37 o -3 -8 1 0.77 -10.68 16.68 o -2 -8 1 413.60 403.01 14.72 o -1 -8 1 930.95 1037.76 24.28 o 0 -8 1 0.75 3.71 6.57 o 1 -8 1 1612.69 1609.78 33.46 o 2 -8 1 789.36 760.86 28.93 o 3 -8 1 27.26 0.93 26.45 o 4 -8 1 32.38 38.64 24.90 o 5 -8 1 271.14 285.44 38.43 o 6 -8 1 646.54 728.11 58.16 o 7 -8 1 1227.77 1237.53 76.55 o 8 -8 1 26.12 19.11 31.30 o -14 -7 1 578.93 692.58 55.99 o -13 -7 1 307.17 300.52 25.62 o -12 -7 1 209.39 220.15 22.21 o -11 -7 1 1026.75 1029.15 39.57 o -10 -7 1 89.93 65.39 15.08 o -9 -7 1 1050.30 988.24 35.85 o -8 -7 1 870.80 784.31 30.06 o -7 -7 1 19.49 14.26 10.02 o -6 -7 1 2082.40 2091.58 44.62 o -5 -7 1 212.84 227.63 11.40 o -4 -7 1 3.51 -8.95 8.95 o -3 -7 1 1551.13 1559.73 39.39 o -2 -7 1 37.59 56.54 10.28 o -1 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