# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' nw0091 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 300.12 _exptl_crystal_F_000 922.00 _reflns_d_resolution_high 0.8393 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.5234 _cell_length_b 12.8263 _cell_length_c 14.1897 _cell_angle_alpha 75.970 _cell_angle_beta 86.453 _cell_angle_gamma 84.108 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 26493.75 26532.05 389.92 o 2 0 0 60.23 82.25 12.25 o 3 0 0 1969.57 1915.26 34.46 o 4 0 0 10348.00 9691.91 133.74 o 5 0 0 7461.27 7407.03 110.34 o 6 0 0 1235.22 1216.59 33.23 o 7 0 0 198.05 204.84 22.51 o 8 0 0 885.06 770.53 85.34 o 9 0 0 1711.76 2004.75 105.80 o 10 0 0 663.39 703.67 64.88 o 11 0 0 112.62 119.10 37.82 o 12 0 0 0.36 -8.29 22.05 o -12 1 0 282.38 385.82 61.69 o -11 1 0 410.18 359.49 55.95 o -10 1 0 9.72 0.73 17.04 o -9 1 0 306.15 355.67 30.39 o -8 1 0 1310.90 1355.53 51.67 o -7 1 0 1868.88 1961.38 47.92 o -6 1 0 905.91 811.99 26.99 o -5 1 0 250.95 229.56 15.42 o -4 1 0 133.41 104.29 13.97 o -3 1 0 1847.46 1847.19 34.73 o -2 1 0 3586.92 3887.07 112.18 o -1 1 0 59.05 34.08 10.11 o 1 1 0 29049.99 29696.86 431.60 o 2 1 0 17377.59 16949.12 253.40 o 3 1 0 844.24 822.03 24.10 o 4 1 0 1315.59 1324.69 27.73 o 5 1 0 1004.28 950.22 25.01 o 6 1 0 2823.00 2709.38 52.23 o 7 1 0 2867.95 2803.98 76.73 o 8 1 0 35.04 20.76 10.22 o 9 1 0 373.92 395.35 53.22 o 10 1 0 424.89 470.79 35.38 o 11 1 0 487.77 526.06 38.99 o 12 1 0 179.08 151.91 42.74 o -12 2 0 322.62 285.04 56.22 o -11 2 0 243.81 290.42 51.21 o -10 2 0 979.90 1128.04 84.66 o -9 2 0 705.20 740.39 65.06 o -8 2 0 217.56 181.89 34.17 o -7 2 0 1704.97 1599.91 42.55 o -6 2 0 3470.35 3374.19 65.17 o -5 2 0 4901.46 4877.34 81.19 o -4 2 0 998.17 981.39 29.15 o -3 2 0 824.35 914.18 25.93 o -2 2 0 41988.95 42979.36 629.69 o -1 2 0 7101.01 7254.29 177.97 o 0 2 0 8515.68 8802.05 179.79 o 1 2 0 24.40 39.09 6.47 o 2 2 0 2196.79 2157.02 42.98 o 3 2 0 10815.94 10232.39 163.98 o 4 2 0 202.44 172.83 12.84 o 5 2 0 2199.01 2075.38 52.58 o 6 2 0 426.24 390.23 23.31 o 7 2 0 3635.98 3450.49 84.43 o 8 2 0 2202.72 2287.47 68.82 o 9 2 0 1002.41 1078.69 48.12 o 10 2 0 67.07 47.01 31.16 o 11 2 0 252.94 208.40 28.13 o 12 2 0 348.95 359.25 47.43 o -11 3 0 0.21 0.00 25.15 o -10 3 0 224.96 243.67 47.93 o -9 3 0 1487.49 1646.27 97.41 o -8 