# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' JDM018_0m in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 333.89 _exptl_crystal_F_000 1280.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.3116 _cell_length_b 11.2435 _cell_length_c 21.2833 _cell_angle_alpha 79.565 _cell_angle_beta 88.961 _cell_angle_gamma 85.125 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.13 -4.44 4.87 o 2 0 0 3380.17 3402.68 68.88 o 3 0 0 15.91 3.74 13.60 o 4 0 0 221.60 261.74 15.10 o 5 0 0 1308.61 1322.14 32.74 o 6 0 0 524.33 601.05 25.50 o 7 0 0 1954.72 1813.18 101.50 o 8 0 0 559.02 469.05 68.38 o 9 0 0 193.03 91.89 45.94 o 10 0 0 290.88 259.64 63.04 o 11 0 0 98.78 99.37 58.77 o 12 0 0 1253.74 1128.30 122.87 o -12 1 0 9.22 103.64 63.04 o -11 1 0 22.81 -11.75 44.88 o -10 1 0 97.70 23.51 38.46 o -9 1 0 19.89 9.62 35.26 o -8 1 0 199.23 240.40 54.49 o -7 1 0 145.68 109.96 30.54 o -6 1 0 2298.12 2582.15 85.79 o -5 1 0 2911.27 3500.10 94.47 o -4 1 0 704.92 762.42 40.61 o -3 1 0 985.55 805.56 37.41 o -2 1 0 1692.32 1576.62 44.86 o -1 1 0 2423.66 2389.99 49.44 o 0 1 0 164.49 14.55 14.42 o 4 1 0 448.54 464.48 31.52 o 5 1 0 26426.54 27194.99 381.96 o 6 1 0 506.65 685.26 58.23 o 7 1 0 930.89 917.65 46.48 o 8 1 0 132.28 139.97 43.81 o 9 1 0 170.45 135.69 47.01 o 10 1 0 176.82 158.13 57.70 o 11 1 0 105.68 131.42 57.70 o 12 1 0 546.58 654.97 104.71 o -11 2 0 243.02 209.42 65.18 o -10 2 0 1051.26 1157.14 106.85 o -9 2 0 764.47 788.51 65.56 o -8 2 0 7.27 20.89 27.47 o -7 2 0 2.74 11.94 21.28 o -6 2 0 568.19 552.94 84.41 o -5 2 0 471.58 529.92 40.28 o -4 2 0 1377.60 1791.80 62.04 o -3 2 0 316.17 335.26 31.94 o -2 2 0 1324.42 1252.99 25.87 o -1 2 0 2535.88 2485.48 37.21 o 0 2 0 234.41 227.30 11.98 o 1 2 0 3115.08 2991.87 63.46 o 4 2 0 140.06 150.65 21.37 o 5 2 0 2103.64 2160.43 70.52 o 6 2 0 189.94 203.81 21.84 o 7 2 0 36.97 48.22 15.08 o 8 2 0 94.66 98.30 41.67 o 9 2 0 1169.58 1245.83 99.37 o 10 2 0 97.37 60.90 43.81 o 11 2 0 102.74 147.45 61.97 o 12 2 0 11.21 22.44 55.56 o -11 3 0 303.18 275.66 75.86 o -10 3 0 339.60 433.36 62.49 o -9 3 0 461.40 501.04 60.03 o -8 3 0 0.20 -5.34 22.67 o -7 3 0 126.73 75.86 45.41 o -6 3 0 135.23 120.27 27.68 o -5 3 0 472.53 403.93 71.59 o -4 3 0 67.48 84.19 20.99 o -3 3 0 482.69 380.41 37.53 o -2 3 0 462.14 361.76 17.01 o -1 3 0 1293.62 1286.51 28.45 