# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 438.93 _exptl_crystal_F_000 1264.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.3387 _cell_length_b 12.9885 _cell_length_c 16.7968 _cell_angle_alpha 81.437 _cell_angle_beta 83.636 _cell_angle_gamma 88.474 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4022.93 4094.11 194.58 o 3 0 0 35.19 22.54 43.39 o 4 0 0 1691.19 1732.73 57.95 o 5 0 0 274.30 315.19 27.59 o 6 0 0 1680.89 1501.20 62.96 o 7 0 0 420.56 431.23 34.77 o 8 0 0 44390.60 41389.52 455.41 o 9 0 0 809.98 708.36 73.84 o 10 0 0 3815.29 3675.10 402.03 o 11 0 0 451.55 288.87 132.66 o 12 0 0 6335.45 7309.22 617.24 o 13 0 0 109.61 229.38 132.85 o 14 0 0 57.06 -85.51 123.80 o 15 0 0 554.88 430.66 171.97 o -15 1 0 1015.82 407.36 189.60 o -14 1 0 1218.86 1138.62 275.46 o -13 1 0 2244.01 2603.61 392.48 o -12 1 0 2350.95 2164.56 342.36 o -11 1 0 14154.46 14815.13 841.28 o -10 1 0 977.30 983.87 59.52 o -9 1 0 776.21 832.31 59.36 o -8 1 0 40.99 45.76 18.79 o -7 1 0 16321.08 17041.33 261.58 o -6 1 0 8463.86 8724.26 176.68 o -5 1 0 4574.11 4664.31 100.71 o -4 1 0 33198.75 33077.84 337.81 o -3 1 0 456.95 402.10 35.90 o -2 1 0 6364.34 6895.50 133.86 o -1 1 0 40542.81 41297.57 425.77 o 2 1 0 17218.23 17241.04 211.41 o 3 1 0 4344.18 4319.74 116.81 o 4 1 0 4554.51 4284.95 99.10 o 5 1 0 2435.02 2537.35 80.30 o 6 1 0 637.03 693.39 83.04 o 7 1 0 17300.91 16996.08 712.75 o 8 1 0 564.24 705.91 167.35 o 9 1 0 12087.10 12200.38 684.29 o 10 1 0 6588.84 6744.22 542.47 o 11 1 0 6155.62 5836.43 533.67 o 12 1 0 4593.13 5068.39 519.51 o 13 1 0 29.35 -129.52 119.57 o 14 1 0 2338.74 2916.01 435.00 o 15 1 0 6645.49 7173.74 701.52 o -15 2 0 5005.82 4250.77 542.48 o -14 2 0 1166.91 1173.16 283.15 o -13 2 0 149.40 -21.92 94.40 o -12 2 0 4092.18 3354.52 370.91 o -11 2 0 279.48 214.81 38.39 o -10 2 0 3430.60 3464.40 140.29 o -9 2 0 3858.60 3885.70 157.28 o -8 2 0 159.54 202.04 41.62 o -7 2 0 22993.31 23462.11 420.82 o -6 2 0 16977.06 16608.54 231.83 o -5 2 0 2052.33 1772.59 99.10 o -4 2 0 17603.00 17294.43 299.61 o -3 2 0 4253.25 4228.74 143.80 o -2 2 0 8195.61 7897.46 189.89 o -1 2 0 15811.40 15676.44 358.04 o 0 2 0 11444.75 11844.33 301.49 o 1 2 0 23403.40 25246.32 316.05 o 2 2 0 128094.02 121047.22 713.55 o 3 2 0 1303.03 1202.30 58.48 o 4 2 0 12032.95 12117.21 226.76 o 5 2 0 3669.62 3748.27 105.64 o 6 2 0 12297.11 12394.93 195.61 o 7 2 0 9861.62 10055.11 257.60 o 8 2 0 11948.18 12241.86 255.77 o 9 2 0 6348.17 6185.54 494.40 o 10 