3 0 1811.26 2056.60 105.80 o -7 3 0 163.99 140.44 22.49 o -6 3 0 34.77 28.68 7.52 o -5 3 0 4481.14 4347.65 85.94 o -4 3 0 8101.82 8396.36 141.17 o -3 3 0 12843.10 12695.69 198.18 o -2 3 0 365.35 356.21 29.62 o -1 3 0 5492.09 5585.66 91.80 o 0 3 0 85.45 75.18 7.11 o 1 3 0 12448.04 12810.74 266.54 o 2 3 0 1702.79 1691.65 52.49 o 3 3 0 117.14 97.73 9.38 o 4 3 0 61.69 38.44 7.76 o 5 3 0 4800.14 4580.83 92.41 o 6 3 0 518.48 479.91 26.22 o 7 3 0 377.74 359.52 25.65 o 8 3 0 199.29 165.70 54.72 o 9 3 0 1219.04 1302.02 53.65 o 10 3 0 1256.20 1409.53 72.63 o 11 3 0 228.22 216.23 33.40 o 12 3 0 0.04 -8.34 14.84 o -11 4 0 318.89 290.32 55.59 o -10 4 0 477.88 428.83 59.05 o -9 4 0 2.02 8.20 21.69 o -8 4 0 1331.82 1366.48 63.32 o -7 4 0 2917.68 3086.41 133.68 o -6 4 0 2748.17 2740.78 107.62 o -5 4 0 143.81 142.44 18.56 o -4 4 0 9291.87 9839.42 268.73 o -3 4 0 4334.17 4085.14 135.14 o -2 4 0 1859.40 1730.28 74.36 o -1 4 0 81.28 87.28 6.30 o 0 4 0 2844.52 2856.91 55.95 o 1 4 0 16685.67 15458.75 321.22 o 2 4 0 7204.88 6865.37 159.65 o 3 4 0 8836.56 8429.17 195.74 o 4 4 0 34.48 14.62 5.52 o 5 4 0 1517.91 1382.53 42.44 o 6 4 0 522.18 489.20 25.89 o 7 4 0 619.64 622.52 36.18 o 8 4 0 1279.07 1283.37 50.72 o 9 4 0 0.73 -7.63 9.45 o 10 4 0 326.19 373.73 75.45 o 11 4 0 256.63 250.39 31.00 o 12 4 0 230.44 307.46 35.26 o -11 5 0 460.83 477.50 66.43 o -10 5 0 698.89 843.45 78.64 o -9 5 0 953.97 843.91 75.63 o -8 5 0 328.76 251.96 44.56 o -7 5 0 755.34 843.65 49.78 o -6 5 0 3080.42 3163.76 98.40 o -5 5 0 6227.72 6363.63 204.76 o -4 5 0 3883.64 3916.92 142.34 o -3 5 0 653.72 669.13 49.94 o -2 5 0 7705.33 7989.31 223.71 o -1 5 0 394.17 351.27 14.76 o 0 5 0 3645.27 3855.29 74.32 o 1 5 0 35.96 -1.00 3.28 o 2 5 0 7983.46 7944.02 184.35 o 3 5 0 7274.81 7188.04 175.05 o 4 5 0 7081.73 6829.92 172.77 o 5 5 0 1305.90 1260.08 56.86 o 6 5 0 48.98 29.60 8.90 o 7 5 0 456.95 415.89 29.24 o 8 5 0 992.76 906.09 65.56 o 9 5 0 1315.57 1285.84 55.14 o 10 5 0 331.98 285.04 31.53 o 11 5 0 6.59 -4.07 14.34 o 12 5 0 145.19 114.05 25.80 o -10 6 0 284.21 280.03 54.58 o -9 6 0 514.74 502.74 64.52 o -8 6 0 1458.75 1514.55 74.88 o -7 6 0 1426.26 1397.34 82.06 o -6 6 0 2.14 -6.58 14.64 o -5 6 0 2037.19 1954.36 100.78 o -4 6 0 6046.05 6159.33 201.02 o -3 6 0 3623.46 3536.75 133.86 o -2 6 0 1732.76 1641.07 82.10 o -1 6 0 2650.00 