Acta Cryst. (2011). E67, m150-m151  [ doi:10.1107/S1600536810054115 ]

[₂-Bis(diphenylphosphanyl)methane][₃-bis(diphenylphosphanyl)methyl]trichloridotetragold(I) tetrahydrofuran disolvate

H.-H. Wang, Q. Gao, Y. Cui, L. Wang and Y.-B. Xie

Online 8 January 2011

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.008 Å
• R factor = 0.027
• wR factor = 0.058
• Data-to-parameter ratio = 16.7

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.16      
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.47 Ratio
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         16      
PLAT243_ALERT_4_C High  'Solvent' Ueq as Compared to Neighbors of         C56     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of         C57     
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600          3      

Alert level G
PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c   .......      P21/n      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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