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Acta Cryst. (2011). E67, o1866-o1867  [ doi:10.1107/S1600536811025128 ]

Benzyl N-(2-hydroxy-1-{N'-[(1E)-2-hydroxybenzylidene]hydrazinecarbonyl}ethyl)carbamate

E. R. T. Tiekink, M. V. N. de Souza, A. C. Pinheiro, S. M. S. V. Wardell and J. L. Wardell

Online 30 June 2011


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Alert level C PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0055 Ang PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2 PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 8
Alert level G REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF. From the CIF: _diffrn_reflns_theta_max 27.48 From the CIF: _reflns_number_total 2034 Count of symmetry unique reflns 2044 Completeness (_total/calc) 99.51% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 0 Fraction of Friedel pairs measured 0.000 Are heavy atom types Z>Si present no PLAT005_ALERT_5_G No _iucr_refine_instruction_details found in CIF ? PLAT791_ALERT_4_G Note: The Model has Chirality at C9 (Verify) S
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 3 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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