2805.54 59.22 o 0 6 0 2444.28 2417.37 62.97 o 1 6 0 8552.21 8636.02 196.19 o 2 6 0 4434.93 4720.10 124.39 o 3 6 0 2.45 8.02 7.84 o 4 6 0 1050.60 957.73 48.21 o 5 6 0 2340.39 2380.10 86.57 o 6 6 0 1689.60 1624.76 72.17 o 7 6 0 323.35 309.73 38.36 o 8 6 0 2.42 4.31 9.81 o 9 6 0 100.51 133.25 21.95 o 10 6 0 526.70 534.77 40.55 o 11 6 0 268.27 276.83 33.21 o -10 7 0 89.16 82.29 38.55 o -9 7 0 13.93 20.05 26.88 o -8 7 0 488.09 470.48 56.32 o -7 7 0 1651.42 1700.72 79.39 o -6 7 0 1444.43 1454.00 80.28 o -5 7 0 477.24 526.61 57.68 o -4 7 0 153.47 130.31 32.35 o -3 7 0 3451.98 3207.88 130.76 o -2 7 0 7462.76 7366.56 227.45 o -1 7 0 1341.17 1451.00 39.32 o 0 7 0 301.53 295.59 29.89 o 1 7 0 1518.96 1566.08 56.41 o 2 7 0 5095.83 5267.49 138.78 o 3 7 0 5037.95 5434.98 147.17 o 4 7 0 642.58 566.34 38.18 o 5 7 0 1.96 -3.01 8.75 o 6 7 0 766.63 792.37 37.05 o 7 7 0 1515.00 1602.25 81.83 o 8 7 0 228.68 175.42 33.17 o 9 7 0 107.80 123.84 32.44 o 10 7 0 0.54 -12.94 15.31 o 11 7 0 247.82 219.06 44.10 o -9 8 0 863.82 845.09 85.48 o -8 8 0 445.20 384.70 46.94 o -7 8 0 541.70 509.82 49.98 o -6 8 0 1060.74 1149.06 66.45 o -5 8 0 2241.81 2094.33 113.82 o -4 8 0 2634.99 2738.13 128.76 o -3 8 0 37.84 3.10 17.50 o -2 8 0 88.04 50.85 26.24 o -1 8 0 2122.99 2248.06 110.44 o 0 8 0 1760.97 1867.00 51.68 o 1 8 0 1649.35 1682.17 61.24 o 2 8 0 41.38 -0.82 6.20 o 3 8 0 2156.87 2091.14 78.37 o 4 8 0 2543.32 2729.47 96.68 o 5 8 0 1941.25 1951.99 82.01 o 6 8 0 123.11 100.60 26.79 o 7 8 0 42.58 11.57 15.22 o 8 8 0 223.77 236.93 37.54 o 9 8 0 396.80 303.26 44.20 o 10 8 0 318.74 312.74 47.48 o 11 8 0 22.96 14.49 24.15 o -9 9 0 502.97 461.25 55.81 o -8 9 0 876.87 934.35 69.62 o -7 9 0 960.20 806.43 62.62 o -6 9 0 25.76 17.96 22.35 o -5 9 0 1360.61 1188.36 89.94 o -4 9 0 3058.51 3288.80 149.17 o -3 9 0 2345.75 2250.43 118.64 o -2 9 0 309.09 257.06 45.93 o -1 9 0 49.18 61.78 27.43 o 0 9 0 603.79 680.61 62.88 o 1 9 0 688.70 648.97 31.10 o 3 9 0 690.53 671.32 42.56 o 4 9 0 113.39 92.13 20.69 o 5 9 0 848.51 803.32 38.23 o 6 9 0 810.49 767.55 57.32 o 7 9 0 323.10 327.23 41.28 o 8 9 0 1.23 0.55 16.04 o 9 9 0 151.39 113.00 31.71 o 10 9 0 215.64 202.75 41.10 o -8 10 0 45.25 72.74 40.05 o -7 10 0 910.03 874.26 83.47 o -6 10 0 1532.93 1603.01 84.69 o -5 10 0 300.02 229.54 50.12 o -4 10 0 209.99 155.28 41.92 o -3 10 0 2971.25 2550.78 133.68 o -2 10 0 4498.29 4727.66 193.64 o -1 10 0 1928.76 1970.95 117.73 o 0 10 0 599.77 642.34 70.44 o 1 10 0 108.16 99.96 34.72 o 2 10 0 2415.16 2577.93 90.03 o 3 10 0 1758.10 2020.15 81.92 o 4 10 0 365.15 307.73 37.82 o 5 10 0 19.76 11.85 16.49 o 6 10 0 118.02 114.09 28.70 o 7 10 0 581.15 463.83 49.03 o 8 10 0 858.61 635.32 58.87 o 9 10 0 83.44 60.51 26.34 o -7 11 0 0.93 -6.24 26.64 o -6 11 0 519.76 475.32 96.96 o -5 11 0 618.61 606.98 75.91 o -4 11 0 87.13 59.05 34.72 o -3 11 0 168.76 198.65 50.21 o -2 11 0 942.30 928.02 88.94 o -1 11 0 2314.29 2288.33 135.41 o 0 11 0 1541.53 1687.18 113.27 o 1 11 0 645.16 568.07 66.70 o 2 11 0 38.61 16.86 26.34 o 3 11 0 729.76 638.97 49.39 o 4 11 0 600.14 570.81 48.48 o 5 11 0 603.31 482.87 47.48 o 6 11 0 251.78 243.40 36.72 o 7 11 0 10.34 1.28 17.13 o 8 11 0 238.97 175.23 35.08 o 9 11 0 231.94 256.06 41.92 o -6 12 0 73.29 88.48 56.95 o -5 12 0 43.18 40.92 37.82 o -4 12 0 557.22 400.77 66.25 o -3 12 0 669.34 680.98 81.65 o -2 12 0 1010.06 949.25 94.68 o -1 12 0 282.89 269.00 61.60 o 0 12 0 180.85 275.84 58.59 o 1 12 0 503.54 610.54 73.54 o 2 12 0 88.98 66.70 33.90 o 4 12 0 4.15 9.48 15.95 o 5 12 0 277.91 256.61 38.45 o 6 12 0 610.71 546.84 53.76 o 7 12 0 258.05 149.81 32.53 o 8 12 0 33.99 20.05 19.32 o -3 13 0 118.36 27.61 39.46 o -2 13 0 1106.29 1210.42 108.35 o -1 13 0 1423.64 1487.34 120.92 o 0 13 0 720.44 756.79 88.57 o 1 13 0 100.48 78.91 42.37 o 2 13 0 10.05 -22.33 25.97 o 3 13 0 282.01 277.38 55.77 o 5 13 0 145.26 82.83 28.61 o 6 13 0 11.07 -7.65 18.23 o 0 14 0 306.45 313.83 68.89 o 1 14 0 184.44 278.93 63.33 o 2 14 0 230.69 75.91 43.56 o 3 14 0 18.96 8.66 32.53 o -4 -14 1 184.69 141.70 52.76 o -3 -14 1 510.10 436.40 69.89 o -2 -14 1 263.83 238.11 60.87 o -1 -14 1 96.27 49.12 43.65 o 0 -14 1 2.69 9.84 42.46 o 1 -14 1 310.65 290.14 70.99 o 2 -14 1 484.75 534.45 89.76 o -6 -13 1 233.22 218.70 40.37 o -5 -13 1 171.75 123.20 31.07 o -3 -13 1 27.48 38.00 32.81 o -2 -13 1 377.96 279.39 58.41 o -1 -13 1 637.37 651.36 84.38 o 0 -13 1 575.25 449.98 75.27 o 1 -13 1 49.83 59.14 47.20 o 2 -13 1 317.83 277.38 67.07 o 3 -13 1 416.00 423.09 75.45 o 4 -13 1 506.37 488.52 77.91 o -7 -12 1 44.67 18.32 21.60 o -6 -12 1 37.13 25.61 21.69 o -5 -12 1 613.26 583.20 55.59 o -4 -12 1 344.70 338.71 41.92 o -2 -12 1 174.53 100.88 39.55 