Received 4 March 2011
In the title compound, C12H16ClO4P, the phosphonate ring adopts a chair conformation. In the crystal, intermolecular O-HO hydrogen bonds link the molecules into chains propagating along the b axis.
For the synthesis of hydroxyphosphonates, see: Zhou et al. (2008). For the synthesis and biological activity of hydroxyphosphonate derivatives, see: Peng et al. (2007); Liu et al. (2006). For standard bond lengths, see: Allen et al. (1987).
Data collection: SMART (Bruker, 2001); cell refinement: SAINT-Plus (Bruker, 2001); data reduction: SAINT-Plus; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: PLATON (Spek, 2009); software used to prepare material for publication: PLATON.
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: WN2424 ).
We gratefully acknowledge financial support of this work by the National Basic Research Program of China (2010CB126100) and the National Natural Science Foundation of China (Nos. 20772042, 21002037). This work was supported in part by the PCSIRT (No. IRT0953).
Allen, F. H., Kennard, O., Watson, D. G., Brammer, L., Orpen, A. G. & Taylor, R. (1987). J. Chem. Soc. Perkin Trans. 2, pp. S1-19.
Bruker (2001). SMART, SAINT-Plus and SADABS. Bruker AXS Inc., Madison, Wisconsin, USA.
Liu, H., Zhou, Y. G., Yu, Z. K., Xiao, W. J., Liu, S. H. & He, H. W. (2006). Tetrahedron Lett. 62, 11207-11217.
Peng, H., Wang, T., Xie, P., Chen, T., He, H. W. & Wan, J. (2007). J. Agric. Food Chem. 55, 1871-1880.
Sheldrick, G. M. (2008). Acta Cryst. A64, 112-122.
Spek, A. L. (2009). Acta Cryst. D65, 148-155.
Zhou, X., Liu, X. H., Yang, X., Shang, D. J., Xin, J. G. & Feng, X. M. (2008). Angew. Chem. Int. Ed. 47, 392-394.