2 0 11238.22 11392.41 704.50 o 11 2 0 1960.16 1907.49 311.69 o 12 2 0 16.23 -122.73 113.60 o 13 2 0 3134.55 3826.56 476.63 o 14 2 0 2669.56 3022.47 452.21 o 15 2 0 2420.61 2812.68 456.78 o -15 3 0 1296.01 1554.97 334.49 o -14 3 0 1993.04 2114.66 380.89 o -13 3 0 5355.43 5803.60 589.06 o -12 3 0 262.37 210.43 85.22 o -11 3 0 47.40 11.83 24.03 o -10 3 0 275.29 305.22 75.38 o -9 3 0 24803.82 25278.64 660.08 o -8 3 0 5256.64 5544.60 200.08 o -7 3 0 432.98 359.82 56.94 o -6 3 0 6976.11 7233.68 236.97 o -5 3 0 38903.25 41061.82 556.25 o -4 3 0 1557.02 1394.07 100.20 o -3 3 0 1979.99 2184.06 146.91 o -2 3 0 1616.21 1305.96 128.57 o -1 3 0 586.78 813.98 100.90 o 0 3 0 1912.08 2316.80 165.44 o 1 3 0 17502.20 17317.90 322.49 o 2 3 0 4597.72 4149.89 128.08 o 3 3 0 92372.63 93115.52 675.18 o 4 3 0 4099.79 3714.83 124.45 o 5 3 0 15634.30 15829.17 349.14 o 6 3 0 2872.97 2950.50 110.93 o 7 3 0 61.79 76.48 19.77 o 8 3 0 3074.54 3014.79 97.63 o 9 3 0 4675.38 4953.84 259.41 o 10 3 0 229.58 185.37 49.68 o 11 3 0 13785.09 15035.06 870.73 o 12 3 0 3336.23 3434.13 440.92 o 13 3 0 4771.12 5666.55 591.56 o 14 3 0 461.59 328.72 181.48 o 15 3 0 626.31 1087.89 295.25 o -14 4 0 626.44 703.21 238.83 o -13 4 0 5823.99 5876.15 609.37 o -12 4 0 603.48 426.47 81.07 o -11 4 0 168.22 146.40 40.89 o -10 4 0 471.54 351.99 87.35 o -9 4 0 653.08 589.23 60.15 o -8 4 0 25903.00 25958.90 517.80 o -7 4 0 421.71 389.28 65.98 o -6 4 0 12488.95 12559.20 351.77 o -5 4 0 5449.13 5641.09 232.21 o -4 4 0 3467.89 3692.49 184.79 o -3 4 0 7816.09 8173.94 269.85 o -2 4 0 1448.68 1191.07 141.93 o -1 4 0 37262.46 39822.43 788.97 o 0 4 0 41652.99 41123.11 380.15 o 1 4 0 3034.00 3270.64 114.84 o 2 4 0 55199.13 56794.88 680.09 o 3 4 0 44707.15 46475.45 497.33 o 4 4 0 12569.68 12790.36 260.66 o 5 4 0 3714.00 3611.76 142.45 o 6 4 0 11.48 36.60 18.85 o 7 4 0 7066.94 7039.67 193.75 o 8 4 0 1762.09 1913.97 93.42 o 9 4 0 49.25 47.35 18.99 o 10 4 0 12773.31 13211.17 354.43 o 11 4 0 27.08 9.06 14.77 o 12 4 0 4371.32 4534.02 513.74 o 13 4 0 27.10 -159.49 124.94 o 14 4 0 2400.90 3671.06 510.14 o 15 4 0 1881.23 1954.24 380.92 o -14 5 0 196.55 279.56 157.40 o -13 5 0 268.62 350.54 186.01 o -12 5 0 16760.71 17032.06 836.00 o -11 5 0 58.33 15.53 31.86 o -10 5 0 1237.46 1310.52 96.55 o -9 5 0 11658.06 11863.32 388.74 o -8 5 0 1723.42 1794.40 151.65 o -7 5 0 2648.39 1828.56 946.46 o -6 5 0 3079.78 649.51 1395.99 o -5 5 0 457.52 310.19 111.66 o -4 5 0 29460.77 28899.36 571.65 o -3 5 0 10607.59 10610.11 370.48 o -2 5 0 20244.27 19690.27 629.72 o -1 5 0 13867.02 13845.18 523.97 o 0 5 0 99.66 159.01 28.08 o 1 5 0 2818.59 3067.14 172.28 o 2 5 0 2378.63 2859.60 103.31 o 3 5 0 34822.87 34122.63 477.91 o 4 5 0 28511.00 30230.82 458.75 o 5 5 0 248.68 273.77 37.64 o 6 5 0 16928.70 16733.08 350.42 o 7 5 0 2407.52 2378.60 117.39 o 8 5 0 1805.93 1919.47 112.68 o 9 5 0 2930.49 3304.96 153.36 o 10 5 0 1659.66 1481.83 86.54 o 11 5 0 6721.58 7084.13 631.59 o 12 5 0 1729.26 1486.54 315.56 o 13 5 0 808.41 1257.05 303.53 o 14 5 0 7469.38 8465.29 786.77 o -14 6 0 3999.14 4285.83 561.23 o -13 6 0 6602.19 6538.05 675.76 o -12 6 0 101.29 141.90 203.46 o -11 6 0 4063.63 4047.34 182.80 o -10 6 0 2969.05 2923.44 193.95 o -9 6 0 0.36 6.09 46.30 o -8 6 0 1197.90 998.99 163.86 o -7 6 0 2128.52 2123.05 237.20 o -6 6 0 12022.72 11804.06 550.77 o -5 6 0 24739.09 25756.93 664.16 o -4 6 0 4238.23 4305.50 242.32 o -3 6 0 5797.88 4831.42 652.54 o -2 6 0 13824.47 14610.33 594.13 o -1 6 0 8870.32 9598.23 475.31 o 0 6 0 151.22 221.89 35.17 o 1 6 0 246.37 244.57 56.31 o 2 6 0 15863.83 16284.17 406.57 o 3 6 0 34776.78 35026.69 732.81 o 4 6 0 11511.86 11167.97 300.96 o 5 6 0 97.88 51.15 26.85 o 6 6 0 11463.40 12150.78 284.32 o 7 6 0 8862.82 9107.27 281.59 o 8 6 0 1429.16 1286.63 103.44 o 9 6 0 52.03 47.99 25.80 o 10 6 0 535.95 523.26 61.33 o 11 6 0 2568.23 2526.46 395.00 o 12 6 0 2665.03 2972.49 444.49 o 13 6 0 42.05 114.43 111.90 o 14 6 0 1638.92 1356.86 343.04 o -13 7 0 1901.59 1719.36 352.19 o -12 7 0 1031.85 864.73 139.98 o -11 7 0 3415.11 3507.64 232.15 o -10 7 0 3007.07 2805.29 228.54 o -9 7 0 1848.67 1723.68 175.90 o -8 7 0 1411.72 1273.26 153.45 o -7 7 0 3999.14 3968.61 260.80 o -6 7 0 2047.54 1984.49 235.95 o -5 7 0 14960.50 14723.87 657.83 o -4 7 0 20505.70 20107.95 765.21 o -3 7 0 16113.50 15611.47 670.86 o -2 7 0 1276.57 1161.63 184.21 o -1 7 0 2131.55 2263.31 250.38 o 0 7 0 41.35 45.40 19.75 o 1 7 0 5251.37 5216.52 270.49 o 2 7 0 6470.64 6159.08 291.05 o 3 7 0 9917.78 10165.07 233.25 o 4 7 0 2587.62 2596.74 158.73 o 5 7 0 34262.83 34739.76 508.49 o 6 7 0 538.43 606.50 60.68 o 7 7 0 57.68 105.43 34.57 o 8 7 0 3606.21 3641.44 189.61 o 9 7 0 594.54 626.96 79.56 o 10 7 0 5760.18 5663.17 245.75 o 11 7 0 467.42 449.57 193.72 o 12 7 0 540.49 851.25 248.52 o 13 7 0 10346.59 11831.43 940.55 o 14 7 0 1576.18 1287.24 337.81 o -13 8 0 1701.76 2000.12 417.73 o -12 8 0 2.85 -63.26 42.17 o -11 8 0 1794.18 1556.15 237.92 o -10 8 0 188.92 145.49 