o -1 -12 1 145.75 123.11 45.47 o 0 -12 1 1647.82 1820.68 129.58 o 1 -12 1 1667.33 1637.88 125.21 o 2 -12 1 239.50 295.06 63.33 o 3 -12 1 10.09 32.62 36.45 o 4 -12 1 76.33 28.70 33.63 o 5 -12 1 551.80 454.53 74.36 o 6 -12 1 765.17 824.68 95.68 o -8 -11 1 200.00 144.98 35.17 o -7 -11 1 448.86 438.59 50.76 o -6 -11 1 492.10 429.84 49.21 o -5 -11 1 121.26 87.75 27.61 o -4 -11 1 125.87 75.73 25.15 o -3 -11 1 631.91 549.76 45.74 o -2 -11 1 1314.80 1204.49 91.67 o -1 -11 1 402.09 367.51 59.05 o 0 -11 1 115.86 78.64 40.10 o 1 -11 1 1495.10 1682.99 119.10 o 2 -11 1 3158.88 3233.48 170.40 o 3 -11 1 642.64 898.13 92.22 o 4 -11 1 97.21 78.19 38.45 o 5 -11 1 1.12 -5.19 28.25 o 6 -11 1 574.50 533.72 76.18 o 7 -11 1 1098.50 1240.15 84.53 o -9 -10 1 224.59 218.34 40.92 o -8 -10 1 30.69 4.83 16.86 o -7 -10 1 133.92 129.22 31.80 o -6 -10 1 218.49 186.72 34.63 o -5 -10 1 229.76 232.55 35.36 o -4 -10 1 712.87 832.15 56.68 o -3 -10 1 49.86 15.49 14.76 o -2 -10 1 818.31 894.76 51.39 o -1 -10 1 1419.29 1437.95 97.32 o 0 -10 1 733.34 929.20 83.47 o 1 -10 1 3.69 -4.19 23.33 o 2 -10 1 236.49 187.90 47.93 o 3 -10 1 2294.16 2074.65 126.21 o 4 -10 1 1980.19 1998.56 122.75 o 5 -10 1 380.08 338.62 59.23 o 6 -10 1 138.16 96.23 40.92 o 7 -10 1 374.17 397.52 52.22 o 8 -10 1 516.19 542.17 128.40 o -10 -9 1 40.65 5.47 20.59 o -9 -9 1 230.94 228.18 41.92 o -8 -9 1 972.30 902.96 68.53 o -7 -9 1 252.71 292.69 41.37 o -6 -9 1 0.14 0.36 13.49 o -5 -9 1 11.94 -1.46 13.12 o -4 -9 1 1159.86 1074.37 62.33 o -3 -9 1 1336.10 1505.02 70.08 o -2 -9 1 14.57 43.01 16.58 o -1 -9 1 837.26 765.69 35.46 o 0 -9 1 835.59 892.57 76.27 o 1 -9 1 1069.54 1031.35 83.56 o 2 -9 1 1397.56 1432.85 99.24 o 3 -9 1 684.65 574.18 65.79 o 4 -9 1 130.64 192.64 44.47 o 5 -9 1 1219.71 1100.88 89.21 o 6 -9 1 1034.56 980.96 86.75 o 7 -9 1 280.39 317.26 46.34 o 8 -9 1 69.87 97.84 34.52 o 9 -9 1 187.97 99.78 45.74 o -10 -8 1 174.35 226.17 43.19 o -9 -8 1 2.89 -3.92 17.68 o -8 -8 1 164.78 135.87 32.62 o -7 -8 1 816.22 916.54 63.61 o -6 -8 1 1469.36 1373.62 76.00 o -5 -8 1 777.03 766.64 53.58 o -4 -8 1 51.30 37.09 18.13 o -3 -8 1 280.77 235.74 28.61 o -2 -8 1 1822.10 1865.51 72.17 o -1 -8 1 575.35 551.76 33.90 o 0 -8 1 170.61 187.13 18.41 o 1 -8 1 681.43 755.15 66.25 o 2 -8 1 2074.65 2342.46 119.37 o 3 -8 1 4635.78 4366.63 174.14 o 4 -8 1 4199.50 