o 0 3 0 498.85 501.27 18.20 o 1 3 0 359.80 333.90 20.82 o 2 3 0 1301.62 1349.91 55.03 o 3 3 0 1291.24 1091.97 49.15 o 4 3 0 11606.08 12075.76 252.16 o 5 3 0 87.32 75.86 20.30 o 6 3 0 313.02 300.24 33.12 o 7 3 0 588.26 602.61 43.81 o 8 3 0 794.88 792.49 43.47 o 9 3 0 305.96 364.35 67.31 o 10 3 0 2.72 10.68 39.53 o 11 3 0 1.96 -43.81 42.74 o 12 3 0 162.05 308.79 76.93 o -11 4 0 0.76 -5.01 106.85 o -10 4 0 17.80 40.07 36.24 o -9 4 0 740.72 713.93 64.80 o -8 4 0 29.91 11.19 36.33 o -7 4 0 99.22 68.65 79.60 o -6 4 0 487.18 479.83 46.70 o -5 4 0 1827.07 1865.56 77.41 o -4 4 0 59.80 83.66 11.24 o -3 4 0 2124.17 2033.92 47.19 o -2 4 0 850.52 858.05 28.07 o -1 4 0 123.51 161.04 15.64 o 0 4 0 2053.04 2027.97 39.35 o 1 4 0 45.99 43.45 10.65 o 2 4 0 528.80 547.21 25.31 o 3 4 0 4403.49 4308.19 91.33 o 4 4 0 862.93 893.22 40.02 o 5 4 0 2917.22 3012.00 100.44 o 6 4 0 208.57 242.54 34.19 o 7 4 0 435.18 597.27 49.15 o 8 4 0 941.72 1015.04 60.90 o 9 4 0 1072.69 1062.05 99.37 o 10 4 0 166.79 123.94 51.29 o 11 4 0 87.49 68.38 53.42 o -10 5 0 2875.94 2822.19 110.56 o -9 5 0 3.07 -10.26 29.72 o -8 5 0 202.04 260.34 41.49 o -7 5 0 25.60 38.57 23.78 o -6 5 0 202.97 213.98 33.23 o -5 5 0 204.42 193.43 29.04 o -4 5 0 493.44 555.65 25.62 o -3 5 0 1726.64 1843.54 42.62 o -2 5 0 344.62 362.72 20.98 o -1 5 0 2789.66 2803.70 52.46 o 0 5 0 632.73 599.91 34.84 o 1 5 0 1416.91 1274.31 41.95 o 2 5 0 9240.79 8652.54 131.15 o 3 5 0 2.17 -9.18 12.82 o 4 5 0 193.11 194.20 24.39 o 5 5 0 43.29 44.96 27.78 o 6 5 0 2591.97 2555.13 77.53 o 7 5 0 200.87 219.03 39.53 o 8 5 0 309.00 355.80 48.08 o 9 5 0 1222.81 1209.50 75.86 o 10 5 0 102.92 80.13 51.29 o 11 5 0 28.06 53.42 52.35 o -10 6 0 58.85 50.30 37.73 o -9 6 0 99.35 60.94 36.04 o -8 6 0 863.92 734.93 128.90 o -7 6 0 59.10 62.69 28.63 o -6 6 0 619.52 590.75 56.13 o -5 6 0 202.99 188.88 31.72 o -4 6 0 1644.33 1604.65 42.61 o -3 6 0 176.58 123.81 16.59 o -2 6 0 694.48 648.70 28.11 o -1 6 0 94.29 94.03 14.47 o 0 6 0 224.03 208.98 18.94 o 1 6 0 2834.27 3194.20 71.25 o 2 6 0 5674.77 5642.28 98.85 o 3 6 0 32.91 55.63 17.71 o 4 6 0 5945.50 6274.93 133.24 o 5 6 0 65.68 68.07 20.77 o 6 6 0 575.83 632.53 54.49 o 7 6 0 15160.26 15824.99 362.21 o 8 6 0 3327.83 3629.57 134.63 o 9 6 0 352.67 366.48 53.42 o 11 6 0 157.09 292.76 82.27 o -9 7 0 118.45 95.80 40.93 o -8 7 0 558.21 641.55 62.42 o -7 7 0 755.94 732.07 58.89 o -6 7 0 93.12 125.52 53.02 o -5 7 0 322.07 309.93 45.06 o -4 7 0 83.81 58.05 24.02 o -3 7 0 1.13 25.71 13.53 o -2 7 0 252.77 237.91 22.07 o -1 7 0 524.35 573.93 27.82 o 0 7 0 218.35 227.98 23.60 o 1 7 0 0.01 6.22 11.79 o 2 7 0 395.42 425.22 29.14 o 3 7 0 28.74 24.44 18.16 o 4 7 0 333.32 313.80 36.86 o 5 7 0 0.00 -7.48 22.44 o 6 7 0 264.75 344.04 50.22 o 7 7 0 147.15 141.04 37.40 o 8 7 0 1559.44 1683.90 95.09 o 9 7 0 1650.74 1858.06 103.64 o -9 8 0 291.31 184.07 53.07 o -8 8 0 18.50 -5.82 34.91 o -7 8 0 102.18 85.16 39.73 o -6 8 0 3214.72 3329.37 129.71 o -5 8 0 678.86 746.39 62.11 o -4 8 0 452.26 402.66 52.10 o -3 8 0 399.53 404.69 48.66 o -2 8 0 665.78 719.86 37.69 o -1 8 0 101.06 108.52 20.65 o 0 8 0 9.06 -5.21 14.57 o 1 8 0 753.18 727.73 37.57 o 2 8 0 0.36 -4.27 17.78 o 3 8 0 1320.36 1420.60 61.75 o 4 8 0 41.10 52.35 28.85 o 5 8 0 1.10 -8.55 22.44 o 6 8 0 1977.24 1858.06 100.44 o 7 8 0 1365.56 1502.26 90.82 o 8 8 0 17.15 35.26 32.05 o 9 8 0 16.60 24.57 33.12 o 10 8 0 51.68 39.53 38.46 o -8 9 0 21.98 23.78 43.40 o -7 9 0 25.01 19.95 37.70 o -6 9 0 579.08 612.38 146.91 o -5 9 0 177.09 208.12 45.44 o -4 9 0 93.41 51.81 35.83 o -3 9 0 72.43 103.38 34.65 o -2 9 0 192.14 162.48 25.78 o -1 9 0 230.41 164.18 25.91 o 0 9 0 114.77 108.04 25.41 o 1 9 0 1125.22 1132.52 152.35 o 2 9 0 240.17 307.23 52.35 o 3 9 0 13.34 -13.62 19.24 o 4 9 0 19.96 26.71 27.78 o 5 9 0 28.36 17.10 28.85 o 6 9 0 369.89 426.32 59.83 o 7 9 0 730.33 622.91 65.18 o 8 9 0 531.84 612.23 68.38 o 9 9 0 16.37 -12.82 34.19 o -7 10 0 215.13 168.70 51.95 o -6 10 0 12.27 1.42 36.24 o -5 10 0 411.28 455.64 133.02 o -4 10 0 1.06 32.72 57.70 o -3 10 0 164.65 122.60 40.71 o -2 10 0 74.26 57.11 22.22 o -1 10 0 938.08 983.26 58.11 o 0 10 0 339.19 308.74 33.66 o 1 10 0 14.22 -12.83 17.75 o 2 10 0 569.04 564.10 47.63 o 3 10 0 1220.90 1233.01 84.41 o 4 10 0 5.19 -6.41 27.78 o 5 10 0 290.26 256.43 51.29 o 6 10 0 123.33 146.38 43.81 o 7 10 0 70.35 84.41 38.46 o 8 10 0 108.98 82.27 42.74 o -5 11 0 26.04 77.70 41.85 o -4 11 0 85.09 13.74 35.90 o -3 11 0 396.92 391.88 155.46 o -2 11 0 98.91 65.70 25.15 o -1 11 0 206.92 235.59 33.94 o 0 11 0 62.12 43.77 28.72 o 1 11 0 147.43 107.05 27.30 o 2 11 0 847.05 975.51 79.07 o 3 11 0 42.15 72.66 39.53 o 4 11 0 54.03 48.08 36.33 o 5 11 