90.16 o -9 8 0 10089.03 11314.69 631.07 o -8 8 0 1319.42 1627.12 243.17 o -7 8 0 2550.87 2581.46 227.72 o -6 8 0 19282.06 17997.89 678.84 o -5 8 0 4.09 -25.28 43.82 o -4 8 0 708.87 702.90 116.73 o -3 8 0 11195.47 11217.35 443.57 o -2 8 0 48.50 0.30 43.19 o -1 8 0 24166.95 24242.41 877.70 o 0 8 0 1418.38 1539.22 221.33 o 1 8 0 12356.63 12340.40 447.85 o 2 8 0 11711.64 12552.72 964.22 o 3 8 0 270.99 341.07 45.36 o 4 8 0 532.24 509.58 53.95 o 5 8 0 7200.24 7855.27 258.88 o 6 8 0 7022.31 6925.09 239.67 o 7 8 0 778.71 847.98 100.24 o 8 8 0 681.30 601.35 86.78 o 9 8 0 17173.13 17398.31 441.41 o 10 8 0 3071.27 3211.45 236.29 o 11 8 0 1258.63 1369.29 316.65 o 12 8 0 2860.21 2939.80 472.79 o 13 8 0 0.60 -223.10 174.14 o -12 9 0 1752.10 1350.18 237.85 o -11 9 0 677.52 777.32 184.20 o -10 9 0 16449.27 16454.87 803.03 o -9 9 0 67.87 -74.95 77.13 o -8 9 0 193.50 233.70 102.57 o -7 9 0 475.39 704.38 169.52 o -6 9 0 1092.53 815.36 186.69 o -5 9 0 456.01 418.95 135.58 o -4 9 0 87.43 145.59 84.25 o -3 9 0 851.14 892.83 184.30 o -2 9 0 30453.44 31870.68 1167.89 o -1 9 0 2280.65 2344.58 126.83 o 0 9 0 1724.21 1853.59 154.78 o 1 9 0 161.41 83.96 39.06 o 2 9 0 7203.68 7519.34 332.20 o 3 9 0 1899.60 1918.93 154.77 o 4 9 0 2231.87 2205.99 134.89 o 5 9 0 8.15 22.77 22.79 o 6 9 0 20329.63 20628.91 513.59 o 7 9 0 309.64 312.37 70.49 o 8 9 0 3011.48 3048.64 202.10 o 9 9 0 256.51 236.92 61.87 o 10 9 0 4709.35 5057.37 368.08 o 11 9 0 193.58 200.36 131.51 o 12 9 0 0.21 -8.79 92.65 o -12 10 0 1012.95 799.58 194.86 o -11 10 0 57.67 -122.56 104.94 o -10 10 0 35.97 -90.33 93.55 o -9 10 0 2329.15 2636.53 344.59 o -8 10 0 1572.00 1649.96 273.87 o -7 10 0 1207.63 1204.59 242.76 o -6 10 0 3024.27 2458.69 332.47 o -5 10 0 2950.17 2790.51 347.30 o -4 10 0 2183.13 1903.57 289.17 o -3 10 0 7082.10 7663.44 560.26 o -2 10 0 347.38 405.15 142.06 o -1 10 0 10980.83 11281.14 424.87 o 0 10 0 8168.70 7229.14 540.19 o 1 10 0 479.82 622.39 166.54 o 2 10 0 2958.13 2745.96 332.51 o 3 10 0 400.95 515.95 150.50 o 4 10 0 6223.88 6645.99 510.05 o 5 10 0 7653.12 7546.38 309.81 o 6 10 0 0.75 -32.51 26.82 o 7 10 0 7671.34 7950.32 427.22 o 8 10 0 3217.90 3205.82 273.83 o 9 10 0 1013.87 1097.87 342.77 o 10 10 0 690.54 732.69 133.24 o 11 10 0 1813.59 1247.53 318.46 o 12 10 0 36.44 214.55 162.71 o -11 11 0 1176.43 1062.09 239.58 o -10 11 0 168.25 196.69 119.56 o -9 11 0 3947.53 3944.87 443.09 o -8 11 0 4980.68 5227.60 506.66 o -7 11 0 2446.27 2083.17 315.15 o -6 11 0 6852.19 