Acta Cryst. (2011). E67, m796-m797  [ doi:10.1107/S1600536811019118 ]

Bis(-2-{[2-(1,3-benzothiazol-2-yl)hydrazinylidene]methyl}-6-methoxyphenolato)bis[dinitratodysprosium(III)] methanol disolvate

X. Xu, S. Ding, S. Shen, J. Tang and Z. Liu

Online 25 May 2011

Key indicators

• Single-crystal X-ray study
• T = 159 K
• Mean (C-C) = 0.007 Å
• R factor = 0.025
• wR factor = 0.057
• Data-to-parameter ratio = 12.0

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT480_ALERT_4_C Long H...A H-Bond Reported H9A    ..  O3      ..       2.64 Ang. 
PLAT774_ALERT_1_C Suspect X-Y Bond in CIF:   DY1    --  DY1     ..       3.72 Ang. 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.597         56      

Alert level G
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal  (x 10000)        100 Deg. 
PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still          81 Perc.

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   3 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   2 ALERT level G = General information/check it is not something unexpected

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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