0 2.74 -8.55 35.26 o 6 11 0 8.05 3.21 34.19 o 7 11 0 40.50 -14.96 33.12 o -4 12 0 201.60 191.96 55.53 o -3 12 0 42.13 64.97 41.57 o -2 12 0 835.57 782.40 73.42 o -1 12 0 916.02 1100.89 58.27 o 0 12 0 293.45 334.59 77.46 o 1 12 0 4.82 -34.96 23.30 o 2 12 0 312.25 349.39 59.83 o 3 12 0 24.22 34.19 33.12 o 4 12 0 26.41 13.89 36.33 o 5 12 0 26.91 44.88 38.46 o 0 13 0 212.93 137.61 43.27 o 1 13 0 8.32 30.99 42.74 o 2 13 0 225.84 286.35 60.90 o -2 -13 1 202.57 410.29 69.45 o -1 -13 1 47.69 -6.41 34.19 o -5 -12 1 223.71 310.92 64.11 o -4 -12 1 34.23 83.34 42.74 o -3 -12 1 104.40 232.92 50.22 o -2 -12 1 239.45 359.00 60.90 o -1 -12 1 60.44 88.68 42.74 o 0 -12 1 480.47 563.96 51.95 o 1 -12 1 20.45 36.55 25.36 o 2 -12 1 377.03 390.21 62.05 o 3 -12 1 233.92 270.77 56.22 o -7 -11 1 107.06 226.51 61.97 o -6 -11 1 90.82 87.61 42.74 o -5 -11 1 520.90 438.07 68.38 o -4 -11 1 169.68 245.75 50.22 o -3 -11 1 50.77 16.03 32.05 o -2 -11 1 599.49 666.72 68.38 o -1 -11 1 35.45 44.66 35.79 o 0 -11 1 64.56 35.85 37.39 o 1 -11 1 634.58 672.84 48.03 o 2 -11 1 100.08 89.11 26.65 o 3 -11 1 16.26 -17.54 34.32 o 4 -11 1 397.26 346.60 59.46 o 5 -11 1 35.02 41.39 53.96 o -8 -10 1 25.66 35.26 41.67 o -7 -10 1 24.14 79.07 37.40 o -6 -10 1 116.59 80.13 39.53 o -5 -10 1 102.20 126.08 41.67 o -4 -10 1 0.06 4.27 29.92 o -3 -10 1 60.99 44.88 32.05 o -2 -10 1 902.48 770.36 67.31 o -1 -10 1 193.17 207.70 29.38 o 0 -10 1 408.50 447.88 40.16 o 1 -10 1 535.14 536.42 40.90 o 2 -10 1 2179.14 2341.35 74.56 o 3 -10 1 600.52 579.73 79.07 o 4 -10 1 5.72 3.13 32.60 o 5 -10 1 0.76 39.23 42.20 o 6 -10 1 36.22 -11.04 36.71 o 7 -10 1 49.53 23.73 39.66 o -9 -9 1 2.23 11.75 37.40 o -8 -9 1 312.75 286.35 55.56 o -7 -9 1 40.80 12.82 30.99 o -6 -9 1 41.41 39.53 34.19 o -5 -9 1 269.39 216.90 44.88 o -4 -9 1 248.89 328.02 52.35 o -3 -9 1 0.21 14.96 26.71 o -2 -9 1 6.51 -5.50 26.71 o -1 -9 1 2279.65 2292.58 106.20 o 0 -9 1 348.89 343.59 33.39 o 1 -9 1 218.41 232.68 41.24 o 2 -9 1 3473.85 3574.00 88.73 o 3 -9 1 953.99 1088.36 71.79 o 4 -9 1 133.47 143.09 40.28 o 5 -9 1 0.00 -6.36 60.90 o 6 -9 1 89.70 114.74 42.57 o 7 -9 1 20.69 -10.36 34.07 o 8 -9 1 33.72 3.36 40.16 o -10 -8 1 161.46 156.00 51.29 o -9 -8 1 3.96 16.03 38.46 o -8 -8 1 305.92 240.40 51.29 o -7 -8 1 221.00 198.73 45.94 o -6 -8 1 1139.25 1131.50 80.13 o -5 -8 1 1.67 26.71 27.78 o -4 -8 1 25.77 25.64 26.71 o -3 -8 1 2850.71 3008.89 90.66 o -2 -8 1 2247.82 2249.96 219.57 o -1 -8 1 17.06 0.08 14.16 o 0 -8 1 20.21 15.91 15.25 o 1 -8 1 974.91 972.73 48.96 o 2 -8 1 25.67 18.52 16.93 o 3 -8 1 122.92 107.84 21.26 o 4 -8 1 324.85 319.47 119.13 o 5 -8 1 0.29 27.78 41.67 o 6 -8 1 360.55 330.38 52.35 o 7 -8 1 36.52 27.11 34.36 o 8 -8 1 270.05 217.13 73.19 o -9 -7 1 72.09 74.79 36.33 o -8 -7 1 108.25 86.55 37.40 o -7 -7 1 32.64 3.21 25.64 o -6 -7 1 5.64 -25.64 21.37 o -5 -7 1 253.32 275.66 44.88 o -4 -7 1 61.89 62.22 20.79 o -3 -7 1 335.73 366.36 29.50 o -2 -7 1 455.24 507.31 31.25 o -1 -7 1 2600.71 2602.80 57.03 o 0 -7 1 37.53 51.93 14.16 o 1 -7 1 704.48 728.56 32.09 o 2 -7 1 91.08 112.80 17.39 o 3 -7 1 748.44 837.68 34.55 o 4 -7 1 12.50 44.80 22.22 o 5 -7 1 114.61 78.08 27.61 o 6 -7 1 263.77 303.96 40.85 o 7 -7 1 313.89 270.18 48.07 o 8 -7 1 463.05 405.72 52.33 o 9 -7 1 202.87 98.08 39.92 o -11 -6 1 11.43 47.01 56.63 o -9 -6 1 602.65 623.98 60.90 o -8 -6 1 179.98 226.51 44.88 o -7 -6 1 1963.05 2066.41 98.30 o -6 -6 1 88.16 114.33 32.05 o -5 -6 1 9.78 7.02 18.16 o -4 -6 1 128.96 123.95 23.28 o -3 -6 1 171.23 145.85 19.74 o -2 -6 1 12.60 40.49 14.58 o -1 -6 1 98.65 130.39 15.74 o 0 -6 1 517.39 498.55 24.71 o 1 -6 1 71.01 49.83 14.81 o 2 -6 1 528.67 541.37 26.75 o 3 -6 1 625.04 582.76 50.61 o 4 -6 1 1163.60 1122.50 36.19 o 5 -6 1 462.24 501.83 42.54 o 6 -6 1 780.46 784.92 51.65 o 7 -6 1 107.78 84.17 29.69 o 8 -6 1 243.03 222.39 40.51 o 9 -6 1 19.07 -21.46 32.21 o 10 -6 1 1.21 99.90 39.49 o -11 -5 1 107.79 166.68 61.97 o -10 -5 1 0.01 -56.09 37.40 o -9 -5 1 384.97 441.27 55.56 o -8 -5 1 1008.68 1078.08 69.45 o -7 -5 1 76.50 72.66 26.71 o -6 -5 1 200.71 188.26 26.43 o -5 -5 1 291.43 249.34 43.81 o -4 -5 1 184.53 221.35 26.18 o -3 -5 1 4117.71 4323.44 81.62 o -2 -5 1 511.00 552.70 27.89 o -1 -5 1 1608.90 1634.02 38.76 o 0 -5 1 3780.13 3870.09 64.51 o 1 -5 1 4807.60 4850.85 75.68 o 2 -5 1 709.36 682.28 43.49 o 3 -5 1 2854.13 3025.36 57.52 o 4 -5 1 1.57 -0.91 8.64 o 5 -5 1 22.89 31.63 24.78 o 6 -5 1 127.74 152.66 30.01 o 7 -5 1 158.43 133.18 46.25 o 8 -5 1 289.09 266.09 41.50 o 9 -5 1 639.61 533.17 57.81 o 10 -5 1 21.09 43.37 35.70 o -11 -4 1 709.27 597.27 98.30 o -10 -4 1 22.87 20.30 42.74 o -9 -4 1 8.67 23.51 37.40 o -8 -4 1 3843.71 3886.00 