6711.07 569.71 o -5 11 0 853.38 833.93 207.55 o -4 11 0 649.22 401.75 151.30 o -3 11 0 4673.97 4593.21 461.71 o -2 11 0 3004.07 3177.42 249.63 o -1 11 0 6713.33 6254.88 530.69 o 0 11 0 14114.78 14603.20 806.19 o 1 11 0 4946.21 4939.72 471.65 o 2 11 0 2653.27 2725.77 351.35 o 3 11 0 761.12 725.39 181.52 o 4 11 0 2674.83 2923.36 361.76 o 5 11 0 3233.00 3307.60 218.34 o 6 11 0 2020.46 478.87 1133.08 o 7 11 0 3741.79 3796.51 337.05 o 8 11 0 2997.86 3332.16 294.40 o 9 11 0 174.86 111.60 67.11 o 10 11 0 152.86 504.72 218.77 o 11 11 0 1081.71 734.30 268.69 o -10 12 0 419.17 115.79 108.79 o -9 12 0 73.02 185.67 128.65 o -8 12 0 121.78 298.76 143.64 o -7 12 0 15185.95 15360.20 906.46 o -6 12 0 1900.23 2064.13 336.18 o -5 12 0 448.42 437.50 172.25 o -4 12 0 109.40 -113.62 104.08 o -3 12 0 4582.20 4935.06 501.62 o -2 12 0 696.75 606.54 116.26 o -1 12 0 1673.60 1914.62 316.64 o 0 12 0 738.69 730.58 198.61 o 1 12 0 13987.80 13722.95 820.14 o 2 12 0 830.00 791.92 203.12 o 3 12 0 273.14 324.15 141.15 o 4 12 0 164.53 0.90 75.53 o 5 12 0 156.13 0.45 57.03 o 6 12 0 74.94 144.22 106.36 o 7 12 0 1391.79 1470.97 269.85 o 8 12 0 225.94 290.42 94.15 o 9 12 0 10892.75 10714.21 549.49 o 10 12 0 1110.00 1353.86 348.41 o -9 13 0 808.97 1023.50 251.99 o -8 13 0 2451.86 2471.95 384.93 o -7 13 0 1482.32 1142.73 271.55 o -6 13 0 1415.65 1084.72 267.45 o -5 13 0 31.96 -44.60 84.20 o -4 13 0 1072.40 1154.58 267.45 o -3 13 0 2867.56 2126.61 353.24 o -2 13 0 3442.08 3385.35 434.65 o -1 13 0 15.51 -128.69 87.63 o 0 13 0 11755.71 11874.99 802.03 o 1 13 0 254.25 290.03 129.12 o 2 13 0 6825.82 6599.40 599.41 o 3 13 0 378.88 493.98 179.17 o 4 13 0 460.45 384.71 152.43 o 5 13 0 3706.10 3759.20 453.03 o 6 13 0 533.56 324.66 149.90 o 7 13 0 2303.25 2180.52 341.48 o 8 13 0 10834.70 10033.80 717.53 o 9 13 0 21.40 -56.13 71.53 o -8 14 0 22.54 -2.38 92.03 o -7 14 0 554.45 257.41 156.01 o -6 14 0 5569.24 5859.28 606.11 o -5 14 0 779.33 795.38 231.71 o -4 14 0 4500.33 4407.93 527.90 o -3 14 0 3261.30 3889.81 485.54 o -2 14 0 581.91 386.25 176.32 o -1 14 0 828.96 725.66 211.98 o 0 14 0 504.18 520.83 186.30 o 1 14 0 2081.57 2087.02 360.89 o 2 14 0 6728.25 8079.36 691.35 o 3 14 0 4414.71 4371.52 506.89 o 4 14 0 5185.82 5579.97 573.55 o 5 14 0 784.53 739.06 222.19 o 6 14 0 59.61 12.38 71.61 o 7 14 0 668.98 282.46 140.82 o 8 14 0 899.75 752.75 195.34 o -6 15 0 259.77 202.29 145.92 o -5 15 0 213.25 220.91 151.60 o -4 15 0 2812.12 2493.88 417.79 o -3 15 0 1273.22 1536.74 