Acta Cryst. (2011). E67, m549-m550 [ doi:10.1107/S1600536811012396 ]
Online 7 April 2011
No syntax errors found
Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.14 Ratio PLAT915_ALERT_3_C Low Friedel Pair Coverage ...................... 88 Perc.
Alert level G REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF. From the CIF: _diffrn_reflns_theta_max 26.00 From the CIF: _reflns_number_total 4906 Count of symmetry unique reflns 2697 Completeness (_total/calc) 181.91% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 2209 Fraction of Friedel pairs measured 0.819 Are heavy atom types Z>Si present yes
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 1 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check
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