Acta Cryst. (2011). E67, m457  [ doi:10.1107/S1600536811008798 ]

(³-Allyl)bromido(1-phenyl-1H-imidazole-N³)palladium(II)

J. Huang and X. Zhang

Online 15 March 2011

Key indicators

• Single-crystal X-ray study
• T = 566 K
• Mean (C-C) = 0.004 Å
• Disorder in main residue
• R factor = 0.021
• wR factor = 0.049
• Data-to-parameter ratio = 19.4

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        Pd1     
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          3      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600          4      

Alert level G
PLAT301_ALERT_3_G Note: Main Residue  Disorder ...................          6 Perc.
PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels ..........          4      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   3 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   2 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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