4107.74 169.22 o 5 -8 1 592.23 427.38 58.87 o 6 -8 1 89.62 68.43 31.07 o 7 -8 1 1290.53 1366.31 76.36 o 8 -8 1 820.62 797.57 63.44 o 9 -8 1 192.64 210.77 52.49 o -11 -7 1 30.71 33.72 24.06 o -10 -7 1 529.88 518.41 58.23 o -9 -7 1 309.45 333.52 45.93 o -8 -7 1 11.36 11.12 15.31 o -7 -7 1 8.27 1.73 12.39 o -6 -7 1 2256.82 2331.89 98.96 o -5 -7 1 4758.57 4716.73 148.26 o -4 -7 1 499.43 448.52 37.73 o -3 -7 1 24.94 55.95 16.86 o -2 -7 1 648.35 646.53 38.55 o -1 -7 1 10141.52 10539.08 238.66 o 0 -7 1 1428.60 1511.04 43.82 o 1 -7 1 2988.70 3136.71 67.54 o 2 -7 1 261.77 302.63 43.83 o 3 -7 1 1494.26 1461.01 87.75 o 4 -7 1 3462.76 3443.25 146.44 o 5 -7 1 2013.71 1921.83 107.89 o 6 -7 1 665.18 605.98 65.97 o 7 -7 1 58.95 63.71 25.47 o 8 -7 1 912.22 837.36 61.66 o 9 -7 1 1012.81 1031.90 91.76 o 10 -7 1 398.91 332.79 62.06 o -11 -6 1 47.35 37.73 27.61 o -10 -6 1 69.40 12.85 19.59 o -9 -6 1 543.74 576.91 55.95 o -8 -6 1 1383.89 1463.47 81.01 o -7 -6 1 2573.30 2665.68 108.35 o -6 -6 1 57.37 73.54 21.69 o -5 -6 1 64.06 43.65 17.13 o -4 -6 1 908.42 849.65 48.84 o -3 -6 1 3628.34 3571.29 109.44 o -2 -6 1 3703.97 3609.83 104.52 o -1 -6 1 110.07 126.12 16.22 o 0 -6 1 1529.47 1737.75 45.51 o 1 -6 1 11227.68 12990.83 211.64 o 2 -6 1 7107.72 6685.03 210.68 o 3 -6 1 855.20 885.10 63.70 o 4 -6 1 5.92 -2.73 15.22 o 5 -6 1 413.18 354.11 48.30 o 6 -6 1 781.04 830.70 69.89 o 7 -6 1 795.17 882.51 85.29 o 8 -6 1 344.81 304.03 40.21 o 9 -6 1 100.91 139.79 41.10 o 10 -6 1 435.05 337.35 60.60 o -11 -5 1 386.02 379.28 43.28 o -10 -5 1 242.61 208.40 27.42 o -9 -5 1 9.43 6.39 11.80 o -8 -5 1 817.01 807.11 40.91 o -7 -5 1 2447.80 2413.63 70.75 o -6 -5 1 3022.57 3172.98 112.18 o -5 -5 1 1000.06 1064.62 55.86 o -4 -5 1 313.33 287.14 28.80 o -3 -5 1 1564.98 1524.07 60.69 o -2 -5 1 3130.21 3122.13 91.03 o -1 -5 1 12187.18 12679.52 273.10 o 0 -5 1 3761.89 4255.20 104.16 o 1 -5 1 153.20 148.20 9.84 o 2 -5 1 8278.92 8075.15 232.28 o 3 -5 1 8088.32 8409.39 243.21 o 4 -5 1 5922.51 5690.77 188.99 o 5 -5 1 312.14 286.77 40.55 o 6 -5 1 528.09 494.35 55.13 o 7 -5 1 994.28 995.22 56.23 o 8 -5 1 1213.89 1224.17 114.54 o 9 -5 1 840.94 926.38 82.10 o 10 -5 1 19.33 19.32 27.79 o 11 -5 1 150.37 129.76 44.29 o -12 -4 1 0.42 4.29 15.98 o -11 -4 1 104.52 91.58 22.28 o -10 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