327.98 o -2 15 0 13.04 98.42 98.03 o -1 15 0 8.00 -20.56 73.11 o 0 15 0 837.01 754.95 221.35 o 1 15 0 3735.07 3703.91 491.93 o 2 15 0 2428.19 2771.79 433.70 o 3 15 0 276.02 248.19 161.80 o 4 15 0 4020.70 3697.11 493.89 o 5 15 0 4432.91 4249.01 517.04 o 6 15 0 228.32 61.17 93.37 o 7 15 0 703.03 679.09 222.30 o -1 16 0 939.24 1266.84 312.49 o 0 16 0 1125.69 1038.37 279.57 o 1 16 0 1158.36 866.87 266.74 o 2 16 0 533.86 453.25 194.52 o 3 16 0 6580.43 6560.03 677.70 o 4 16 0 21.08 -192.03 128.02 o -4 -16 1 3570.92 3791.73 523.96 o -3 -16 1 13.35 -19.42 96.77 o -2 -16 1 36.16 -0.67 90.30 o -1 -16 1 2458.34 2391.14 419.02 o 0 -16 1 1511.96 1864.49 378.58 o -6 -15 1 2979.32 3012.95 443.62 o -5 -15 1 744.35 679.85 219.29 o -4 -15 1 1079.68 568.92 211.39 o -3 -15 1 2722.87 2020.14 378.12 o -2 -15 1 3735.25 2799.62 437.93 o -1 -15 1 311.09 335.35 141.07 o 0 -15 1 421.75 587.64 208.30 o 1 -15 1 19.66 -145.41 131.42 o 2 -15 1 1060.02 1139.89 284.56 o 3 -15 1 279.55 275.48 151.02 o 4 -15 1 41.55 23.88 118.27 o 5 -15 1 3721.48 4138.14 535.95 o -8 -14 1 1543.44 1949.54 335.92 o -7 -14 1 46.09 64.42 86.97 o -6 -14 1 62.03 17.83 83.50 o -5 -14 1 7754.17 7675.62 682.62 o -4 -14 1 3004.06 3294.11 448.21 o -3 -14 1 30.18 -5.64 60.40 o -2 -14 1 919.44 1113.25 269.99 o -1 -14 1 1651.97 1768.63 325.61 o 0 -14 1 1605.28 1814.39 338.39 o 1 -14 1 718.62 533.72 191.76 o 2 -14 1 298.89 340.59 173.76 o 3 -14 1 11369.40 12475.64 877.15 o 4 -14 1 2019.16 2200.83 374.22 o 5 -14 1 2684.71 2983.49 439.13 o 6 -14 1 783.76 473.90 193.68 o 7 -14 1 2745.00 2315.49 391.00 o 8 -14 1 38.46 106.42 106.74 o -9 -13 1 5529.98 4249.53 476.32 o -8 -13 1 2933.03 2892.64 390.08 o -7 -13 1 443.00 474.84 163.83 o -6 -13 1 3081.90 3123.69 414.37 o -5 -13 1 27.93 -22.05 71.81 o -4 -13 1 3019.21 3136.90 417.67 o -3 -13 1 11.00 -124.26 103.85 o -2 -13 1 620.41 847.12 227.48 o -1 -13 1 14389.65 14074.29 886.43 o 0 -13 1 487.39 217.03 102.59 o 1 -13 1 414.55 284.37 140.56 o 2 -13 1 3993.92 4172.50 487.57 o 3 -13 1 1707.39 1497.73 298.21 o 4 -13 1 2985.11 3020.53 418.84 o 5 -13 1 741.71 767.55 220.14 o 6 -13 1 4365.13 5239.34 552.87 o 7 -13 1 4675.99 4739.71 533.09 o 8 -13 1 32.16 15.56 81.36 o 9 -13 1 238.31 273.49 144.51 o -10 -12 1 2248.45 2049.72 426.89 o -9 -12 1 620.62 442.15 172.68 o -8 -12 1 6596.00 6500.46 435.69 o -7 -12 1 27.22 -145.73 104.20 o -6 -12 1 7.83 -65.20 69.80 o -5 -12 1 387.56 779.57 194.14 o -4 -12 1 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