126.08 o -7 -4 1 534.49 497.90 45.94 o -6 -4 1 520.31 646.42 47.01 o -5 -4 1 43.69 12.82 16.03 o -4 -4 1 599.75 692.02 43.27 o -3 -4 1 152.60 143.39 17.04 o -2 -4 1 1614.95 1555.91 49.67 o -1 -4 1 8181.50 8124.40 103.46 o 0 -4 1 163.38 183.70 20.97 o 1 -4 1 1379.53 1278.45 56.75 o 2 -4 1 4983.94 5058.85 75.02 o 3 -4 1 743.79 750.35 25.20 o 4 -4 1 5393.31 5303.34 119.21 o 5 -4 1 152.17 187.02 28.97 o 6 -4 1 521.74 561.65 52.04 o 7 -4 1 31.96 14.83 24.63 o 8 -4 1 167.62 217.43 42.68 o 9 -4 1 10.21 -35.94 25.29 o 10 -4 1 464.81 442.29 60.43 o 11 -4 1 293.34 320.54 66.90 o -12 -3 1 214.48 176.30 72.66 o -11 -3 1 14.11 23.51 44.88 o -10 -3 1 46.91 -3.21 39.53 o -9 -3 1 1127.36 1236.21 100.44 o -8 -3 1 3.33 -15.12 14.97 o -7 -3 1 808.63 776.77 51.29 o -6 -3 1 511.29 555.60 40.60 o -5 -3 1 919.43 956.27 49.15 o -4 -3 1 60.15 48.08 18.16 o -3 -3 1 330.08 393.13 50.22 o -2 -3 1 355.23 341.55 28.79 o -1 -3 1 4.56 19.45 9.61 o 0 -3 1 3132.51 2995.84 46.83 o 1 -3 1 68.50 77.61 10.75 o 2 -3 1 44.97 39.72 16.25 o 3 -3 1 2085.66 1940.23 44.26 o 4 -3 1 1057.21 1041.41 50.01 o 5 -3 1 30.45 37.61 33.66 o 6 -3 1 127.34 146.01 30.54 o 7 -3 1 306.78 265.40 41.03 o 8 -3 1 15.77 0.78 24.62 o 9 -3 1 2151.64 1974.04 96.78 o 10 -3 1 75.31 78.00 53.42 o 11 -3 1 0.56 -27.78 48.08 o -12 -2 1 152.22 119.67 65.18 o -11 -2 1 1328.39 1333.44 116.46 o -10 -2 1 955.10 790.66 92.96 o -9 -2 1 630.46 751.13 81.20 o -8 -2 1 1001.83 1013.97 85.48 o -7 -2 1 289.95 290.46 25.98 o -6 -2 1 881.35 767.33 35.27 o -5 -2 1 344.73 298.10 27.78 o -4 -2 1 277.64 214.76 24.57 o -3 -2 1 19.84 4.27 12.82 o -2 -2 1 1533.50 1390.79 46.48 o -1 -2 1 1793.14 1871.59 35.74 o 0 -2 1 2209.42 2052.60 36.62 o 1 -2 1 2868.39 2858.48 41.85 o 2 -2 1 17038.63 16320.63 223.11 o 3 -2 1 137.63 130.82 18.78 o 4 -2 1 1282.60 1315.91 53.35 o 5 -2 1 2487.35 2606.91 82.90 o 6 -2 1 962.15 948.21 55.20 o 7 -2 1 3241.84 3286.93 107.38 o 8 -2 1 476.16 459.15 49.50 o 9 -2 1 679.80 699.84 80.13 o 10 -2 1 20.99 11.75 43.81 o 11 -2 1 684.07 507.52 90.82 o -12 -1 1 15.15 -18.16 54.49 o -11 -1 1 199.02 123.94 60.90 o -10 -1 1 686.77 736.17 86.55 o -9 -1 1 236.30 227.58 56.63 o -8 -1 1 282.73 246.81 52.35 o -7 -1 1 8886.84 8638.37 150.99 o -6 -1 1 478.65 451.23 61.97 o -5 -1 1 4550.58 5051.62 107.91 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