Acta Cryst. (2011). E67, m765  [ doi:10.1107/S1600536811017752 ]

Chlorido(1H-imidazole-N³)bis(triphenylphosphane-P)copper(I)

M. Hossaini Sadr, R. Kia and B. Soltani

Online 20 May 2011

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.004 Å
• R factor = 0.046
• wR factor = 0.112
• Data-to-parameter ratio = 22.5

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT241_ALERT_2_B Check High      Ueq as Compared to Neighbors for         C6     

Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.47 Ratio
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         C2     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C36     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C4     
PLAT331_ALERT_2_C Small Average Phenyl   C-C Dist. C4     -C9            1.37 Ang. 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         11      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         26      
PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF ....          2      

Alert level G
PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c   .......      P21/n      
PLAT153_ALERT_1_G The su's on the Cell Axes   are Equal (x 100000)        500 Ang. 
PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X)  Cu1    --  Cl1     ..       6.00 su   
PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X)  Cu1    --  P1      ..      10.67 su   
PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X)  Cu1    --  P2      ..      10.00 su   

   0 ALERT level A = Most likely a serious problem - resolve or explain
   1 ALERT level B = A potentially serious problem, consider carefully
   8 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   5 ALERT level G = General information/check it is not something unexpected

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   9 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster