Acta Cryst. (2011). E67, m668  [ doi:10.1107/S1600536811015431 ]

trans-Bis{1-[2-(2,6-diisopropylanilino)phenyl]-3-isopropylimidazolin-2-ylidenyl-C²}diiodidopalladium(II) benzene disolvate

C. G. Daly, K. Singh and W. B. Cross

Online 7 May 2011

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.012 Å
• R factor = 0.063
• wR factor = 0.128
• Data-to-parameter ratio = 17.2

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT973_ALERT_2_B Large Calcd. Positive Residual Density on    Pd1       1.52 eA-3 

Alert level C
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C10     
PLAT331_ALERT_2_C Small Average Phenyl   C-C Dist. C25    -C30           1.37 Ang. 
PLAT342_ALERT_3_C Low Bond Precision on  C-C Bonds (x 1000) Ang ..         12      
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          1      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         50      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         14      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   1 ALERT level B = A potentially serious problem, consider carefully
   6 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   0 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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