Acta Cryst. (2011). E67, m663  [ doi:10.1107/S160053681101573X ]

Chloridobis(2-chlorobenzyl)(quinolin-8-olato-²N,O)tin(IV)

T. C. Keng, K. M. Lo and S. W. Ng

Online 7 May 2011

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.005 Å
• R factor = 0.037
• wR factor = 0.086
• Data-to-parameter ratio = 18.6

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT141_ALERT_4_C su on a - Axis Small or Missing (x 100000) .....         10 Ang. 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         31      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         75      
PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density      -1.61 eA-3 

Alert level G
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large.      14.35      
PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c   .......      P21/n      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   4 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   2 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster